Ariful Islam , Bashir Ahamed , Abu Saifullah , Anamul Hoque Bhuiyan , Emdadul Haq , Abu Sayeed , Hom N. Dhakal , Forkan Sarker
{"title":"基于短黄麻纤维预成型的环氧树脂复合材料在低速冲击载荷下的响应","authors":"Ariful Islam , Bashir Ahamed , Abu Saifullah , Anamul Hoque Bhuiyan , Emdadul Haq , Abu Sayeed , Hom N. Dhakal , Forkan Sarker","doi":"10.1016/j.jcomc.2024.100488","DOIUrl":null,"url":null,"abstract":"<div><p>This work aimed to investigate the low velocity impact behaviour of short jute fibre non-woven preform epoxy matrix composites experimentally. Dry fibre preforms were developed using an optimised process and a laboratory made preforming device. The effects of alkali and poly vinyl alcohol (PVA binder) treatments on impact performances of jute composites were investigated and compared at 3 J and 6 J impact energy levels. To identify the failure modes of tested composites, the X-ray µCT tomography was employed. The results demonstrated that the developed untreated short jute fibre preform reinforced composites absorbed a higher impact energy, when they were compared to treated (alkali or PVA binder) composites. For untreated composites, maximum impact forces at 3 J and 6 J energies, were found as ⁓2478 N and ⁓2319 N, respectively; for the PVA treatment these values were measured as ⁓2457 N and ⁓2216 N, while, at same energy levels, alkali treated composites showed the lowest values as ⁓1683 N and ⁓1440 N, respectively. Untreated jute fibre contains natural matrices such as hemicellulose, lignin and waxes, which ensured a positive response to absorb more energy upon impact loading. In contrast, the alkali treatment facilitates a highly fibre packed composite structure, which accelerated the impact crack propagation in tested composites, resulting in lower resistance to impact energy. Although, PVA treated composites showed reduced impact properties compared to untreated composites due to the PVA polymer brittleness on the treated fibre surface during the impact incidents, this treatment demonstrated better impact responses over the alkali treatment. The application of PVA binder on alkali-treated fibres provided an extra support to fibres and a better fibre/matrix interface and hence, this combined treatment demonstrated a slightly better impact resistance (⁓2027 N and ⁓1874 N impact forces at 3 J and 6 J respectively) compared to only alkali treated fibre composites. The SEM fracture images and the X-ray µCT damage analysis revealed different impact damage modes, which supported the observed impact results. The obtained results from this investigation could be helpful for using short jute fibre composites in various load demanding applications where impact incidents are likely to be happened.</p></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":null,"pages":null},"PeriodicalIF":5.3000,"publicationDate":"2024-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S2666682024000574/pdfft?md5=1226e3868f8786c6043ea89c4f9b11ca&pid=1-s2.0-S2666682024000574-main.pdf","citationCount":"0","resultStr":"{\"title\":\"Response of short jute fibre preform based epoxy composites subjected to low-velocity impact loadings\",\"authors\":\"Ariful Islam , Bashir Ahamed , Abu Saifullah , Anamul Hoque Bhuiyan , Emdadul Haq , Abu Sayeed , Hom N. Dhakal , Forkan Sarker\",\"doi\":\"10.1016/j.jcomc.2024.100488\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>This work aimed to investigate the low velocity impact behaviour of short jute fibre non-woven preform epoxy matrix composites experimentally. Dry fibre preforms were developed using an optimised process and a laboratory made preforming device. The effects of alkali and poly vinyl alcohol (PVA binder) treatments on impact performances of jute composites were investigated and compared at 3 J and 6 J impact energy levels. To identify the failure modes of tested composites, the X-ray µCT tomography was employed. The results demonstrated that the developed untreated short jute fibre preform reinforced composites absorbed a higher impact energy, when they were compared to treated (alkali or PVA binder) composites. For untreated composites, maximum impact forces at 3 J and 6 J energies, were found as ⁓2478 N and ⁓2319 N, respectively; for the PVA treatment these values were measured as ⁓2457 N and ⁓2216 N, while, at same energy levels, alkali treated composites showed the lowest values as ⁓1683 N and ⁓1440 N, respectively. Untreated jute fibre contains natural matrices such as hemicellulose, lignin and waxes, which ensured a positive response to absorb more energy upon impact loading. In contrast, the alkali treatment facilitates a highly fibre packed composite structure, which accelerated the impact crack propagation in tested composites, resulting in lower resistance to impact energy. Although, PVA treated composites showed reduced impact properties compared to untreated composites due to the PVA polymer brittleness on the treated fibre surface during the impact incidents, this treatment demonstrated better impact responses over the alkali treatment. The application of PVA binder on alkali-treated fibres provided an extra support to fibres and a better fibre/matrix interface and hence, this combined treatment demonstrated a slightly better impact resistance (⁓2027 N and ⁓1874 N impact forces at 3 J and 6 J respectively) compared to only alkali treated fibre composites. The SEM fracture images and the X-ray µCT damage analysis revealed different impact damage modes, which supported the observed impact results. The obtained results from this investigation could be helpful for using short jute fibre composites in various load demanding applications where impact incidents are likely to be happened.</p></div>\",\"PeriodicalId\":34525,\"journal\":{\"name\":\"Composites Part C Open Access\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":5.3000,\"publicationDate\":\"2024-07-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.sciencedirect.com/science/article/pii/S2666682024000574/pdfft?md5=1226e3868f8786c6043ea89c4f9b11ca&pid=1-s2.0-S2666682024000574-main.pdf\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Composites Part C Open Access\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2666682024000574\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, COMPOSITES\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Composites Part C Open Access","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2666682024000574","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, COMPOSITES","Score":null,"Total":0}
引用次数: 0
摘要
这项工作旨在通过实验研究短黄麻纤维无纺预制环氧基复合材料的低速冲击行为。采用优化的工艺和实验室自制的预成型装置开发了干纤维预成型件。在 3 J 和 6 J 的冲击能量水平下,研究并比较了碱和聚乙烯醇(PVA 粘合剂)处理对黄麻复合材料冲击性能的影响。为了确定测试复合材料的失效模式,采用了 X 射线 µCT 层析成像技术。结果表明,与经过处理(碱或 PVA 粘合剂)的复合材料相比,未经处理的短黄麻纤维预成型增强复合材料吸收的冲击能量更高。对于未经处理的复合材料,在 3 J 和 6 J 能量下的最大冲击力分别为⁓2478 N 和 ⁓2319 N;对于经过 PVA 处理的复合材料,这些值分别为⁓2457 N 和 ⁓2216 N,而在相同的能量水平下,经过碱处理的复合材料的最低值分别为⁓1683 N 和 ⁓1440 N。未经处理的黄麻纤维含有半纤维素、木质素和蜡质等天然基质,这些基质确保了黄麻纤维在受到冲击载荷时吸收更多能量的积极反应。与此相反,碱处理有利于形成高度纤维密集的复合材料结构,从而加速了测试复合材料中冲击裂纹的扩展,降低了抗冲击能量的能力。虽然与未处理的复合材料相比,经过 PVA 处理的复合材料的冲击性能有所降低,这是因为在冲击事件中,经过处理的纤维表面上的 PVA 聚合物会变脆,但与碱处理相比,这种处理方法显示出更好的冲击响应。碱处理纤维上的 PVA 粘合剂为纤维提供了额外的支撑,纤维/基质界面更好,因此,与只经过碱处理的纤维复合材料相比,这种组合处理的耐冲击性略有提高(在 3 J 和 6 J 下的冲击力分别为 2027 N 和 1874 N)。扫描电子显微镜断裂图像和 X 射线 µCT 损伤分析显示了不同的冲击损伤模式,这与观察到的冲击结果相吻合。这项研究获得的结果有助于将短黄麻纤维复合材料用于可能发生撞击事故的各种高负载应用中。
Response of short jute fibre preform based epoxy composites subjected to low-velocity impact loadings
This work aimed to investigate the low velocity impact behaviour of short jute fibre non-woven preform epoxy matrix composites experimentally. Dry fibre preforms were developed using an optimised process and a laboratory made preforming device. The effects of alkali and poly vinyl alcohol (PVA binder) treatments on impact performances of jute composites were investigated and compared at 3 J and 6 J impact energy levels. To identify the failure modes of tested composites, the X-ray µCT tomography was employed. The results demonstrated that the developed untreated short jute fibre preform reinforced composites absorbed a higher impact energy, when they were compared to treated (alkali or PVA binder) composites. For untreated composites, maximum impact forces at 3 J and 6 J energies, were found as ⁓2478 N and ⁓2319 N, respectively; for the PVA treatment these values were measured as ⁓2457 N and ⁓2216 N, while, at same energy levels, alkali treated composites showed the lowest values as ⁓1683 N and ⁓1440 N, respectively. Untreated jute fibre contains natural matrices such as hemicellulose, lignin and waxes, which ensured a positive response to absorb more energy upon impact loading. In contrast, the alkali treatment facilitates a highly fibre packed composite structure, which accelerated the impact crack propagation in tested composites, resulting in lower resistance to impact energy. Although, PVA treated composites showed reduced impact properties compared to untreated composites due to the PVA polymer brittleness on the treated fibre surface during the impact incidents, this treatment demonstrated better impact responses over the alkali treatment. The application of PVA binder on alkali-treated fibres provided an extra support to fibres and a better fibre/matrix interface and hence, this combined treatment demonstrated a slightly better impact resistance (⁓2027 N and ⁓1874 N impact forces at 3 J and 6 J respectively) compared to only alkali treated fibre composites. The SEM fracture images and the X-ray µCT damage analysis revealed different impact damage modes, which supported the observed impact results. The obtained results from this investigation could be helpful for using short jute fibre composites in various load demanding applications where impact incidents are likely to be happened.