NiO-ZnO纳米复合材料的微结构、抗真菌和光催化活性

IF 1.3 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Science-Poland Pub Date : 2024-05-31 DOI:10.2478/msp-2024-0006
Yixuan Wang, G. Balakrishnan
{"title":"NiO-ZnO纳米复合材料的微结构、抗真菌和光催化活性","authors":"Yixuan Wang, G. Balakrishnan","doi":"10.2478/msp-2024-0006","DOIUrl":null,"url":null,"abstract":"In this work, NiO–ZnOnanocomposite (NC)was prepared through a facile, low-temperature,sol–gel route. Zinc acetate dihydrate, nickel chloride hexahydrate, cetyltrimethyl ammonium bromide (CTAB), and citric acid were used in the synthesis of the material. Then, the sample was kept in the muffle furnace at a temperature of 600°C for 2 h. X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, field emission scanning electron microscopy (FESEM), UV–Visible spectroscopy, and photocatalytic and antifungal investigations were used to characterize the synthesized nanocrystallites. The XRD data showedthe polycrystalline hexagonal ZnO nanoparticles and cubic NiO crystallites. FTIR studies confirmed the presence of Zn-O and Ni-O bonds in the sample. The FESEM analysis showed the morphology of nanocrystallitescharacterized by their homogeneous shape and size. The absorbance curves from the UV–Visible spectroscopy investigation revealed the bandgap of 3.17 eV. The research findings demonstrate that the NiO–ZnO NC possesses the significant level of selected microbial pathogens. Industrial dyesmake water unhealthy for drinking. Among these dyes, methylene blue (MB) is toxic, carcinogenic, and non-biodegradable, and causes a severe threat to human health and environmental safety. Hence, it is necessary to develop efficient and environmentally friendly technology to remove MB from wastewater. The ZnO–NiO NC degraded the MB dye pollutant under visible irradiation (125 W), according to photocatalytic tests. After 120 min of exposure, the photocatalytic investigations demonstrated 75% degradation efficiency.","PeriodicalId":18269,"journal":{"name":"Materials Science-Poland","volume":"37 1","pages":""},"PeriodicalIF":1.3000,"publicationDate":"2024-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microstructural, antifungal and photocatalytic activity of NiO–ZnO nanocomposite\",\"authors\":\"Yixuan Wang, G. Balakrishnan\",\"doi\":\"10.2478/msp-2024-0006\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this work, NiO–ZnOnanocomposite (NC)was prepared through a facile, low-temperature,sol–gel route. Zinc acetate dihydrate, nickel chloride hexahydrate, cetyltrimethyl ammonium bromide (CTAB), and citric acid were used in the synthesis of the material. Then, the sample was kept in the muffle furnace at a temperature of 600°C for 2 h. X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, field emission scanning electron microscopy (FESEM), UV–Visible spectroscopy, and photocatalytic and antifungal investigations were used to characterize the synthesized nanocrystallites. The XRD data showedthe polycrystalline hexagonal ZnO nanoparticles and cubic NiO crystallites. FTIR studies confirmed the presence of Zn-O and Ni-O bonds in the sample. The FESEM analysis showed the morphology of nanocrystallitescharacterized by their homogeneous shape and size. The absorbance curves from the UV–Visible spectroscopy investigation revealed the bandgap of 3.17 eV. The research findings demonstrate that the NiO–ZnO NC possesses the significant level of selected microbial pathogens. Industrial dyesmake water unhealthy for drinking. Among these dyes, methylene blue (MB) is toxic, carcinogenic, and non-biodegradable, and causes a severe threat to human health and environmental safety. Hence, it is necessary to develop efficient and environmentally friendly technology to remove MB from wastewater. The ZnO–NiO NC degraded the MB dye pollutant under visible irradiation (125 W), according to photocatalytic tests. After 120 min of exposure, the photocatalytic investigations demonstrated 75% degradation efficiency.\",\"PeriodicalId\":18269,\"journal\":{\"name\":\"Materials Science-Poland\",\"volume\":\"37 1\",\"pages\":\"\"},\"PeriodicalIF\":1.3000,\"publicationDate\":\"2024-05-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Science-Poland\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.2478/msp-2024-0006\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Science-Poland","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.2478/msp-2024-0006","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0

摘要

本研究通过一种简便的低温溶胶-凝胶路线制备了镍锌锰复合材料(NC)。合成过程中使用了二水醋酸锌、六水氯化镍、十六烷基三甲基溴化铵(CTAB)和柠檬酸。利用 X 射线衍射(XRD)、傅立叶变换红外光谱(FTIR)、场发射扫描电子显微镜(FESEM)、紫外-可见光谱、光催化和抗真菌研究对合成的纳米晶体进行了表征。XRD 数据显示了多晶六方氧化锌纳米颗粒和立方氧化镍晶体。傅立叶变换红外光谱研究证实了样品中存在 Zn-O 和 Ni-O 键。FESEM 分析表明了纳米晶体的形态,其形状和大小都很均匀。紫外-可见光谱研究的吸光曲线显示带隙为 3.17 eV。研究结果表明,NiO-ZnO NC 对所选微生物病原体具有显著的抑制作用。工业染料会使饮用水变得不健康。在这些染料中,亚甲基蓝(MB)具有毒性、致癌性和不可生物降解性,对人类健康和环境安全造成严重威胁。因此,有必要开发高效、环保的技术来去除废水中的甲基溴。根据光催化测试,ZnO-NiO NC 在可见光(125 W)照射下可降解甲基溴染料污染物。照射 120 分钟后,光催化研究表明降解效率为 75%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Microstructural, antifungal and photocatalytic activity of NiO–ZnO nanocomposite
In this work, NiO–ZnOnanocomposite (NC)was prepared through a facile, low-temperature,sol–gel route. Zinc acetate dihydrate, nickel chloride hexahydrate, cetyltrimethyl ammonium bromide (CTAB), and citric acid were used in the synthesis of the material. Then, the sample was kept in the muffle furnace at a temperature of 600°C for 2 h. X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, field emission scanning electron microscopy (FESEM), UV–Visible spectroscopy, and photocatalytic and antifungal investigations were used to characterize the synthesized nanocrystallites. The XRD data showedthe polycrystalline hexagonal ZnO nanoparticles and cubic NiO crystallites. FTIR studies confirmed the presence of Zn-O and Ni-O bonds in the sample. The FESEM analysis showed the morphology of nanocrystallitescharacterized by their homogeneous shape and size. The absorbance curves from the UV–Visible spectroscopy investigation revealed the bandgap of 3.17 eV. The research findings demonstrate that the NiO–ZnO NC possesses the significant level of selected microbial pathogens. Industrial dyesmake water unhealthy for drinking. Among these dyes, methylene blue (MB) is toxic, carcinogenic, and non-biodegradable, and causes a severe threat to human health and environmental safety. Hence, it is necessary to develop efficient and environmentally friendly technology to remove MB from wastewater. The ZnO–NiO NC degraded the MB dye pollutant under visible irradiation (125 W), according to photocatalytic tests. After 120 min of exposure, the photocatalytic investigations demonstrated 75% degradation efficiency.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Materials Science-Poland
Materials Science-Poland MATERIALS SCIENCE, MULTIDISCIPLINARY-
自引率
18.20%
发文量
18
期刊介绍: Material Sciences-Poland is an interdisciplinary journal devoted to experimental research into results on the relationships between structure, processing, properties, technology, and uses of materials. Original research articles and review can be only submitted.
期刊最新文献
Nanofibrous membranes loaded with bupivacaine and carica papaya extract for pain management and wound healing in postoperative wounds Dental pulp regeneration via dental pulp stem cells conditioned media and curcumin-loaded nanocomposite hydrogel: an in vitro and in vivo study The performance of CFRP-strengthened heat-damaged metakaolin-based geopolymer concrete cylinders containing reclaimed asphalt aggregate Non-isothermal melt- and cold-crystallization, melting process, and optical and mechanical properties of PLLA: the effect of TAPH A Review of Biomass-Derived Biochar and Its Potential in Asphalt Pavement Engineering
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1