通过现场观察研究 40Cr10Si2Mo 钢的奥氏体晶粒长大行为和马氏体相变机理

Tongyao Yang, Qingjuan Wang, Zhongze Du, Wen Wang, Longxin Li, Zhiyi Li, Bofan Xu
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摘要

40Cr10Si2Mo 钢因其优异的机械性能而得到广泛应用,其中晶粒大小是决定后续相变过程和材料微观结构性能的关键因素。本文报道了利用高温激光扫描共聚焦显微镜(HT-LSCM)进行原位观察实验,系统研究了 40Cr10Si2Mo 钢在 900 ℃ 至 1250 ℃ 温度范围内进行 1800 秒等温保温期间奥氏体晶粒的生长和马氏体相变机制。建立了奥氏体晶粒生长的动态模型,以优化奥氏体化过程的参数。结果表明,奥氏体晶粒大小随温度升高和时间延长而不断增大。Dong 模型预测的晶粒尺寸与实验值非常吻合。奥氏体晶粒通过晶界迁移和晶粒吞并而长大,而 M(Cr,Mo)23C6 的沉淀和溶解则影响晶粒长大。随着时间的延长,一些晶界通过亚晶粒旋转扩展成新的晶界。较低温度下的细晶粒降低了马氏体转变(Ms)的初始温度,初级马氏体沿着先前奥氏体的晶界成核。二次马氏体以一定角度附着在一次马氏体核上,并平行生长,同时抑制周围未转变奥氏体的相变。
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Research on the Austenite Grain Growth Behavior and Martensitic Phase Transformation Mechanism of 40Cr10Si2Mo Steel via In Situ Observation

40Cr10Si2Mo steel is widely utilized because of its excellent mechanical properties, with grain size being a critical factor determining subsequent phase transformation processes and material microstructure performance. This paper reports the use of high-temperature laser scanning confocal microscopy (HT-LSCM) for in situ observation experiments to systematically investigate the growth of austenite grains and the martensitic phase transformation mechanism in 40Cr10Si2Mo steel during an 1800-second isothermal hold at temperatures ranging from 900 °C to 1250 °C. A dynamic model of austenite grain growth is established to optimize the parameters of the austenitic process. The results indicate that the austenite grain size increases continuously with increasing temperature and prolonged time. The Dong model predicts grain sizes that align well with experimental values. Austenite grains grow through grain boundary migration and grain annexation, whereas the precipitation and dissolution of M(Cr, Mo)23C6 affect grain growth. With prolonged time, some grain boundaries extend into new boundaries through subgrain rotation. The fine grains at lower temperatures reduce the initial temperature of the martensite transition (Ms), and the primary martensite nucleates along the grain boundaries of the prior austenite. The secondary martensite is attached to the primary martensite nucleus at a certain angle and grows in parallel while inhibiting the phase transition of the surrounding untransformed austenite.

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