近表面粘附形态和粘合线填料对剪切加载复合材料粘接应变分布的微观力学影响

IF 3.2 3区 材料科学 Q2 ENGINEERING, CHEMICAL International Journal of Adhesion and Adhesives Pub Date : 2024-07-20 DOI:10.1016/j.ijadhadh.2024.103798
Jörg Gregor Diez , Jens Holtmannspötter , Elisa Arikan , Philipp Höfer
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引用次数: 0

摘要

粘合剂连接区域的近表面形态对粘合复合材料的疲劳行为有重大影响。在复合材料的生产过程中,有很多机会可以通过使用不同的表层半成品来决定表面形态。例如,可以使用离型膜和剥离层织物来调节上层树脂的厚度和形貌。这些材料随后会在复合材料的进一步加工和组装之前被去除,在材料表面留下负面印记。由此产生的结构尺寸通常只有几微米。粘合剂中的另一种成分是填料,其直径也在相同的尺寸范围内。粘合形态和填料都会影响粘合接头的宏观行为。通过在扫描电子显微镜下对粘接的端面缺口挠曲试样进行检查,可以观察到粘合剂层和粘合剂近表面区域在负载下的细节。利用数字图像相关技术对这些扫描电子显微镜图像进行评估,可对微米范围内的应变分布进行定量分析。这样就能确定粘合剂的近表面形态和粘合线的组成(如填充物、网格)对沿粘合线的剪切应变分布的影响。因此,可以得出它们对粘合剂使用寿命影响的结论。
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Micromechanical influence of near-surface adherend morphology and bondline fillers on the strain distribution in shear-loaded composite bonds

The near-surface morphology in the joining areas of adherends has a significant impact on the fatigue behavior of adhesively bonded composites. In the production process of composites, numerous opportunities exist for dictating surface morphology through the utilization of different top-layer semi-finished products. For instance, release films and peel ply fabrics can be employed to modulate the thickness and topography of the upper resin layer. These materials are subsequently removed prior to the further processing and assembly of the composites, leaving their negative imprint on the material surface. The resultant structures typically exhibit dimensions on the scale of a few micrometers. Another component in adhesive bonds are fillers, which have diameters in the same size range. Both adherend morphology and fillers influence the macroscopic behavior of the bonded joint. By in situ examining bonded end-notched flexure specimens inside a scanning electron microscope, the adhesive layer and the near-surface region of the adherends can be observed in detail under load. Evaluating these scanning electron microscope images using digital image correlation enables quantitative analysis of the strain distribution within the micrometer range. This allows the identification of the effects the adherend's near-surface morphology and the composition of the bondline (e.g. fillers, meshes) have on the shear strain distribution along bondlines. Consequently, conclusions can be drawn regarding their influence on the service life of adhesive bonds.

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来源期刊
International Journal of Adhesion and Adhesives
International Journal of Adhesion and Adhesives 工程技术-材料科学:综合
CiteScore
6.90
自引率
8.80%
发文量
200
审稿时长
8.3 months
期刊介绍: The International Journal of Adhesion and Adhesives draws together the many aspects of the science and technology of adhesive materials, from fundamental research and development work to industrial applications. Subject areas covered include: interfacial interactions, surface chemistry, methods of testing, accumulation of test data on physical and mechanical properties, environmental effects, new adhesive materials, sealants, design of bonded joints, and manufacturing technology.
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