揭示环保型纳米氧化锌的合成、特性、导电性、光催化活性和电化学活性

Redwanul Islam , Suprio Shantanu Saha , Reana Raen , Nayeemul Islam , Torikul Islam
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摘要

从观察到的白色沉淀可以看出,Nigella Sativa 种子被用于制造环保型氧化锌纳米粒子(ZnO NPs)。我们利用 XRD、FTIR、UV-vis、SEM 和 EDX 等多种分析技术来描述试样的结构、光学和电学特性。XRD 分析用于确认氧化锌纳米粒子是晶体。在紫外可见光谱中,在 401 纳米处观察到一个吸光峰,表明氧化锌氮氧化物具有 2.91 eV 的带隙。从傅立叶变换红外光谱图中可以看出,氧化锌纳米粒子中含有官能团。扫描电镜图像证实了纳米粒子呈球形,平均尺寸为 37.9 纳米。EDX 分析证实了纳米颗粒的成分,其中锌占 73.17%,氧占 26.83%。ZnO NPs 具有较高的表面体积比,因此具有出色的导电性。此外,合成的 ZnO NPs 还能有效降解亚甲基蓝染料。这些结果表明,ZnO NPs 在电子、生物医学设备、工业和农业等多个领域都有潜在的应用前景,需要立即开展后续研究。
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Unveiling the synthesis, characteristics, electrical conductivity, photocatalytic activity, and electrochemical activity of eco-friendly zinc oxide nanoparticles

The Nigella Sativa seeds were utilized for the environment-friendly zinc oxide nanoparticles (ZnO NPs), as evident by the observation of a white precipitate. Numerous analytical techniques, such as XRD, FTIR, UV–vis, SEM, and EDX, were utilized to describe the specimen's structural, optical, and electrical properties. XRD analysis was used to confirm that the ZnO NPs were crystalline. An absorbance peak at 401 nm was observed in the UV–vis, indicating that the ZnO NPs have a 2.91 eV bandgap. Functional groups are present in ZnO NPs, as seen by the FTIR graph. The nanoparticles' spherical form and average size of 37.9 nm were confirmed by the SEM image. EDX analysis confirmed the composition of the nanoparticles, with zinc accounting for 73.17% and oxygen for 26.83%. ZnO NPs demonstrated excellent electrical conductivity because of their higher surface-to-volume ratio. Additionally, the synthesis of ZnO NPs exhibited effective degradation of methylene blue dye. These results point to potential applications in several domains, including electronics, biomedical devices, industry, and agriculture, and they call for immediate follow-up research.

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