添加不同比例的钛酸钡对β-磷酸三钙特性的影响

IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS Journal of the Australian Ceramic Society Pub Date : 2024-09-05 DOI:10.1007/s41779-024-01086-8
Yagmur Hafizoglu, Suleyman Serdar Pazarlioglu
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引用次数: 0

摘要

本研究探讨了钛酸钡 3 种不同添加量(BaTiO3;1 wt%、3 wt% 和 5 wt%)对β-磷酸三钙(β-TCP)的机械性能、体外生物活性和形态结构的影响。在 1200 摄氏度烧结时,β-TCP 的结果最好,平均晶粒大小为 5.077 ± 0.571 µ。然而,在 1250 摄氏度烧结时,β-TCP 的晶粒大小增加了 45%,出现微裂纹,3.2% 分解成α-磷酸三钙(α-TCP),导致其性能下降。根据 BaTiO3 的比例,在复合材料中检测到 9 种不同的相,其化学成分一般为 Bax/Cay-Tim-On 以及 α-TCP。随着烧结温度和 BaTiO3 比率的增加,复合材料中的α-TCP 比率增至 49.7%。在烧结温度为 1200 摄氏度和掺入 3wt%BaTiO3 时,复合材料的机械性能最高。体外研究表明,这种复合材料的表面在第 28 天完全被磷灰石覆盖。
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Effect of addition of varying percentages of barium titanate on the properties of beta-tricalcium phosphate

This study examines the effect of barium titanate addition at 3 different rates (BaTiO3; 1wt%, 3 wt% and 5 wt%) on the mechanical performance, in vitro bioactivity and morphological structure of beta tricalcium phosphate (β-TCP). The best results for β-TCP were achieved after sintering at 1200oC and with an average grain size of 5.077 ± 0.571 µ. However, sintering at 1250oC caused a 45% increase in the grain size of β-TCP, micro cracking and decomposition of 3.2% into alpha tricalcium phosphate (α-TCP) resulting in a decrease in its properties. Depending on the BaTiO3 ratio, 9 different phases with general chemical compositions of Bax/Cay-Tim-On, as well as α-TCP, were detected in the composites. As the sintering temperature and BaTiO3 ratio increased, the α-TCP ratio in the composites increased to 49.7%. The highest mechanical performances in composites were achieved at the sintering temperature of 1200oC and with the addition of 3wt%-BaTiO3. In vitro studies showed that the surface of this composite was completely covered with apatite on the 28th day.

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来源期刊
Journal of the Australian Ceramic Society
Journal of the Australian Ceramic Society Materials Science-Materials Chemistry
CiteScore
3.70
自引率
5.30%
发文量
123
期刊介绍: Publishes high quality research and technical papers in all areas of ceramic and related materials Spans the broad and growing fields of ceramic technology, material science and bioceramics Chronicles new advances in ceramic materials, manufacturing processes and applications Journal of the Australian Ceramic Society since 1965 Professional language editing service is available through our affiliates Nature Research Editing Service and American Journal Experts at the author''s cost and does not guarantee that the manuscript will be reviewed or accepted
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