用于现场快速监测 E120 食品添加剂的简单通用电化学测定法

IF 4 2区 农林科学 Q2 CHEMISTRY, APPLIED Journal of Food Composition and Analysis Pub Date : 2024-09-06 DOI:10.1016/j.jfca.2024.106709
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引用次数: 0

摘要

本研究开发了一种经济有效的电化学方法,用于快速监测胭脂虫酸(E120 食品添加剂)的含量。这种检测方法将 50 μL 液体样品直接涂抹在市售的丝网印刷伏安传感器上,从而简化了检测过程。随后的阳极氧化专门针对复合基质中的卡米尼克酸。为了针对常见饮料的不同成分实现最大的选择性,峰面积电流响应在每 100 mL-1 含 0.01-50 mg 氨基甲酸的线性范围内进行了校准,灵敏度为 2.232 μA V mg-1 mL,检测限为每 100 mL 含 4 × 10-3 mg 氨基甲酸。一次使用五个传感器就能获得令人满意的精确度(相对标准偏差小于 4.5%)。所开发的筛选电化学测定法在食品安全控制方面的实用性已在甜味糖果、软饮料和能量饮料的分析中得到了成功验证。
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A simple and universal electrochemical assay for rapid field monitoring of E120 food additive

A cost-effective electrochemical method was developed to rapidly monitor carminic acid (E120 food additive) levels. This assay simplifies the process by directly applying 50 μL of liquid sample onto a commercially available screen-printed voltammetric sensor. The subsequent anodic oxidation specifically targets the carminic acid within the complex matrix. To achieve maximum selectivity with regard to the variable composition of common beverages, the peak area current response was calibrated within a linear range 0.01–50 mg per 100 mL−1 of carminic acid, with a sensitivity of 2.232 μA V mg−1 mL, and a detection limit of 4 × 10−3 mg per 100 mL. A satisfactory precision (relative standard deviation less than 4.5 %) has been found with a single use of five sensors. Practical applicability of the developed screening electrochemical assay in the food safety control was successfully verified in analysis of sweet candies, soft beverages, and energy drinks.

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来源期刊
Journal of Food Composition and Analysis
Journal of Food Composition and Analysis 工程技术-食品科技
CiteScore
6.20
自引率
11.60%
发文量
601
审稿时长
53 days
期刊介绍: The Journal of Food Composition and Analysis publishes manuscripts on scientific aspects of data on the chemical composition of human foods, with particular emphasis on actual data on composition of foods; analytical methods; studies on the manipulation, storage, distribution and use of food composition data; and studies on the statistics, use and distribution of such data and data systems. The Journal''s basis is nutrient composition, with increasing emphasis on bioactive non-nutrient and anti-nutrient components. Papers must provide sufficient description of the food samples, analytical methods, quality control procedures and statistical treatments of the data to permit the end users of the food composition data to evaluate the appropriateness of such data in their projects. The Journal does not publish papers on: microbiological compounds; sensory quality; aromatics/volatiles in food and wine; essential oils; organoleptic characteristics of food; physical properties; or clinical papers and pharmacology-related papers.
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