以 Al-B-C 作为烧结添加剂的浆料浸渍热压烧结碳化硅纳米纤维/碳化硅复合材料

IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS International Journal of Applied Ceramic Technology Pub Date : 2024-05-22 DOI:10.1111/ijac.14800
Jiyu Tao, Yongwei Lou, Jinxia Li, Hao Chen, Jianjun Chen
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引用次数: 0

摘要

以铝(Al)粉末、硼(B)粉末和炭黑为烧结助剂,通过浆料浸渍热压烧结法制备了具有层状堆积结构的碳化硅纳米纤维/碳化硅(SiCnf/SiC)复合材料。使用纳米纤维制造 SiCnf 纸,并用 SiCnp 浆料和烧结助剂进行浸渍,通过 SiCnf 纸和 SiCnp 的交替堆叠制造 SiCnf/SiC 预型件。通过化学气相沉积法和真空浸渍-热解法在 SiCnf 表面沉积了热解碳和氮化硼界面层。研究了不同烧结温度对复合材料相对密度、孔隙率、截面微观形貌和力学性能的影响。结果表明,SiCnf/SiC 复合材料的断裂韧性显著提高。在烧结温度为 1950°C 和烧结压力为 30 MPa 时,复合材料的力学性能达到最佳,弯曲强度和断裂韧性分别为 548 MPa 和 15.86 MPa-m1/2。高温下生成的液相 Al8B4C7 化合物促进了复合材料的致密化。
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Slurry-impregnating hot-press sintered silicon carbide nanofiber/silicon carbide composites with Al-B-C as sintering additives

Silicon carbide nanofiber/silicon carbide (SiCnf/SiC) composites with a laminar stacking structure were prepared by the slurry impregnation hot-press sintering using aluminum (Al) powder, boron (B) powder, and carbon black as sintering aids. SiCnf paper was fabricated using nanofibers and impregnated with the slurry of SiCnp and sintering aids, and the SiCnf/SiC preforms were fabricated by the alternating stack of the SiCnf paper and SiCnp. The pyrolysis carbon and boron nitride interface layers were deposited on the surface of SiCnf by chemical vapor deposition and vacuum impregnation-pyrolysis methods. The effects of different sintering temperatures on the relative density, porosity, sectional microscopic morphology, and mechanical properties of the composites were investigated. The results show that the fracture toughness of SiCnf/SiC composites is significantly improved. The mechanical properties of the composites were optimized at a sintering temperature of 1950°C and a sintering pressure of 30 MPa, with flexural strength and fracture toughness of 548 MPa and 15.86 MPa·m1/2, respectively. The liquid phase Al8B4C7 compound generated at the high temperature promoted the densification of the composites.

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来源期刊
International Journal of Applied Ceramic Technology
International Journal of Applied Ceramic Technology 工程技术-材料科学:硅酸盐
CiteScore
3.90
自引率
9.50%
发文量
280
审稿时长
4.5 months
期刊介绍: The International Journal of Applied Ceramic Technology publishes cutting edge applied research and development work focused on commercialization of engineered ceramics, products and processes. The publication also explores the barriers to commercialization, design and testing, environmental health issues, international standardization activities, databases, and cost models. Designed to get high quality information to end-users quickly, the peer process is led by an editorial board of experts from industry, government, and universities. Each issue focuses on a high-interest, high-impact topic plus includes a range of papers detailing applications of ceramics. Papers on all aspects of applied ceramics are welcome including those in the following areas: Nanotechnology applications; Ceramic Armor; Ceramic and Technology for Energy Applications (e.g., Fuel Cells, Batteries, Solar, Thermoelectric, and HT Superconductors); Ceramic Matrix Composites; Functional Materials; Thermal and Environmental Barrier Coatings; Bioceramic Applications; Green Manufacturing; Ceramic Processing; Glass Technology; Fiber optics; Ceramics in Environmental Applications; Ceramics in Electronic, Photonic and Magnetic Applications;
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