波兰西里西亚圣维博津哥特式教堂的热释光研究

Q2 Engineering Optical Materials: X Pub Date : 2024-07-01 DOI:10.1016/j.omx.2024.100308
Andrzej Legendziewicz , Janina Legendziewicz
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引用次数: 0

摘要

本文介绍了热释光(TL)研究,旨在确定使用这种分析方法确定历史教堂的建造、改造和/或重建日期的可能性。使用建筑师和考古学家现在使用的绝对年代测定法来确定建筑结构的年代既困难又复杂。在考古研究中可以观察到相对较大的估计误差。就中世纪的样本而言,这种误差是不可接受的。作者试图为此类研究开发一种替代的 TL 光谱方法,并建议使用 X 射线衍射、电子显微镜(EM)和 TL 光谱来测量砖块的成分。用于测试的砖块取自教堂的内墙和阁楼墙壁,即建筑工程最后阶段建造的地方。TL 测量是在 25-500°C 的温度范围内使用 X 射线和 β 源激励进行的。研究了两种不同大小的颗粒:小颗粒(∼0.1 毫米)和大颗粒(∼0.5 毫米)。调查选择了位于圣十字维博津(Świebodzin)的一座哥特式教堂,该教堂建于 1555 年,其建造历史众所周知。由于该教堂比 [1] 中评估和描述的两座教堂年轻 326 年,其砖块的成分可能有所不同。因此,作者决定比较所有三座教堂砖块的 XRD 数据、EM 结果和 TL 光谱。确定了 TL 强度和综合 TL 强度。测量结果对于建立 TL 强度与建筑物体建造日期之间的关系非常重要。此外,通过测量结果还可以验证华沙萨斯基宫的建造日期。
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Thermoluminescence studies of a Gothic church in Świebodzin from Silesia in Poland

The paper presents thermoluminescence (TL) studies that aim to establish the possibility of using such analysis to determine the date of the construction, transformation and/or rebuilding of a historical church. The determination of the age of building structures using the form of absolute dating that is now used by architects and archeologists is difficult and complex. A relatively large error of estimation can be observed in archeological studies. In the case of samples from the Middle Ages, such errors are not acceptable. The authors attempted to develop an alternative spectroscopic TL method for such studies, and proposed that the composition of bricks should be measured using X-ray diffraction, electron microscopy (EM) and TL spectra. The bricks for the testing were taken from internal walls and the walls in the attics of churches, i.e. from places built during the last stage of construction works. The TL measurements were made using x-ray and β source excitation within the temperature range of 25–500°C. Two different sizes of grains were studied: small (∼0.1 mm) and large (∼0.5 mm). A gothic church in Świebodzin from 1555, which has a well-known history of its construction, was selected for the investigations. Due to the fact that this church is 326 years younger than the two churches evaluated and described in [1], the composition of its bricks could be different. Therefore, the authors decided to compare the XRD data, EM results and TL spectra for bricks taken from all three churches. The intensities of the TL and the integrated TL intensities were determined. The measurement results are important for creating a relationship between the TL intensity and the date a building object was constructed. Moreover, thanks to this it was possible to verify the construction date of Saski Palace in Warsaw.

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来源期刊
Optical Materials: X
Optical Materials: X Engineering-Electrical and Electronic Engineering
CiteScore
3.30
自引率
0.00%
发文量
73
审稿时长
91 days
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