{"title":"添加不同比例的钛酸钡对β-磷酸三钙特性的影响","authors":"Yagmur Hafizoglu, Suleyman Serdar Pazarlioglu","doi":"10.1007/s41779-024-01086-8","DOIUrl":null,"url":null,"abstract":"<p>This study examines the effect of barium titanate addition at 3 different rates (BaTiO<sub>3</sub>; 1wt%, 3 wt% and 5 wt%) on the mechanical performance, in vitro bioactivity and morphological structure of beta tricalcium phosphate (β-TCP). The best results for β-TCP were achieved after sintering at 1200<sup>o</sup>C and with an average grain size of 5.077 ± 0.571 µ. However, sintering at 1250<sup>o</sup>C caused a 45% increase in the grain size of β-TCP, micro cracking and decomposition of 3.2% into alpha tricalcium phosphate (α-TCP) resulting in a decrease in its properties. Depending on the BaTiO<sub>3</sub> ratio, 9 different phases with general chemical compositions of Ba<sub>x</sub>/Ca<sub>y</sub>-Ti<sub>m</sub>-O<sub>n</sub>, as well as α-TCP, were detected in the composites. As the sintering temperature and BaTiO<sub>3</sub> ratio increased, the α-TCP ratio in the composites increased to 49.7%. The highest mechanical performances in composites were achieved at the sintering temperature of 1200<sup>o</sup>C and with the addition of 3wt%-BaTiO<sub>3</sub>. In vitro studies showed that the surface of this composite was completely covered with apatite on the 28th day.</p>","PeriodicalId":673,"journal":{"name":"Journal of the Australian Ceramic Society","volume":null,"pages":null},"PeriodicalIF":1.8000,"publicationDate":"2024-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of addition of varying percentages of barium titanate on the properties of beta-tricalcium phosphate\",\"authors\":\"Yagmur Hafizoglu, Suleyman Serdar Pazarlioglu\",\"doi\":\"10.1007/s41779-024-01086-8\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>This study examines the effect of barium titanate addition at 3 different rates (BaTiO<sub>3</sub>; 1wt%, 3 wt% and 5 wt%) on the mechanical performance, in vitro bioactivity and morphological structure of beta tricalcium phosphate (β-TCP). The best results for β-TCP were achieved after sintering at 1200<sup>o</sup>C and with an average grain size of 5.077 ± 0.571 µ. However, sintering at 1250<sup>o</sup>C caused a 45% increase in the grain size of β-TCP, micro cracking and decomposition of 3.2% into alpha tricalcium phosphate (α-TCP) resulting in a decrease in its properties. Depending on the BaTiO<sub>3</sub> ratio, 9 different phases with general chemical compositions of Ba<sub>x</sub>/Ca<sub>y</sub>-Ti<sub>m</sub>-O<sub>n</sub>, as well as α-TCP, were detected in the composites. As the sintering temperature and BaTiO<sub>3</sub> ratio increased, the α-TCP ratio in the composites increased to 49.7%. The highest mechanical performances in composites were achieved at the sintering temperature of 1200<sup>o</sup>C and with the addition of 3wt%-BaTiO<sub>3</sub>. In vitro studies showed that the surface of this composite was completely covered with apatite on the 28th day.</p>\",\"PeriodicalId\":673,\"journal\":{\"name\":\"Journal of the Australian Ceramic Society\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":1.8000,\"publicationDate\":\"2024-09-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of the Australian Ceramic Society\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1007/s41779-024-01086-8\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the Australian Ceramic Society","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1007/s41779-024-01086-8","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
Effect of addition of varying percentages of barium titanate on the properties of beta-tricalcium phosphate
This study examines the effect of barium titanate addition at 3 different rates (BaTiO3; 1wt%, 3 wt% and 5 wt%) on the mechanical performance, in vitro bioactivity and morphological structure of beta tricalcium phosphate (β-TCP). The best results for β-TCP were achieved after sintering at 1200oC and with an average grain size of 5.077 ± 0.571 µ. However, sintering at 1250oC caused a 45% increase in the grain size of β-TCP, micro cracking and decomposition of 3.2% into alpha tricalcium phosphate (α-TCP) resulting in a decrease in its properties. Depending on the BaTiO3 ratio, 9 different phases with general chemical compositions of Bax/Cay-Tim-On, as well as α-TCP, were detected in the composites. As the sintering temperature and BaTiO3 ratio increased, the α-TCP ratio in the composites increased to 49.7%. The highest mechanical performances in composites were achieved at the sintering temperature of 1200oC and with the addition of 3wt%-BaTiO3. In vitro studies showed that the surface of this composite was completely covered with apatite on the 28th day.
期刊介绍:
Publishes high quality research and technical papers in all areas of ceramic and related materials
Spans the broad and growing fields of ceramic technology, material science and bioceramics
Chronicles new advances in ceramic materials, manufacturing processes and applications
Journal of the Australian Ceramic Society since 1965
Professional language editing service is available through our affiliates Nature Research Editing Service and American Journal Experts at the author''s cost and does not guarantee that the manuscript will be reviewed or accepted