利用 WDS 和 EDS 对锡-铋-锑焊料中的锑分布进行对比分析

IF 2.7 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Letters Pub Date : 2024-06-26 DOI:10.1016/j.matlet.2024.136922
Fusheng Li , Zhigang Wang , Xixue Liu , Lei Xu , Fuwen Zhang , Huijun He
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引用次数: 0

摘要

这项研究通过 WDS 制图、EDS 计数图和 EDS 净图对 Sn-57Bi-1Sb 焊料中的锑分布进行了对比分析。对同一区域的图谱分析表明,与 EDS 分析相比,WDS 图谱能提供更准确的锑分布数据,包括溶解锑的浓度梯度和尺寸小于 1 μm 的细小锑颗粒。WDS 具有更高的光谱分辨率,是分离复杂重叠光谱的关键技术,建议用于掺锑焊料中锑的检测。
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A contrastive analysis of Sb distribution in Sn-Bi-Sb solder by WDS and EDS

This work provides a contrastive analysis of Sb distribution in Sn-57Bi-1Sb solder by WDS mapping, EDS count map and EDS net map. The mapping analysis on the same region shows that the WDS mapping provides the more accurate data on the distribution of Sb compared with EDS analysis, including the concentration gradient of dissolved Sb and the fine SnSb particles with size less than 1 μm. WDS equipped with the enhanced spectral resolution is a critical technique to separate the complex overlap spectrum, which was recommended for the Sb detection in Sb-doped solders.

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来源期刊
Materials Letters
Materials Letters 工程技术-材料科学:综合
CiteScore
5.60
自引率
3.30%
发文量
1948
审稿时长
50 days
期刊介绍: Materials Letters has an open access mirror journal Materials Letters: X, sharing the same aims and scope, editorial team, submission system and rigorous peer review. Materials Letters is dedicated to publishing novel, cutting edge reports of broad interest to the materials community. The journal provides a forum for materials scientists and engineers, physicists, and chemists to rapidly communicate on the most important topics in the field of materials. Contributions include, but are not limited to, a variety of topics such as: • Materials - Metals and alloys, amorphous solids, ceramics, composites, polymers, semiconductors • Applications - Structural, opto-electronic, magnetic, medical, MEMS, sensors, smart • Characterization - Analytical, microscopy, scanning probes, nanoscopic, optical, electrical, magnetic, acoustic, spectroscopic, diffraction • Novel Materials - Micro and nanostructures (nanowires, nanotubes, nanoparticles), nanocomposites, thin films, superlattices, quantum dots. • Processing - Crystal growth, thin film processing, sol-gel processing, mechanical processing, assembly, nanocrystalline processing. • Properties - Mechanical, magnetic, optical, electrical, ferroelectric, thermal, interfacial, transport, thermodynamic • Synthesis - Quenching, solid state, solidification, solution synthesis, vapor deposition, high pressure, explosive
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