利用碳化硅粉末床采用 SPS 法制造 Si3N4 陶瓷球

IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS International Journal of Applied Ceramic Technology Pub Date : 2024-08-07 DOI:10.1111/ijac.14879
Zhen-Quan Liang, Jia-Ji Liang, Jun-Jie Yu, Pei-Bin Cai, Wei-Ming Guo, Hua-Tay Lin
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引用次数: 0

摘要

火花等离子烧结(SPS)是一种超快烧结方法,可结合单轴压力制备几何形状简单的陶瓷和陶瓷复合材料。本研究旨在为 Si3N4 陶瓷球提出一种无需改变工具和设备的 SPS 致密化方法。用于烧结的 Si3N4 陶瓷球被放置在用于 SPS 的传统模具内的 SiC 粉末床中。研究系统地探讨了烧结前温度(1400°C、1500°C 和 1600°C)和 SPS 温度(1600°C、1700°C 和 1800°C)对 Si3N4 陶瓷球的球度、相对密度、相组成、微观结构和机械性能的影响。实验结果表明,在 1600°C 的预烧结温度和 SPS 温度下,结合使用碳化硅粉末床和 SPS 方法,Si3N4 陶瓷球成功实现了球度(0.94 ± 0.02)、相对密度(98.4%)和机械性能(维氏硬度:17.5 ± 0.4 GPa,断裂韧性:6.4 ± 0.1 MPa-m1/2)的最佳组合。因此,SPS 方法证明了其制造性能优异的 Si3N4 陶瓷球的能力。
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Fabrication of Si3N4 ceramic balls by SPS method with SiC powder bed

Spark plasma sintering (SPS) is an ultrafast sintering method for the preparation of ceramics and ceramic composites with simple geometrical shapes, with the combined application of uniaxial pressure. This study aims to propose an SPS densification method for Si3N4 ceramic balls without necessitating alterations to tools and equipment. The Si3N4 ceramic balls intended for sintering are positioned within a SiC powder bed inside the conventional die used in SPS. The study systematically investigates the effects of presintering temperature (1400°C, 1500°C, and 1600°C) and SPS temperature (1600°C, 1700°C, and 1800°C) on the sphericity, relative density, phase composition, microstructure, and mechanical properties of Si3N4 ceramic balls. Experimental findings reveal that Si3N4 ceramic balls exhibiting an optimal combination of sphericity (0.94 ± 0.02), relative density (98.4%), and mechanical properties (Vickers hardness: 17.5 ± 0.4 GPa, fracture toughness: 6.4 ± 0.1 MPa·m1/2) were successfully achieved at a pre-sintering temperature and SPS temperature of 1600°C, coupled with the use of a SiC powder bed and SPS method. Consequently, the SPS method demonstrates its capability to fabricate Si3N4 ceramic balls with excellent performance.

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来源期刊
International Journal of Applied Ceramic Technology
International Journal of Applied Ceramic Technology 工程技术-材料科学:硅酸盐
CiteScore
3.90
自引率
9.50%
发文量
280
审稿时长
4.5 months
期刊介绍: The International Journal of Applied Ceramic Technology publishes cutting edge applied research and development work focused on commercialization of engineered ceramics, products and processes. The publication also explores the barriers to commercialization, design and testing, environmental health issues, international standardization activities, databases, and cost models. Designed to get high quality information to end-users quickly, the peer process is led by an editorial board of experts from industry, government, and universities. Each issue focuses on a high-interest, high-impact topic plus includes a range of papers detailing applications of ceramics. Papers on all aspects of applied ceramics are welcome including those in the following areas: Nanotechnology applications; Ceramic Armor; Ceramic and Technology for Energy Applications (e.g., Fuel Cells, Batteries, Solar, Thermoelectric, and HT Superconductors); Ceramic Matrix Composites; Functional Materials; Thermal and Environmental Barrier Coatings; Bioceramic Applications; Green Manufacturing; Ceramic Processing; Glass Technology; Fiber optics; Ceramics in Environmental Applications; Ceramics in Electronic, Photonic and Magnetic Applications;
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