树脂胶合剂中硅烷偶联剂的功效

IF 3.2 3区 材料科学 Q2 ENGINEERING, CHEMICAL International Journal of Adhesion and Adhesives Pub Date : 2024-08-14 DOI:10.1016/j.ijadhadh.2024.103808
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引用次数: 0

摘要

本研究的目的是通过剪切粘结强度和接触角研究来确定树脂粘结剂中的硅烷是否会与二硅酸锂表面发生化学粘结,从而研究一种新型含硅烷的自粘树脂粘结剂。我们将含硅烷的水泥 Panavia SA Cement Universal(可乐丽,日本东京)与传统硅烷处理的树脂衬垫水泥 Duo-Link Universal(Bisco Inc.结果表明,微机械保留对粘接强度有很大的贡献。然而,在经过 20,000 次热循环和在 37 °C 水中存放 6 个月的老化研究后,与对照组相比,含硅烷的自粘性树脂粘接剂的剪切粘接强度明显下降。接触角研究表明,虽然含有硅烷的浆料确实有效地增加了经处理的二硅酸锂表面的疏水性,但它需要超过 3 小时的接触时间,这在临床使用中并不具有代表性。
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Effectiveness of a silane coupling agent in a resin luting cement

The objective of this study was to investigate a new silane-containing self-adhesive resin luting cement with both shear bond strength and contact angle studies to determine if silane in a resin cement would chemically bond to a lithium disilicate surface. The silane-containing cement, Panavia SA Cement Universal (Kuraray, Tokyo, Japan) was tested against a control case where a traditional silane treatment was paired with resin-luting cement, Duo-Link Universal (Bisco Inc., Schaumburg, IL, USA) with immediate shear bond strength testing on both polished and etched lithium disilicate, as well as after thermocycling. It was determined that micromechanical retention provided a substantial contribution to bond strength. However, after an aging study with 20,000 thermocycles and then storage for 6 months in 37 °C water, the silane-containing, self-adhesive resin cement significantly decreased in shear bond strength when compared to the control. From contact angle studies, while it was shown that the paste containing the silane did effectively increase hydrophobicity of the treated lithium disilicate surface, it required over 3 h contact time, which was not representative of clinical use.

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来源期刊
International Journal of Adhesion and Adhesives
International Journal of Adhesion and Adhesives 工程技术-材料科学:综合
CiteScore
6.90
自引率
8.80%
发文量
200
审稿时长
8.3 months
期刊介绍: The International Journal of Adhesion and Adhesives draws together the many aspects of the science and technology of adhesive materials, from fundamental research and development work to industrial applications. Subject areas covered include: interfacial interactions, surface chemistry, methods of testing, accumulation of test data on physical and mechanical properties, environmental effects, new adhesive materials, sealants, design of bonded joints, and manufacturing technology.
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