通过优化 FFF 工艺参数提高聚乳酸/碳纳米管复合材料的拉伸模量和抗弯强度

IF 3.6 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Journal of Thermoplastic Composite Materials Pub Date : 2024-08-07 DOI:10.1177/08927057241268831
Hatam Hardani, Mahmoud Afshari, Mohammad Reza Samadi, Hossein Afshari, Santi Ago López
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引用次数: 0

摘要

熔融长丝制造(FFF)是热塑性聚合物和复合材料最常见的三维打印方法之一,因为它易于使用且成本低廉。用于工业应用的打印聚合物部件需要理想的机械性能。因此,本研究对熔融长丝制造的工艺参数进行了优化,以提高聚乳酸/碳纳米管(PLA/CNT)复合材料的杨氏模量和抗弯强度。为此,应用响应面法(RSM)和可取函数技术(DFT)找到了 CNT 含量、印刷速度和喷嘴温度等有效参数的最佳值。印刷样品通过 DSC、TGA 和 SEM 分析进行检测。DSC 和 TGA 分析结果表明,在聚乳酸中添加 CNT 增强了聚乳酸/CNT 复合材料的热稳定性。优化结果还表明,当 CNT 含量为 2.9 wt%、打印速度为 20 mm/s、喷嘴温度为 210°C 时,聚乳酸/CNT 复合材料的杨氏模量和抗弯强度都有所提高。
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An enhancement in the tensile modulus and bending resistance of polylactic acid/carbon nanotube composite by optimizing FFF process parameters
Fused-filament fabrication (FFF) is one of the most common 3D printing methods for thermoplastic polymers and composite materials because it is easy to use and is low-cost. The printed polymer parts for industrial applications require desirable mechanical properties. Therefore, in the present research, the process parameters of fused filament fabrication are optimized to enhance the Young’s modulus and bending resistance of polylactic acid/carbon nanotube (PLA/CNT) composite. For this purpose, the response surface method (RSM) and desirability function technique (DFT) are applied to find the optimal values of the effective parameters of CNT content, printing speed and nozzle temperature. The printed samples were examined by using DSC, TGA and SEM analyses. The results of DSC and TGA analyses indicated that the addition of CNT into PLA enhanced the thermal stability of PLA/CNT composite. It was also observed from the optimization results that the Young’s modulus and bending resistance of PLA/CNT composite improved at CNT content of 2.9 wt%, printing speed of 20 mm/s and nozzle temperature of 210°C.
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来源期刊
Journal of Thermoplastic Composite Materials
Journal of Thermoplastic Composite Materials 工程技术-材料科学:复合
CiteScore
8.00
自引率
18.20%
发文量
104
审稿时长
5.9 months
期刊介绍: The Journal of Thermoplastic Composite Materials is a fully peer-reviewed international journal that publishes original research and review articles on polymers, nanocomposites, and particulate-, discontinuous-, and continuous-fiber-reinforced materials in the areas of processing, materials science, mechanics, durability, design, non destructive evaluation and manufacturing science. This journal is a member of the Committee on Publication Ethics (COPE).
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