Yu. F. Ivanov, V. E. Gromov, T. P. Guseva, A. S. Chapaikin, E. S. Vashchuk, D. A. Romanov
{"title":"经脉冲电子束辐照的高速钢保护层的结构和特性","authors":"Yu. F. Ivanov, V. E. Gromov, T. P. Guseva, A. S. Chapaikin, E. S. Vashchuk, D. A. Romanov","doi":"10.1134/S102745102402006X","DOIUrl":null,"url":null,"abstract":"<p>The methods of light, scanning, and transmission electron microscopy are used to study the structure, phase composition, and properties of multilayer plasma surfacings made of high-speed steel R18YU in a protective-alloying nitrogen medium, followed by a fourfold high-temperature tempering and additional electron beam processing. After tempering, the deposited layer on the 30KHGSA high-speed steel R18YU has a polycrystalline structure with a cell size of 7–22.5 µm with layers of the second phase along the boundaries and at the joints of the grains. It is shown that the irradiation of surfaised layers with a pulsed electron beam (energy density 30 J/cm<sup>2</sup>, pulse duration 50 µs, number of pulses 5, and pulse repetition rate 0.3 s<sup>–1</sup>) leads to the formation of a thin (30–50 µm) surface layer with a cellular crystallization structure. The volume of grains is formed by a solid solution based on α-Fe. Nanoscale (10–45 nm) particles of iron, chromium, and tungsten carbides of complex composition, such as M<sub>6</sub>C and M<sub>23</sub>C<sub>6</sub>, are located in the volume and along the boundaries of the crystallization cells. Fragmentation of the surface layer by a grid of microcracks is revealed, indicating relaxation of thermal stresses formed during high-speed cooling after electron beam processing. The particles have a faceted or globular shape. After irradiation with an electron beam, the wear resistance of the material increases by more than 3 times, while maintaining the microhardness of the modified layer (~5.3 GPa).</p>","PeriodicalId":671,"journal":{"name":"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques","volume":"18 2","pages":"361 - 371"},"PeriodicalIF":0.5000,"publicationDate":"2024-05-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Structure and Properties of High-Speed Steel Surfaised Layer Irradiated by Pulsed Electron Beam\",\"authors\":\"Yu. F. Ivanov, V. E. Gromov, T. P. Guseva, A. S. Chapaikin, E. S. Vashchuk, D. A. Romanov\",\"doi\":\"10.1134/S102745102402006X\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>The methods of light, scanning, and transmission electron microscopy are used to study the structure, phase composition, and properties of multilayer plasma surfacings made of high-speed steel R18YU in a protective-alloying nitrogen medium, followed by a fourfold high-temperature tempering and additional electron beam processing. After tempering, the deposited layer on the 30KHGSA high-speed steel R18YU has a polycrystalline structure with a cell size of 7–22.5 µm with layers of the second phase along the boundaries and at the joints of the grains. It is shown that the irradiation of surfaised layers with a pulsed electron beam (energy density 30 J/cm<sup>2</sup>, pulse duration 50 µs, number of pulses 5, and pulse repetition rate 0.3 s<sup>–1</sup>) leads to the formation of a thin (30–50 µm) surface layer with a cellular crystallization structure. The volume of grains is formed by a solid solution based on α-Fe. Nanoscale (10–45 nm) particles of iron, chromium, and tungsten carbides of complex composition, such as M<sub>6</sub>C and M<sub>23</sub>C<sub>6</sub>, are located in the volume and along the boundaries of the crystallization cells. Fragmentation of the surface layer by a grid of microcracks is revealed, indicating relaxation of thermal stresses formed during high-speed cooling after electron beam processing. The particles have a faceted or globular shape. After irradiation with an electron beam, the wear resistance of the material increases by more than 3 times, while maintaining the microhardness of the modified layer (~5.3 GPa).</p>\",\"PeriodicalId\":671,\"journal\":{\"name\":\"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques\",\"volume\":\"18 2\",\"pages\":\"361 - 371\"},\"PeriodicalIF\":0.5000,\"publicationDate\":\"2024-05-07\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.1134/S102745102402006X\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"PHYSICS, CONDENSED MATTER\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.1134/S102745102402006X","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"PHYSICS, CONDENSED MATTER","Score":null,"Total":0}
Structure and Properties of High-Speed Steel Surfaised Layer Irradiated by Pulsed Electron Beam
The methods of light, scanning, and transmission electron microscopy are used to study the structure, phase composition, and properties of multilayer plasma surfacings made of high-speed steel R18YU in a protective-alloying nitrogen medium, followed by a fourfold high-temperature tempering and additional electron beam processing. After tempering, the deposited layer on the 30KHGSA high-speed steel R18YU has a polycrystalline structure with a cell size of 7–22.5 µm with layers of the second phase along the boundaries and at the joints of the grains. It is shown that the irradiation of surfaised layers with a pulsed electron beam (energy density 30 J/cm2, pulse duration 50 µs, number of pulses 5, and pulse repetition rate 0.3 s–1) leads to the formation of a thin (30–50 µm) surface layer with a cellular crystallization structure. The volume of grains is formed by a solid solution based on α-Fe. Nanoscale (10–45 nm) particles of iron, chromium, and tungsten carbides of complex composition, such as M6C and M23C6, are located in the volume and along the boundaries of the crystallization cells. Fragmentation of the surface layer by a grid of microcracks is revealed, indicating relaxation of thermal stresses formed during high-speed cooling after electron beam processing. The particles have a faceted or globular shape. After irradiation with an electron beam, the wear resistance of the material increases by more than 3 times, while maintaining the microhardness of the modified layer (~5.3 GPa).
期刊介绍:
Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques publishes original articles on the topical problems of solid-state physics, materials science, experimental techniques, condensed media, nanostructures, surfaces of thin films, and phase boundaries: geometric and energetical structures of surfaces, the methods of computer simulations; physical and chemical properties and their changes upon radiation and other treatments; the methods of studies of films and surface layers of crystals (XRD, XPS, synchrotron radiation, neutron and electron diffraction, electron microscopic, scanning tunneling microscopic, atomic force microscopic studies, and other methods that provide data on the surfaces and thin films). Articles related to the methods and technics of structure studies are the focus of the journal. The journal accepts manuscripts of regular articles and reviews in English or Russian language from authors of all countries. All manuscripts are peer-reviewed.