{"title":"添加不同比例的钛酸钡对β-磷酸三钙特性的影响","authors":"Yagmur Hafizoglu, Suleyman Serdar Pazarlioglu","doi":"10.1007/s41779-024-01086-8","DOIUrl":null,"url":null,"abstract":"<p>This study examines the effect of barium titanate addition at 3 different rates (BaTiO<sub>3</sub>; 1wt%, 3 wt% and 5 wt%) on the mechanical performance, in vitro bioactivity and morphological structure of beta tricalcium phosphate (β-TCP). The best results for β-TCP were achieved after sintering at 1200<sup>o</sup>C and with an average grain size of 5.077 ± 0.571 µ. However, sintering at 1250<sup>o</sup>C caused a 45% increase in the grain size of β-TCP, micro cracking and decomposition of 3.2% into alpha tricalcium phosphate (α-TCP) resulting in a decrease in its properties. Depending on the BaTiO<sub>3</sub> ratio, 9 different phases with general chemical compositions of Ba<sub>x</sub>/Ca<sub>y</sub>-Ti<sub>m</sub>-O<sub>n</sub>, as well as α-TCP, were detected in the composites. As the sintering temperature and BaTiO<sub>3</sub> ratio increased, the α-TCP ratio in the composites increased to 49.7%. The highest mechanical performances in composites were achieved at the sintering temperature of 1200<sup>o</sup>C and with the addition of 3wt%-BaTiO<sub>3</sub>. In vitro studies showed that the surface of this composite was completely covered with apatite on the 28th day.</p>","PeriodicalId":673,"journal":{"name":"Journal of the Australian Ceramic Society","volume":"29 1","pages":""},"PeriodicalIF":1.8000,"publicationDate":"2024-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Effect of addition of varying percentages of barium titanate on the properties of beta-tricalcium phosphate\",\"authors\":\"Yagmur Hafizoglu, Suleyman Serdar Pazarlioglu\",\"doi\":\"10.1007/s41779-024-01086-8\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>This study examines the effect of barium titanate addition at 3 different rates (BaTiO<sub>3</sub>; 1wt%, 3 wt% and 5 wt%) on the mechanical performance, in vitro bioactivity and morphological structure of beta tricalcium phosphate (β-TCP). The best results for β-TCP were achieved after sintering at 1200<sup>o</sup>C and with an average grain size of 5.077 ± 0.571 µ. However, sintering at 1250<sup>o</sup>C caused a 45% increase in the grain size of β-TCP, micro cracking and decomposition of 3.2% into alpha tricalcium phosphate (α-TCP) resulting in a decrease in its properties. Depending on the BaTiO<sub>3</sub> ratio, 9 different phases with general chemical compositions of Ba<sub>x</sub>/Ca<sub>y</sub>-Ti<sub>m</sub>-O<sub>n</sub>, as well as α-TCP, were detected in the composites. As the sintering temperature and BaTiO<sub>3</sub> ratio increased, the α-TCP ratio in the composites increased to 49.7%. The highest mechanical performances in composites were achieved at the sintering temperature of 1200<sup>o</sup>C and with the addition of 3wt%-BaTiO<sub>3</sub>. In vitro studies showed that the surface of this composite was completely covered with apatite on the 28th day.</p>\",\"PeriodicalId\":673,\"journal\":{\"name\":\"Journal of the Australian Ceramic Society\",\"volume\":\"29 1\",\"pages\":\"\"},\"PeriodicalIF\":1.8000,\"publicationDate\":\"2024-09-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of the Australian Ceramic Society\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1007/s41779-024-01086-8\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the Australian Ceramic Society","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1007/s41779-024-01086-8","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
Effect of addition of varying percentages of barium titanate on the properties of beta-tricalcium phosphate
This study examines the effect of barium titanate addition at 3 different rates (BaTiO3; 1wt%, 3 wt% and 5 wt%) on the mechanical performance, in vitro bioactivity and morphological structure of beta tricalcium phosphate (β-TCP). The best results for β-TCP were achieved after sintering at 1200oC and with an average grain size of 5.077 ± 0.571 µ. However, sintering at 1250oC caused a 45% increase in the grain size of β-TCP, micro cracking and decomposition of 3.2% into alpha tricalcium phosphate (α-TCP) resulting in a decrease in its properties. Depending on the BaTiO3 ratio, 9 different phases with general chemical compositions of Bax/Cay-Tim-On, as well as α-TCP, were detected in the composites. As the sintering temperature and BaTiO3 ratio increased, the α-TCP ratio in the composites increased to 49.7%. The highest mechanical performances in composites were achieved at the sintering temperature of 1200oC and with the addition of 3wt%-BaTiO3. In vitro studies showed that the surface of this composite was completely covered with apatite on the 28th day.
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Journal of the Australian Ceramic Society since 1965
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