用于潜伏指纹识别的氧化铜纳米结构评估

IF 1.7 4区 综合性期刊 Q2 MULTIDISCIPLINARY SCIENCES Journal of Radiation Research and Applied Sciences Pub Date : 2024-07-07 DOI:10.1016/j.jrras.2024.101018
Shalu Atri , Gurvinder Singh Bumbrah , Kapil Verma , Bhawana Joshi
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引用次数: 0

摘要

纳米技术给法医学的各个领域带来了革命性的变化,尤其是在证据的高效检验方面。在本研究中,我们报告了利用水热法可扩展地合成氧化铜(CuO)纳米片及其在潜伏指纹法证检验中的应用。我们使用粉末 X 射线衍射 (PXRD)、拉曼光谱和傅立叶变换红外光谱 (FTIR) 等先进光谱方法对 CuO 纳米颗粒进行了鉴定和结构表征。通过 Le Bail 精炼,确认了 CuO 纳米片在单斜对称性(空间群 C2/c)上的稳定性。利用扫描电子显微镜(SEM)进行的形态学研究表明,CuO 纳米片呈现出矩形薄板状形态。采用粉末撒粉法测试了这些纳米片在干燥、非吸收性基底上检验和显现新鲜和老化(7 天)潜指纹的适用性。该配方成功地在各种基底上显现出清晰锐利的指纹,可以在没有任何背景干扰的情况下观察指纹的二级细节。此外,这些纳米片不具危险性且成本效益高,因此适合作为指纹显影剂用于从犯罪现场回收的各种干燥、非吸收性表面。
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Nanostructured assessment of copper oxide for latent fingerprint recognition

Nanotechnology has revolutionized the different fields of forensic science, particularly in the efficient examination of evidence. In this study, we report scalable synthesis of copper oxide (CuO) nanosheets by using hydrothermal method and its exploration in the forensic examination of latent fingerprints. The identification and structural characterization of CuO nanoparticles were carried out using advanced spectroscopic methods such as powder X-ray diffraction (PXRD), Raman spectroscopy, and Fourier transform infrared spectroscopy (FTIR). The stabilization of CuO nanosheets in monoclinic symmetry (space group C2/c) was confirmed through Le Bail refinements. Morphological studies based on scanning electron microscopy (SEM) revealed that the CuO nanosheets exhibit, a rectangular, thin plate like morphology.

The applicability of these nanosheets was tested for examining and developing fresh and aged (7 days old) latent fingerprints on dry, non-absorbent substrates using the powder dusting method. The formulation successfully developed sharp and clear fingerprints on various substrates, allowing the second-level details of the fingerprints to be viewed without any background interference. Additionally, these nanosheets are non-hazardous and cost-effective, making them a suitable fingerprint developing agent for a wide range of dry, non-absorbent surfaces recovered from crime scenes.

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来源期刊
自引率
5.90%
发文量
130
审稿时长
16 weeks
期刊介绍: Journal of Radiation Research and Applied Sciences provides a high quality medium for the publication of substantial, original and scientific and technological papers on the development and applications of nuclear, radiation and isotopes in biology, medicine, drugs, biochemistry, microbiology, agriculture, entomology, food technology, chemistry, physics, solid states, engineering, environmental and applied sciences.
期刊最新文献
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