模拟体液下氮化钛涂层 316 L 不锈钢摩擦学行为的实验研究

IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS Journal of the Australian Ceramic Society Pub Date : 2024-08-13 DOI:10.1007/s41779-024-01075-x
R. Gopi, I. Saravanan, A. Devaraju, M. Karthikeyan
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引用次数: 0

摘要

本研究讨论了使用阴极电弧沉积(CAD)技术在不锈钢(SS)316 L 基体上沉积硬氮化钛(TiN)涂层的效果。研究了原样和陶瓷涂层样品的硬度、X 射线衍射和涂层粗糙度。从 X 射线衍射分析中可以观察到,由于 TiN 的存在,涂层试样中的乌斯邦石相有所增加。SS 316 L 试样的硬度为 217.66 HV,阴极电弧沉积涂层试样的硬度是未涂层圆盘的五倍。在模拟体液(SBF)条件下,使用球盘摩擦仪对硬质 TiN 涂层 316 L 不锈钢进行了生物摩擦学测试。在 2、4 和 6 N 的测试条件下,对不锈钢进行了特定磨损率及其机理测试。对磨损表面的扫描电子显微镜观察揭示了接触表面的磨损机理。为了证实陶瓷涂层 SS 316 L 试样与正常细胞系的生物相容性,还进行了 3-(4,5-二甲基噻唑基-2)-2,5-二苯基溴化四氮唑(MTT)和细胞活力测试。本研究的重点是对 316 L 不锈钢的需求以及在生物植入应用中使用 CAD 涂层来抑制磨损。
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Experimental investigation on tribological behavior of titanium nitride-coated 316 L stainless steel under simulated body fluid

The present study discusses the effect of a hard titanium nitride (TiN) coating deposited on the stainless steel (SS) 316 L substrate using the cathodic arc deposition (CAD) technique. The hardness, X-ray diffraction, and roughness of the coating properties of as-received, and ceramic coated samples were studied. The osbornite phase increased in the coated specimen due to TiN which is observed from X-ray diffraction analysis. The SS 316 L sample showed a hardness of 217.66 HV, and the cathodic arc deposition coating samples increased five times compared to uncoated disc in hardness. The bio tribological testing of the hard TiN coated 316 L stainless steel was carried out using a ball-on-disc tribometer under simulated body fluid (SBF). The specific wear rate and its mechanism were carried out for the testing conditions of 2, 4, and 6 N with the counterpart of stainless steel. Scanning electron microscopy observation of the worn surfaces revealed the wear mechanisms of the contact surfaces. The 3-(4, 5-dimethylthiazolyl-2)-2, 5-diphenyltetrazolium bromide (MTT) and cell viability tests were conducted in order to confirm the biocompatibility with the normal cell line on the ceramic coated SS 316 L specimen. The present study focused on the demand for stainless steel 316 L and the usage of CAD coatings to suppress wear in bioimplant applications.

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来源期刊
Journal of the Australian Ceramic Society
Journal of the Australian Ceramic Society Materials Science-Materials Chemistry
CiteScore
3.70
自引率
5.30%
发文量
123
期刊介绍: Publishes high quality research and technical papers in all areas of ceramic and related materials Spans the broad and growing fields of ceramic technology, material science and bioceramics Chronicles new advances in ceramic materials, manufacturing processes and applications Journal of the Australian Ceramic Society since 1965 Professional language editing service is available through our affiliates Nature Research Editing Service and American Journal Experts at the author''s cost and does not guarantee that the manuscript will be reviewed or accepted
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