Ines Mössinger, Lukas Raps, Daniel Fricke, Jonathan Freund, Miriam Löbbecke, Ashley R Chadwick
{"title":"原位自动纤维铺放碳纤维增强低熔聚芳醚酮层压板的特性,第 1 部分:生产影响因素","authors":"Ines Mössinger, Lukas Raps, Daniel Fricke, Jonathan Freund, Miriam Löbbecke, Ashley R Chadwick","doi":"10.1177/00219983241244882","DOIUrl":null,"url":null,"abstract":"This study presents an investigation into mechanical and thermal properties, as well as the microstructure of Automated Fiber Placement-manufactured laminates using a novel carbon fiber-reinforced low-melt polyaryl ether ketone polymer material. The material’s lower melting temperature and lower melt viscosity as compared to established high-temperature thermoplastic materials as PEEK, promises favourable characteristics for the Automated Fiber Placement process. This work aims at in-situ consolidation and the influence of a heated tooling and a post process tempering step, which both turned out to be promising in previous investigations. Laminates were manufactured using a cold tooling, a heated tooling configuration, a cold tooling with a subsequent tempering process step and a hot-pressed reference laminate. Differential Scanning Calorimetry showed that crystallinity values more than doubled for the heated tooling and post process tempering configurations, compared to the cold tooling, reaching 24% and 30%, respectively. Mechanical strength values showed an increase in interlaminar shear strength and compression strength but did not increase to the same extent as was expected from the increase in crystallinity. With Scanning Electron Microscopy differences in the microscopic structure of the polymer matrix could be detected. While the post process tempering step leads to a mostly lamellar crystalline structure, the heated tooling configuration and the post process hot pressing induce a predominance of crystalline spherulites, which might positively affect the mechanical performance. Computed Tomography scans revealed a high amount of porosity in the in-situ-manufactured samples and unprocessed tape material, which likely mitigated the positive effect of increased crystallinity.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":"6 1","pages":""},"PeriodicalIF":2.3000,"publicationDate":"2024-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Characteristics of in-situ automated fiber placement carbon-fiber-reinforced low-melt polyaryl ether ketone laminates part 1: Manufacturing influences\",\"authors\":\"Ines Mössinger, Lukas Raps, Daniel Fricke, Jonathan Freund, Miriam Löbbecke, Ashley R Chadwick\",\"doi\":\"10.1177/00219983241244882\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"This study presents an investigation into mechanical and thermal properties, as well as the microstructure of Automated Fiber Placement-manufactured laminates using a novel carbon fiber-reinforced low-melt polyaryl ether ketone polymer material. The material’s lower melting temperature and lower melt viscosity as compared to established high-temperature thermoplastic materials as PEEK, promises favourable characteristics for the Automated Fiber Placement process. This work aims at in-situ consolidation and the influence of a heated tooling and a post process tempering step, which both turned out to be promising in previous investigations. Laminates were manufactured using a cold tooling, a heated tooling configuration, a cold tooling with a subsequent tempering process step and a hot-pressed reference laminate. Differential Scanning Calorimetry showed that crystallinity values more than doubled for the heated tooling and post process tempering configurations, compared to the cold tooling, reaching 24% and 30%, respectively. Mechanical strength values showed an increase in interlaminar shear strength and compression strength but did not increase to the same extent as was expected from the increase in crystallinity. With Scanning Electron Microscopy differences in the microscopic structure of the polymer matrix could be detected. While the post process tempering step leads to a mostly lamellar crystalline structure, the heated tooling configuration and the post process hot pressing induce a predominance of crystalline spherulites, which might positively affect the mechanical performance. Computed Tomography scans revealed a high amount of porosity in the in-situ-manufactured samples and unprocessed tape material, which likely mitigated the positive effect of increased crystallinity.\",\"PeriodicalId\":15489,\"journal\":{\"name\":\"Journal of Composite Materials\",\"volume\":\"6 1\",\"pages\":\"\"},\"PeriodicalIF\":2.3000,\"publicationDate\":\"2024-04-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Composite Materials\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1177/00219983241244882\",\"RegionNum\":3,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"MATERIALS SCIENCE, COMPOSITES\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Composite Materials","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1177/00219983241244882","RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, COMPOSITES","Score":null,"Total":0}
Characteristics of in-situ automated fiber placement carbon-fiber-reinforced low-melt polyaryl ether ketone laminates part 1: Manufacturing influences
This study presents an investigation into mechanical and thermal properties, as well as the microstructure of Automated Fiber Placement-manufactured laminates using a novel carbon fiber-reinforced low-melt polyaryl ether ketone polymer material. The material’s lower melting temperature and lower melt viscosity as compared to established high-temperature thermoplastic materials as PEEK, promises favourable characteristics for the Automated Fiber Placement process. This work aims at in-situ consolidation and the influence of a heated tooling and a post process tempering step, which both turned out to be promising in previous investigations. Laminates were manufactured using a cold tooling, a heated tooling configuration, a cold tooling with a subsequent tempering process step and a hot-pressed reference laminate. Differential Scanning Calorimetry showed that crystallinity values more than doubled for the heated tooling and post process tempering configurations, compared to the cold tooling, reaching 24% and 30%, respectively. Mechanical strength values showed an increase in interlaminar shear strength and compression strength but did not increase to the same extent as was expected from the increase in crystallinity. With Scanning Electron Microscopy differences in the microscopic structure of the polymer matrix could be detected. While the post process tempering step leads to a mostly lamellar crystalline structure, the heated tooling configuration and the post process hot pressing induce a predominance of crystalline spherulites, which might positively affect the mechanical performance. Computed Tomography scans revealed a high amount of porosity in the in-situ-manufactured samples and unprocessed tape material, which likely mitigated the positive effect of increased crystallinity.
期刊介绍:
Consistently ranked in the top 10 of the Thomson Scientific JCR, the Journal of Composite Materials publishes peer reviewed, original research papers from internationally renowned composite materials specialists from industry, universities and research organizations, featuring new advances in materials, processing, design, analysis, testing, performance and applications. This journal is a member of the Committee on Publication Ethics (COPE).