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Experimental study on a new generation of recycled composite laminates
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-02-13 DOI: 10.1016/j.jcomc.2025.100571
P. Bettini , L. Calervo , R. Palazzetti
Composite manufacturing processes generate a significant amount of waste due to the raw material being supplied in sheet form and cut-outs. The unused scraps of prepreg are typically discarded, leading to the disposal of up to 35 % of the purchased material, accompanied by economic losses and negative environmental impacts. The authors propose collecting these scraps, cutting them into smaller, regular patches, and assembling them into a new, patched prepreg sheet. This study presents an experimental investigation into the mechanical properties of such patched material, assembled using two different architectures and three patch geometries. Five different configurations are designed, manufactured, and tested, with results compared to samples made from the original unpatched material through four-point bending tests. When patches are assembled in a regular geometry, the new material possesses around 50 % and 90 % of the original strength and stiffness, respectively, demonstrating potential for use in load-bearing applications. The methods of assembling the patches following a regular pattern also resulted in significantly better properties than a random deposition, which despite its lower cost to implement does not retain relevant mechanical characteristics. Of the two arranged investigated architectures, the one being more complex to manufacture shows 9 % and 5 % higher stiffness and strength, respectively, than the simpler one. Fracture analysis shows that failure mainly takes place in between of a patch, rather than the superposition areas.
{"title":"Experimental study on a new generation of recycled composite laminates","authors":"P. Bettini ,&nbsp;L. Calervo ,&nbsp;R. Palazzetti","doi":"10.1016/j.jcomc.2025.100571","DOIUrl":"10.1016/j.jcomc.2025.100571","url":null,"abstract":"<div><div>Composite manufacturing processes generate a significant amount of waste due to the raw material being supplied in sheet form and cut-outs. The unused scraps of prepreg are typically discarded, leading to the disposal of up to 35 % of the purchased material, accompanied by economic losses and negative environmental impacts. The authors propose collecting these scraps, cutting them into smaller, regular patches, and assembling them into a new, patched prepreg sheet. This study presents an experimental investigation into the mechanical properties of such patched material, assembled using two different architectures and three patch geometries. Five different configurations are designed, manufactured, and tested, with results compared to samples made from the original unpatched material through four-point bending tests. When patches are assembled in a regular geometry, the new material possesses around 50 % and 90 % of the original strength and stiffness, respectively, demonstrating potential for use in load-bearing applications. The methods of assembling the patches following a regular pattern also resulted in significantly better properties than a random deposition, which despite its lower cost to implement does not retain relevant mechanical characteristics. Of the two arranged investigated architectures, the one being more complex to manufacture shows 9 % and 5 % higher stiffness and strength, respectively, than the simpler one. Fracture analysis shows that failure mainly takes place in between of a patch, rather than the superposition areas.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100571"},"PeriodicalIF":5.3,"publicationDate":"2025-02-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143422623","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of fiber orientation on the strength of thermoplastic composite tubes subject to four-point bending 纤维取向对四点弯曲热塑性复合管强度的影响
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-02-10 DOI: 10.1016/j.jcomc.2025.100569
Mohammadali Rastak , Suong Van Hoa
This paper presents a study on the effect of fiber orientation on the strength of thermoplastic composite tubes made by automated fiber placement. The tubes are subjected to four-point bending deformation, representing the loading conditions in helicopter landing gears. The methodology for the study consists of the development of a finite element model for two particular tubes that yields results matching those from experiments. Maximum stress criterion is used for the determination of failure. The finite element model is then used to study the stress distribution and final failure and elongation of tubes with different layers with different fiber orientations. The lay-up sequence that can provide maximum failure load is then determined.
{"title":"Effect of fiber orientation on the strength of thermoplastic composite tubes subject to four-point bending","authors":"Mohammadali Rastak ,&nbsp;Suong Van Hoa","doi":"10.1016/j.jcomc.2025.100569","DOIUrl":"10.1016/j.jcomc.2025.100569","url":null,"abstract":"<div><div>This paper presents a study on the effect of fiber orientation on the strength of thermoplastic composite tubes made by automated fiber placement. The tubes are subjected to four-point bending deformation, representing the loading conditions in helicopter landing gears. The methodology for the study consists of the development of a finite element model for two particular tubes that yields results matching those from experiments. Maximum stress criterion is used for the determination of failure. The finite element model is then used to study the stress distribution and final failure and elongation of tubes with different layers with different fiber orientations. The lay-up sequence that can provide maximum failure load is then determined.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100569"},"PeriodicalIF":5.3,"publicationDate":"2025-02-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143422622","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Post-joining thermal characteristics and repair integrity of carbon fiber-reinforced thermoplastic composites during ultrasonic reconsolidation at 20 kHz
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-01-30 DOI: 10.1016/j.jcomc.2025.100565
Balaji Ragupathi , Lena Burger , Frank Balle
Ultrasonic reconsolidation offers significant potential to replace traditional adhesive bonding techniques used in the aerospace industries for bonding repair patches to damaged composite structures without resin additives. Temperature, a characteristic variable, is a key factor influencing the quality of joints in ultrasonic welding of thermoplastic composites. In this study, instead of measuring temperature during the joining process, the focus was on post-joining analysis on temperature at various hold times and holding forces. The findings revealed that an average hold time of 5 s and a holding force of 750 N produced higher-quality joints with minimal damages to fiber bundles and residual matrix. Additionally, it was recommended that repair patches should only undergo a maximum of two reconsolidation cycles. Beyond this point, the fibers and matrix begins to degrade, leading to a 35% reduction in mechanical performance after the fourth cycle.
{"title":"Post-joining thermal characteristics and repair integrity of carbon fiber-reinforced thermoplastic composites during ultrasonic reconsolidation at 20 kHz","authors":"Balaji Ragupathi ,&nbsp;Lena Burger ,&nbsp;Frank Balle","doi":"10.1016/j.jcomc.2025.100565","DOIUrl":"10.1016/j.jcomc.2025.100565","url":null,"abstract":"<div><div>Ultrasonic reconsolidation offers significant potential to replace traditional adhesive bonding techniques used in the aerospace industries for bonding repair patches to damaged composite structures without resin additives. Temperature, a characteristic variable, is a key factor influencing the quality of joints in ultrasonic welding of thermoplastic composites. In this study, instead of measuring temperature during the joining process, the focus was on post-joining analysis on temperature at various hold times and holding forces. The findings revealed that an average hold time of 5 s and a holding force of 750 N produced higher-quality joints with minimal damages to fiber bundles and residual matrix. Additionally, it was recommended that repair patches should only undergo a maximum of two reconsolidation cycles. Beyond this point, the fibers and matrix begins to degrade, leading to a 35% reduction in mechanical performance after the fourth cycle.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100565"},"PeriodicalIF":5.3,"publicationDate":"2025-01-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143101274","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Monotonic and cyclic compressive performance of self-monitoring MWCNT/PA12 cellular composites manufactured by selective laser sintering
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-01-29 DOI: 10.1016/j.jcomc.2025.100566
Muhammad Umar Azam , S Kumar , Andreas Schiffer
Herein, we experimentally investigate the mechanical and piezoresistive properties of selectively laser-sintered cellular composites under monotonic and cyclic compressive loading. Hexagonal honeycomb structures (HHSs) with relative densities of 20 %, 30 %, and 40 % were 3D printed from a ball-milled nanocomposite powder of multi-walled carbon nanotubes (MWCNTs) and polyamide 12 (PA12) with 0.3 wt.% MWCNTs. The pure PA12 HHSs exhibited lower porosity and superior mechanical properties, including collapse strength, elastic modulus and energy absorption, particularly at higher relative densities (30 % and 40 %). Notably, the specific energy absorption for the PA12 HHSs reached 24 J g⁻¹, under out-of-plane compression at 40 % relative density. Compared to neat PA12, the MWCNT/PA12 HHSs showed a reduction in strength and modulus but demonstrated excellent energy absorption efficiency of up to 53 %. Moreover, MWCNT/PA12 HHSs exhibited exceptional strain-sensing capabilities in the elastic region with gauge factors of up to 25. Cyclic tests showed that the zero-load resistance increased significantly as damage progressed during the collapse phase, highlighting their potential for application in smart, lightweight structures with integrated strain and damage-sensing functionalities.
{"title":"Monotonic and cyclic compressive performance of self-monitoring MWCNT/PA12 cellular composites manufactured by selective laser sintering","authors":"Muhammad Umar Azam ,&nbsp;S Kumar ,&nbsp;Andreas Schiffer","doi":"10.1016/j.jcomc.2025.100566","DOIUrl":"10.1016/j.jcomc.2025.100566","url":null,"abstract":"<div><div>Herein, we experimentally investigate the mechanical and piezoresistive properties of selectively laser-sintered cellular composites under monotonic and cyclic compressive loading. Hexagonal honeycomb structures (HHSs) with relative densities of 20 %, 30 %, and 40 % were 3D printed from a ball-milled nanocomposite powder of multi-walled carbon nanotubes (MWCNTs) and polyamide 12 (PA12) with 0.3 wt.% MWCNTs. The pure PA12 HHSs exhibited lower porosity and superior mechanical properties, including collapse strength, elastic modulus and energy absorption, particularly at higher relative densities (30 % and 40 %). Notably, the specific energy absorption for the PA12 HHSs reached 24 J g⁻¹, under out-of-plane compression at 40 % relative density. Compared to neat PA12, the MWCNT/PA12 HHSs showed a reduction in strength and modulus but demonstrated excellent energy absorption efficiency of up to 53 %. Moreover, MWCNT/PA12 HHSs exhibited exceptional strain-sensing capabilities in the elastic region with gauge factors of up to 25. Cyclic tests showed that the zero-load resistance increased significantly as damage progressed during the collapse phase, highlighting their potential for application in smart, lightweight structures with integrated strain and damage-sensing functionalities.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100566"},"PeriodicalIF":5.3,"publicationDate":"2025-01-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143101276","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Basalt-silk fiber reinforced PLA composites: Effect of graphene fillers and stacking sequence
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-01-27 DOI: 10.1016/j.jcomc.2025.100564
Hasibur R. Hamim , Tanzim Hasan , Farhan Shahriar , Sazidur Rahman Chowdhury , Md.Anisur Rahman , Mohammad Nasim , Mohammad Ahsan Habib
This study explores the development of biocompatible composites using strong basalt fibers and ductile silk fibers, and a polylactic acid (PLA) matrix. Five distinct stacking sequences were fabricated via a replicable hand layup and vacuum bagging technique, with alternating layer specimens (ALT) further enhanced by the addition of graphene nanoplatelets (GNPs) at 3, 6, and 9 wt.% of the PLA matrix. The composites were characterized for tensile, flexural, impact, and interlaminar shear strengths, damping properties, electrical conductivity, moisture absorption, and morphological features. The ALT configuration exhibited superior performance, with its multi-layered structure effectively mitigating delamination. ALT composites without GNPs achieved the highest tensile strength (136.54 MPa), tensile modulus (3.42 GPa), interlaminar shear strength (0.48 MPa), impact energy (36.84 kJ/m²), and flexural strength (18.06 MPa), predominantly failing via delamination. SEM analysis identified the basalt fiber-PLA interface as a critical failure site. The incorporation of 6 wt.% GNP enhanced damping by 1.54 times, but the composites remained nonconductive due to graphene agglomeration and lack of a conductive network. These energy-absorbing, environmentally sustainable composites show promise for multifaceted applications with reduced ecological impact.
{"title":"Basalt-silk fiber reinforced PLA composites: Effect of graphene fillers and stacking sequence","authors":"Hasibur R. Hamim ,&nbsp;Tanzim Hasan ,&nbsp;Farhan Shahriar ,&nbsp;Sazidur Rahman Chowdhury ,&nbsp;Md.Anisur Rahman ,&nbsp;Mohammad Nasim ,&nbsp;Mohammad Ahsan Habib","doi":"10.1016/j.jcomc.2025.100564","DOIUrl":"10.1016/j.jcomc.2025.100564","url":null,"abstract":"<div><div>This study explores the development of biocompatible composites using strong basalt fibers and ductile silk fibers, and a polylactic acid (PLA) matrix. Five distinct stacking sequences were fabricated via a replicable hand layup and vacuum bagging technique, with alternating layer specimens (ALT) further enhanced by the addition of graphene nanoplatelets (GNPs) at 3, 6, and 9 wt.% of the PLA matrix. The composites were characterized for tensile, flexural, impact, and interlaminar shear strengths, damping properties, electrical conductivity, moisture absorption, and morphological features. The ALT configuration exhibited superior performance, with its multi-layered structure effectively mitigating delamination. ALT composites without GNPs achieved the highest tensile strength (136.54 MPa), tensile modulus (3.42 GPa), interlaminar shear strength (0.48 MPa), impact energy (36.84 kJ/m²), and flexural strength (18.06 MPa), predominantly failing via delamination. SEM analysis identified the basalt fiber-PLA interface as a critical failure site. The incorporation of 6 wt.% GNP enhanced damping by 1.54 times, but the composites remained nonconductive due to graphene agglomeration and lack of a conductive network. These energy-absorbing, environmentally sustainable composites show promise for multifaceted applications with reduced ecological impact.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100564"},"PeriodicalIF":5.3,"publicationDate":"2025-01-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143101212","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Fabrication and characterization of the flexible three-layered thin film composites based on MXene/Fe3O4/MWCNT for electromagnetic shielding applications
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-01-22 DOI: 10.1016/j.jcomc.2025.100562
Mariam Mansoori, Shaohong Luo, Daniel Choi
Our research demonstrates the practical implementation of using multilayer (three layers) composites for electromagnetic interference (EMI) shielding. Three layers are: (1) The composites of multi-walled carbon nanotubes (MWCNT)/ carboxymethylcellulose (CMC) as the bottom layer; (2) The composites of MWCNT/CMC/iron oxide (Fe3O4) particles as the middle layer; (3) The composites of MXene/MWCNT/CMC/Fe3O4 as the top layer. Composition of each layer was optimized in order to maximize the electromagnetic properties of each layer. Each composite layer has outstanding electrical conductivity and excellent EMI shielding performance. The multilayer exhibits an EMI SET of 48 dB, SEA of more than 33 dB, and low SER of 15 dB in the X-band frequencies range, significantly enhanced compared to the single-layered materials for EMI applications.
{"title":"Fabrication and characterization of the flexible three-layered thin film composites based on MXene/Fe3O4/MWCNT for electromagnetic shielding applications","authors":"Mariam Mansoori,&nbsp;Shaohong Luo,&nbsp;Daniel Choi","doi":"10.1016/j.jcomc.2025.100562","DOIUrl":"10.1016/j.jcomc.2025.100562","url":null,"abstract":"<div><div>Our research demonstrates the practical implementation of using multilayer (three layers) composites for electromagnetic interference (EMI) shielding. Three layers are: (1) The composites of multi-walled carbon nanotubes (MWCNT)/ carboxymethylcellulose (CMC) as the bottom layer; (2) The composites of MWCNT/CMC/iron oxide (Fe<sub>3</sub>O<sub>4</sub>) particles as the middle layer; (3) The composites of MXene/MWCNT/CMC/Fe<sub>3</sub>O<sub>4</sub> as the top layer. Composition of each layer was optimized in order to maximize the electromagnetic properties of each layer. Each composite layer has outstanding electrical conductivity and excellent EMI shielding performance. The multilayer exhibits an EMI SE<sub>T</sub> of 48 dB, SE<sub>A</sub> of more than 33 dB, and low SE<sub>R</sub> of 15 dB in the X-band frequencies range, significantly enhanced compared to the single-layered materials for EMI applications.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100562"},"PeriodicalIF":5.3,"publicationDate":"2025-01-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143101275","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Flexural characteristics of additively manufactured continuous fiber-reinforced honeycomb sandwich structures
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-01-21 DOI: 10.1016/j.jcomc.2025.100563
Rafael Guerra Silva , Gustavo Morales Pavez
Additive manufacturing of continuous fiber filament is an advanced process that combines continuous strands of reinforcing fibers with thermoplastic materials to create composite parts. Previous studies have explored the potential of this technology to produce solid composite materials, but its potential for the production of sandwich panels has been limited. For instance, continuous fiber can be used to reinforce the faces while lightweight customized lattice structures could be selected for the core, all built integrally in one single process. This study analyzes the effect of reinforcement material and fiber orientation on the flexural behavior of continuous fiber-reinforced sandwich structures built entirely using a commercially available fused filament fabrication printer. Three-point bending tests were carried out on sandwich panel specimens, which were built using nylon reinforced with chopped carbon fiber and two reinforcement fibers, glass or carbon fiber. The carbon fiber-reinforced sandwich panels had a higher rigidity than those reinforced with glass fiber, but carbon fiber showed significant scattering. Additionally, we explored the influence of fiber content on the flexural behavior of the composite sandwich panels. As predicted by the theoretical models, a higher fiber content led to higher values of flexural modulus and strength. The analytical models were able to predict the flexural modulus and critical load with a relative error of approximately 20 % for low fiber volume fraction in the facing. On the other hand, in carbon fiber-reinforced specimens, when doubling the fiber volume fraction in the facing, the relative error was above 60 %.
{"title":"Flexural characteristics of additively manufactured continuous fiber-reinforced honeycomb sandwich structures","authors":"Rafael Guerra Silva ,&nbsp;Gustavo Morales Pavez","doi":"10.1016/j.jcomc.2025.100563","DOIUrl":"10.1016/j.jcomc.2025.100563","url":null,"abstract":"<div><div>Additive manufacturing of continuous fiber filament is an advanced process that combines continuous strands of reinforcing fibers with thermoplastic materials to create composite parts. Previous studies have explored the potential of this technology to produce solid composite materials, but its potential for the production of sandwich panels has been limited. For instance, continuous fiber can be used to reinforce the faces while lightweight customized lattice structures could be selected for the core, all built integrally in one single process. This study analyzes the effect of reinforcement material and fiber orientation on the flexural behavior of continuous fiber-reinforced sandwich structures built entirely using a commercially available fused filament fabrication printer. Three-point bending tests were carried out on sandwich panel specimens, which were built using nylon reinforced with chopped carbon fiber and two reinforcement fibers, glass or carbon fiber. The carbon fiber-reinforced sandwich panels had a higher rigidity than those reinforced with glass fiber, but carbon fiber showed significant scattering. Additionally, we explored the influence of fiber content on the flexural behavior of the composite sandwich panels. As predicted by the theoretical models, a higher fiber content led to higher values of flexural modulus and strength. The analytical models were able to predict the flexural modulus and critical load with a relative error of approximately 20 % for low fiber volume fraction in the facing. On the other hand, in carbon fiber-reinforced specimens, when doubling the fiber volume fraction in the facing, the relative error was above 60 %.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100563"},"PeriodicalIF":5.3,"publicationDate":"2025-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143101260","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
On the thickness and layup dependence on failure mechanisms during unfolding of curved woven composites
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-01-21 DOI: 10.1016/j.jcomc.2025.100559
R.D.R. Sitohang, S. Benou, L.L. Warnet, R. Akkerman
This study investigates the failure mechanisms of curved woven Glass/Polyphenylene sulfide (G/PPS) composites and characterizes the critical strains associated with the occurrence of damages during unfolding. Tensile-bending tests were carried out to study the damage development. The damages were observed by using acoustic emission sensors, a scanning electron microscope, and a camera. The results for the (0,90) ply orientation showed that the mechanism of failure changes from intraply-dominated to interply-dominated as the laminate thickness increases. Furthermore, the change in layup for the thinnest samples, with [(0,90)]2s, [(90,0)]2s, and [(±45)]2s layups, caused a change in the mode of the damage initiation, although all of them showed initiation at the fiber/matrix interfaces. Intra-yarn cracks were found at the compression side of all 4-ply samples. These cracks caused surface yarn buckling in the [(0,90)]2s and [(±45)]2s samples, but not in the [(90,0)]2s.
{"title":"On the thickness and layup dependence on failure mechanisms during unfolding of curved woven composites","authors":"R.D.R. Sitohang,&nbsp;S. Benou,&nbsp;L.L. Warnet,&nbsp;R. Akkerman","doi":"10.1016/j.jcomc.2025.100559","DOIUrl":"10.1016/j.jcomc.2025.100559","url":null,"abstract":"<div><div>This study investigates the failure mechanisms of curved woven Glass/Polyphenylene sulfide (G/PPS) composites and characterizes the critical strains associated with the occurrence of damages during unfolding. Tensile-bending tests were carried out to study the damage development. The damages were observed by using acoustic emission sensors, a scanning electron microscope, and a camera. The results for the (0,90) ply orientation showed that the mechanism of failure changes from intraply-dominated to interply-dominated as the laminate thickness increases. Furthermore, the change in layup for the thinnest samples, with [(0,90)]<sub>2s</sub>, [(90,0)]<sub>2s</sub>, and [(<span><math><mo>±</mo></math></span>45)]<sub>2s</sub> layups, caused a change in the mode of the damage initiation, although all of them showed initiation at the fiber/matrix interfaces. Intra-yarn cracks were found at the compression side of all 4-ply samples. These cracks caused surface yarn buckling in the [(0,90)]<sub>2s</sub> and [(<span><math><mo>±</mo></math></span>45)]<sub>2s</sub> samples, but not in the [(90,0)]<sub>2s</sub>.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100559"},"PeriodicalIF":5.3,"publicationDate":"2025-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143101261","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Safe optimization with grey-box information: Application to composites autoclave processing improvement on the fly
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-01-18 DOI: 10.1016/j.jcomc.2025.100560
Mohammad Amin Roohi , Milad Ramezankhani , Maryam Kamgarpour , Abbas S. Milani
In the manufacture of aerospace-grade composites in the autoclave, the curing process plays a crucial role as it directly governs the quality of the final parts. Maintaining the part’s thermal history, namely, thermal lag and exotherm, under predetermined thresholds as well as achieving a uniform degree of cure throughout the material thickness can result in the desired product quality. Currently, for many such manufacturing applications, the optimization of the curing process (often conducted via trial-and-error) is highly expensive and time-consuming and occasionally leads to failed products. In order to address this problem, in this paper, a Safe Optimization approach is proposed. The suggested framework allows for the on-the-fly optimization of curing process configurations while avoiding interruptions typically encountered during trials. In other words, the proposed algorithm is capable of consistently yielding “pass” products as it navigates toward the optimal configuration. In particular, we introduce a hybrid optimization framework that combines a genetic algorithm, namely NSGA-II, using inexpressive stimulation (white-box) data for finding a safe initial starting point and then, the (black-box) safe logarithmic barrier method for enhancing the product quality presumably using experimental data on-the-fly. Herein, however, as proof of concept, we employ synthetic data throughout the framework in a case study.
{"title":"Safe optimization with grey-box information: Application to composites autoclave processing improvement on the fly","authors":"Mohammad Amin Roohi ,&nbsp;Milad Ramezankhani ,&nbsp;Maryam Kamgarpour ,&nbsp;Abbas S. Milani","doi":"10.1016/j.jcomc.2025.100560","DOIUrl":"10.1016/j.jcomc.2025.100560","url":null,"abstract":"<div><div>In the manufacture of aerospace-grade composites in the autoclave, the curing process plays a crucial role as it directly governs the quality of the final parts. Maintaining the part’s thermal history, namely, thermal lag and exotherm, under predetermined thresholds as well as achieving a uniform degree of cure throughout the material thickness can result in the desired product quality. Currently, for many such manufacturing applications, the optimization of the curing process (often conducted via trial-and-error) is highly expensive and time-consuming and occasionally leads to failed products. In order to address this problem, in this paper, a Safe Optimization approach is proposed. The suggested framework allows for the on-the-fly optimization of curing process configurations while avoiding interruptions typically encountered during trials. In other words, the proposed algorithm is capable of consistently yielding “pass” products as it navigates toward the optimal configuration. In particular, we introduce a hybrid optimization framework that combines a genetic algorithm, namely NSGA-II, using inexpressive stimulation (white-box) data for finding a safe initial starting point and then, the (black-box) safe logarithmic barrier method for enhancing the product quality presumably using experimental data on-the-fly. Herein, however, as proof of concept, we employ synthetic data throughout the framework in a case study.</div></div>","PeriodicalId":34525,"journal":{"name":"Composites Part C Open Access","volume":"16 ","pages":"Article 100560"},"PeriodicalIF":5.3,"publicationDate":"2025-01-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143437730","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Investigation of the effect of extrusion process parameters and filler loading on the performance of LDPE composites reinforced with eggshell powder
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-01-15 DOI: 10.1016/j.jcomc.2025.100561
Yasith S. Perera , Mohammad Naaib , Nisal Ariyasinghe , Chamil Abeykoon
Eggshells are a household waste material that contributes to landfill waste. Polymer composites reinforced with eggshell powder can be produced in large scale with melt blending using twin-screw extrusion, which can aid in reducing eggshell waste. Proper selection of extrusion parameters and filler loading is crucial in achieving composites with desired performance while optimising the extrusion process. Hence, the aim of this study is to investigate the effect of extruder parameters and filler loading on the mechanical, thermal, and rheological properties of low-density polyethylene (LDPE) composites reinforced with eggshell powder, and motor power consumption of the extruder, which should aid in optimising the melt blending process. Composites were produced with three different filler fractions (i.e., 4 wt.%, 8 wt.%, and 12 wt.%), and extruded under three different temperature settings (i.e., low: 160–200 °C, medium: 170–210 °C, and high: 180–220 °C) and three screw speed settings (i.e., 100, 150, and 200 rpm). Injection moulding was used to produce the tensile specimens for mechanical testing using the composite pellets manufactured via melt blending. The motor power consumption of the extruder rose as the screw speed increased and declined as the set temperatures of the barrel heaters increased. The results confirmed that incorporating eggshell powder as a filler led to a slight increase in the extruder's motor power consumption. Scanning electron microscopy results showed non-uniform dispersion of the filler with increasing filler content. The tensile performance of the composites was influenced by both extruder parameters and filler loading. The inclusion of the filler resulted in enhanced stiffness but compromised the ultimate tensile strength. Rheology test results exhibited a reduction in the storage and loss moduli as well as the complex viscosity due to the incorporation of eggshell powder filler. These properties were significantly influenced by the extrusion process parameters as well. However, the influence of extruder parameters and filler loading on the thermal properties of the composites was found to be negligible. This shows that the filler did not significantly disrupt or promote the nucleation and growth of crystalline regions in the LDPE matrix. It was found that, to obtain high tensile properties while retaining good rheological properties, composites with high filler contents of 8–12 wt.% should be processed at a high screw speed of 200 rpm at low set temperature conditions. Overall, the findings of this study indicate that the produced composites could be utilised for applications that require high stiffness. Furthermore, large-scale production of these composites could provide a long-term solution to the eggshell waste problem.
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Composites Part C Open Access
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