Nur Quratul Aini Ismail, Nor Kamilah Sa’at, Mohd Hafiz Mohd Zaid, Norhazlin Zainuddin, Mohd Zul Hilmi Mayzan
{"title":"温度变化对基于 SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 的生物玻璃陶瓷制造的影响","authors":"Nur Quratul Aini Ismail, Nor Kamilah Sa’at, Mohd Hafiz Mohd Zaid, Norhazlin Zainuddin, Mohd Zul Hilmi Mayzan","doi":"10.1007/s41779-024-01049-z","DOIUrl":null,"url":null,"abstract":"<p>Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS<span>\\( -\\)</span>11Na<sub>2</sub>CO<sub>3</sub><span>\\( -\\)</span>24ES<span>\\( -\\)</span>6P<sub>2</sub>O<sub>5</sub><span>\\( -\\)</span>6CaF<sub>2</sub><span>\\( -\\)</span>9Al<sub>2</sub>O<sub>3</sub> (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The physical properties were characterized by density and linear shrinkage. To characterize the structure properties, X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR) were utilized. The high composition of Si and Ca in soda lime silica (SLS) glass and eggshells (ES), respectively, encourage the utilization of waste materials in the production of bioglass-ceramics. The results showed that at a sintering temperature of 950 °C, the crystallization of fluorapatite was the main phase. Moreover, the high density and optimum linear shrinkage were obtained as the sintering temperature increased. Additionally, grain growth and densification took place at this temperature. The compressive strength of bioglass-ceramics is influenced by sintering temperature and the optimal compressive strength is 136.58 MPa.</p>","PeriodicalId":673,"journal":{"name":"Journal of the Australian Ceramic Society","volume":"2016 1","pages":""},"PeriodicalIF":1.8000,"publicationDate":"2024-07-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics\",\"authors\":\"Nur Quratul Aini Ismail, Nor Kamilah Sa’at, Mohd Hafiz Mohd Zaid, Norhazlin Zainuddin, Mohd Zul Hilmi Mayzan\",\"doi\":\"10.1007/s41779-024-01049-z\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS<span>\\\\( -\\\\)</span>11Na<sub>2</sub>CO<sub>3</sub><span>\\\\( -\\\\)</span>24ES<span>\\\\( -\\\\)</span>6P<sub>2</sub>O<sub>5</sub><span>\\\\( -\\\\)</span>6CaF<sub>2</sub><span>\\\\( -\\\\)</span>9Al<sub>2</sub>O<sub>3</sub> (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The physical properties were characterized by density and linear shrinkage. To characterize the structure properties, X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR) were utilized. The high composition of Si and Ca in soda lime silica (SLS) glass and eggshells (ES), respectively, encourage the utilization of waste materials in the production of bioglass-ceramics. The results showed that at a sintering temperature of 950 °C, the crystallization of fluorapatite was the main phase. Moreover, the high density and optimum linear shrinkage were obtained as the sintering temperature increased. Additionally, grain growth and densification took place at this temperature. The compressive strength of bioglass-ceramics is influenced by sintering temperature and the optimal compressive strength is 136.58 MPa.</p>\",\"PeriodicalId\":673,\"journal\":{\"name\":\"Journal of the Australian Ceramic Society\",\"volume\":\"2016 1\",\"pages\":\"\"},\"PeriodicalIF\":1.8000,\"publicationDate\":\"2024-07-08\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of the Australian Ceramic Society\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1007/s41779-024-01049-z\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the Australian Ceramic Society","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1007/s41779-024-01049-z","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics
Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS\( -\)11Na2CO3\( -\)24ES\( -\)6P2O5\( -\)6CaF2\( -\)9Al2O3 (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The physical properties were characterized by density and linear shrinkage. To characterize the structure properties, X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR) were utilized. The high composition of Si and Ca in soda lime silica (SLS) glass and eggshells (ES), respectively, encourage the utilization of waste materials in the production of bioglass-ceramics. The results showed that at a sintering temperature of 950 °C, the crystallization of fluorapatite was the main phase. Moreover, the high density and optimum linear shrinkage were obtained as the sintering temperature increased. Additionally, grain growth and densification took place at this temperature. The compressive strength of bioglass-ceramics is influenced by sintering temperature and the optimal compressive strength is 136.58 MPa.
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