优化卡达巴香蕉淀粉的消化淀粉和淀粉消化指数揭示了多相淀粉消化图谱

Starch Pub Date : 2024-06-20 DOI:10.1002/star.202300274
Babatunde Olawoye, Oladapo Fisoye Fagbohun, Oyekemi Popoola‐Akinola, Oseni Kadiri, Olumide Samson Fawale, Florence Abolaji Bello, Charles Taiwo Akanbi
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引用次数: 0

摘要

使用辛烯基琥珀酸酐(OSA)对卡帕巴香蕉中的淀粉进行改性,使用响应面方法和偏最小二乘法回归分析对改性过程进行建模,目的是优化淀粉改性过程,以生产低消化率淀粉。对改性淀粉进行消化淀粉(DS)和淀粉消化率指数(SDI)分析。此外,还采用多相法研究了优化淀粉和原生淀粉的淀粉消化图。建模结果表明,响应面法(RSM)和偏最小二乘法回归(PLS-R)模型都能准确预测因变量(r2[决定系数] >0.9)。根据统计指数,RSM 模型比 PLS-R 模型的预测结果更好。生产低淀粉消化率变性淀粉的优化条件是 OSA 浓度为 3.98%、反应时间为 47.45 分钟、pH 值为 10,预测 DS 值为 45.99%,SDI 值为 29.86%。对优化后的淀粉消化图和原生淀粉消化图进行建模后发现,消化图遵循多相消化图,消化过程分为三(3)段。淀粉的消化率遵循快速-慢速和慢速-快速的体外淀粉消化率。
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Optimizing the Digested Starch and Starch Digestibility Index of Cardaba Banana Starch Revealed a Multiphasic Starch Digestogram
Starch from cardaba banana is modified using octenyl succinic anhydride (OSA), the modification process is modeled using response surface methodology and partial least square regression analysis with the aim of optimizing the starch modification process to produce low digestibility starch. The modified starch is analyzed for digested starch (DS) as well as the starch digestibility index (SDI). The starch digestogram of the optimized starch, as well as the native, is also investigated using a multiphasic approach. The modeling revealed that both the response surface methodology (RSM) and partial least square regression (PLS‐R) model predict with high accuracy (r2 [coefficient of determinant] > 0.9) the dependent variables. According to the statistical indices, the RSM model makes a better prediction when compared to the PLS‐R model. The optimized conditions for the production of modified starch with low starch digestibility are an OSA concentration of 3.98%, reaction time of 47.45 min, and pH of 10 with a predicted DS of 45.99% and SDI value of 29.86%. Modeling the optimized and native starch digestogram reveals the digestogram follows a multiphasic digestogram with the digestion occurring in three (3) segments. The digestion rate of the starch follows a rapid‐slow and slow‐rapid in vitro starch digestion rate.
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