DLP 3D 打印技术的进步:用于生物医学应用的高强度氧化铝增韧氧化锆陶瓷

IF 2.9 Q1 MATERIALS SCIENCE, CERAMICS Open Ceramics Pub Date : 2024-05-06 DOI:10.1016/j.oceram.2024.100601
Tamanna Thakur, Maria Carretta, Dmitrii Komissarenko, Gurdial Blugan
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引用次数: 0

摘要

数字光处理技术(DLP)可利用感光陶瓷浆料生产复杂的陶瓷部件。氧化锆(ZrO2)和氧化铝(Al2O3)是常用的研究对象,但它们的复合材料尽管应用广泛,却未得到充分开发。本研究使用专为聚合物打印设计的低成本台式 DLP 打印机,研究如何制造高强度、全致密氧化铝增韧氧化锆(ATZ)部件。研究人员制备了含有不同粘合剂和分散剂的各种 ATZ 基陶瓷浆料(30、35、42.5vol%),并对其固化和流变特性进行了评估。前景看好的配方经过脱胶和烧结,形成了两种相混合均匀的微结构。对于掺杂样品,扫描电镜分析表明,掺杂剂分布良好,在较高温度下注入的掺杂剂晶粒细长。35 Vol% ATZ 的平均抗折强度高达 1321 兆帕,超过了以前的 DLP 制成的复合材料。这表明无需增加固体负荷含量。这些发现证明了 DLP 在生产具有定制特性的高性能陶瓷部件方面的潜力。
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Advancements in DLP 3D printing: High strength alumina toughened zirconia ceramics for biomedical applications

Digital Light Processing (DLP) enables intricate ceramic part production from photosensitive ceramic slurry. While ZrO2 and Al2O3 are commonly studied, their composites are underexplored despite diverse applications. This study investigates fabricating high-strength, fully dense alumina-toughened zirconia (ATZ) parts using a low-cost desktop DLP printer designed for polymer printing. Various ATZ-based ceramic slurries (30, 35, 42.5 vol%) with different binders and dispersants were prepared and evaluated for curing and rheological properties. Promising formulations underwent debinding and sintering, resulting in homogenous microstructures with a well-distributed blend of the two phases. For the doped samples, SEM analysis revealed a good distribution of dopants and elongated dopant grains infused at higher temperatures. The 35 vol% ATZ exhibited exceptional average flexural strength of 1321 MPa, surpassing previous DLP-fabricated composites. This suggests no need for increased solid loading content. The findings demonstrate the potential of DLP in producing high-performance ceramic parts with tailored properties.

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来源期刊
Open Ceramics
Open Ceramics Materials Science-Materials Chemistry
CiteScore
4.20
自引率
0.00%
发文量
102
审稿时长
67 days
期刊最新文献
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