Konstantinos Dimitriadis, Dilshat U Tulyaganov, Simeon Agathopoulos
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引用次数: 0
摘要
这项研究的目的是按照 ISO 9693 标准检测氧化锆和陶瓷贴面之间的粘结强度。我们使用两种商用氧化锆(VITA YZ-HTWhite 和 Zolid HT+ White,分别称为 A 组和 B 组)和一种陶瓷贴面材料(Zirkonia 750)制作了总共 50 个氧化锆/陶瓷贴面系统试样。对两组材料的微观结构(通过 X 射线衍射分析 XRD 和二次电子模式 SEM)和机械性能(通过三点弯曲测试)进行了评估。然后,根据 ISO 9693 和用于生产氧化锆/陶瓷贴面修复体的传统规程进行了实验。通过三点弯曲试验测得的粘接强度值为:A 组为 34.42 ± 7.60 兆帕,B 组为 31.92 ± 6.95 兆帕。通过 SEM 扫描仪观察粘合断裂表面(瓷面),并使用 Shapiro-Wilk 检验法检查正态性,表明采用了 Weibull 统计分析方法。A 组和 B 组的中位强度(σ50%)分别为 34.76 和 32.22 兆帕,而特征强度(σ63.2%)分别为 35.78 和 33.14 兆帕。各组之间的 Weibull 模量差异(12.69 和 13.07)并不显著。粘接强度超过了 ISO 9693 规定的 20 兆帕的最低值,这表明临床使用的粘接强度令人满意。
Evaluation of bond strength between zirconia milled ceramic material and veneered dental porcelain
This study aimed at examining the bond strength between zirconia and ceramic veneer, following the ISO 9693 guidelines. A total of fifty specimens of zirconia/ceramic-veneer system were produced using two commercial zirconias (VITA YZ-HTWhite and Zolid HT+ White, referred to as Group A and Group B, respectively) and a ceramic-veneering material (Zirkonia 750). The microstructure (via x-ray diffraction analysis, XRD and Secondary Electron mode, SEM) and the mechanical properties (via 3-point bending tests) of the two groups were assessed. Then, experiments were conducted according to the ISO 9693 and conventional protocols applied for producing zirconia/ceramic-veneer restorations. Bond strength values, measured by 3-point bending tests, were 34.42 ± 7.60 MPa for Group A and 31.92 ± 6.95 MPa for Group B. SEM observations of the cohesively fractured surfaces (on the porcelain side) and the examination for normality using the Shapiro–Wilk test suggested the use of Weibull statistical analysis. Median strength (σ50%) for Group A and Group B was 34.76 and 32.22 MPa, while the characteristic strength (σ63.2%) was 35.78 and 33.14 MPa, respectively. The Weibull modulus disparity between groups (12.69 and 13.07) was not significant. Bond strength exceeded the ISO 9693 minimum of 20 MPa, suggesting satisfactory strength for clinical use.
期刊介绍:
The European Journal of Oral Sciences is an international journal which publishes original research papers within clinical dentistry, on all basic science aspects of structure, chemistry, developmental biology, physiology and pathology of relevant tissues, as well as on microbiology, biomaterials and the behavioural sciences as they relate to dentistry. In general, analytical studies are preferred to descriptive ones. Reviews, Short Communications and Letters to the Editor will also be considered for publication.
The journal is published bimonthly.