H. S. Srikar, A. Hariharan, K. Manikandan, A. Arul Jeya Kumar
{"title":"用于隐身应用的聚苯胺和氧化石墨烯填充环氧树脂增强石墨-碳板复合材料的机械和电磁吸收研究","authors":"H. S. Srikar, A. Hariharan, K. Manikandan, A. Arul Jeya Kumar","doi":"10.1002/pc.28996","DOIUrl":null,"url":null,"abstract":"<jats:label/>This research focuses on understanding of polymer composites' ability to absorb Radio frequency waves for stealth application, specifically for evading radar detection. The composites were developed using a Carbon‐Graphite base plate layered with carbon fiber mat on both sides reinforced in a polyaniline (PANI) and Graphene oxide (GO) mixed Epoxy matrix with added triethylamine (TEA). Four samples with different volume percentage were fabricated, having same Epoxy of 52%, Hardener of 26% and PANI of 10%, but different volume percentages of GO and TEA. The fabricated composites are named as EPCG‐1 (4% GO and 8% TEA), EPCG‐2 (5% GO and 7% TEA, no Carbon fiber), EPCG‐3 (5% GO and 7% TEA) and EPCG‐4 (7% GO and 5% TEA). The developed composites were characterized by subjecting to tensile testing, Scanning Electron Microscopy analysis, Ultraviolet–visible spectroscopy, Fourier Transform Infrared spectroscopy, Impedance spectroscopy and Directional Coupler test. The EPCG‐4 composites achieve a highest tensile strength of 45.61 N/mm<jats:sup>2</jats:sup> and highest absorbance of 1.574 AU corresponding to a wavelength of 875.00 nanometers. The microwave absorbing capacity was evaluated in terms of absorption, reflection and transmission, where the highest shielding efficiency of 32.76 is observed in EPCG‐4 composite when tested in X‐band frequency range (8–12 GHz). Infrared indicated the stretching of bonds like CN and CH due to addition of graphene oxide. The permittivity of the composite is higher for EPCG‐4 composite. Compared to all the tested composites, EPCG‐4 exhibits better mechanical and stealth properties.Highlights<jats:list list-type=\"bullet\"> <jats:list-item>Development of electromagnetic absorbing composites material for stealth application.</jats:list-item> <jats:list-item>Conductive composites of Graphite‐Carbon plate, layered with Carbon fiber mat bonded by PANI and GO mixed Epoxy matrix are prepared.</jats:list-item> <jats:list-item>Analyzing radio‐frequency absorption, reflection and transmission of the composites using wave guide method.</jats:list-item> <jats:list-item>UV–vis spectroscopy analysis the wave absorbing capacity of stealth composites.</jats:list-item> <jats:list-item>Microscopic analysis on stealth composite to understand the conducting fillers distribution.</jats:list-item> </jats:list>","PeriodicalId":20375,"journal":{"name":"Polymer Composites","volume":"44 1","pages":""},"PeriodicalIF":4.8000,"publicationDate":"2024-09-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Mechanical and electromagnetic absorption study on polyaniline and graphene oxide filled epoxy reinforced with graphite‐carbon plate composites for stealth application\",\"authors\":\"H. S. Srikar, A. Hariharan, K. Manikandan, A. Arul Jeya Kumar\",\"doi\":\"10.1002/pc.28996\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<jats:label/>This research focuses on understanding of polymer composites' ability to absorb Radio frequency waves for stealth application, specifically for evading radar detection. The composites were developed using a Carbon‐Graphite base plate layered with carbon fiber mat on both sides reinforced in a polyaniline (PANI) and Graphene oxide (GO) mixed Epoxy matrix with added triethylamine (TEA). Four samples with different volume percentage were fabricated, having same Epoxy of 52%, Hardener of 26% and PANI of 10%, but different volume percentages of GO and TEA. The fabricated composites are named as EPCG‐1 (4% GO and 8% TEA), EPCG‐2 (5% GO and 7% TEA, no Carbon fiber), EPCG‐3 (5% GO and 7% TEA) and EPCG‐4 (7% GO and 5% TEA). The developed composites were characterized by subjecting to tensile testing, Scanning Electron Microscopy analysis, Ultraviolet–visible spectroscopy, Fourier Transform Infrared spectroscopy, Impedance spectroscopy and Directional Coupler test. The EPCG‐4 composites achieve a highest tensile strength of 45.61 N/mm<jats:sup>2</jats:sup> and highest absorbance of 1.574 AU corresponding to a wavelength of 875.00 nanometers. The microwave absorbing capacity was evaluated in terms of absorption, reflection and transmission, where the highest shielding efficiency of 32.76 is observed in EPCG‐4 composite when tested in X‐band frequency range (8–12 GHz). Infrared indicated the stretching of bonds like CN and CH due to addition of graphene oxide. The permittivity of the composite is higher for EPCG‐4 composite. 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引用次数: 0
摘要
这项研究的重点是了解聚合物复合材料在隐形应用中吸收射频波的能力,特别是躲避雷达探测的能力。复合材料的开发使用了碳-石墨基板,两面分层铺设碳纤维毡,并在添加了三乙胺(TEA)的聚苯胺(PANI)和氧化石墨烯(GO)混合环氧树脂基体中进行加固。我们制作了四种不同体积百分比的样品,其中环氧树脂占 52%,固化剂占 26%,PANI 占 10%,但 GO 和 TEA 的体积百分比各不相同。制成的复合材料被命名为 EPCG-1(4% GO 和 8% TEA)、EPCG-2(5% GO 和 7% TEA,无碳纤维)、EPCG-3(5% GO 和 7% TEA)和 EPCG-4(7% GO 和 5% TEA)。通过拉伸测试、扫描电子显微镜分析、紫外-可见光谱、傅立叶变换红外光谱、阻抗光谱和定向耦合器测试对所开发的复合材料进行了表征。EPCG-4 复合材料的最高拉伸强度为 45.61 牛顿/平方毫米,最高吸收率为 1.574 AU,对应波长为 875.00 纳米。微波吸收能力通过吸收、反射和透射进行评估,在 X 波段频率范围(8-12 GHz)测试中,EPCG-4 复合材料的屏蔽效率最高,达到 32.76。红外线显示,由于添加了氧化石墨烯,CN 和 CH 等键被拉伸。EPCG-4 复合材料的介电常数更高。与所有测试过的复合材料相比,EPCG-4 具有更好的机械性能和隐身性能。制备了由石墨-碳板、层状碳纤维毡以及 PANI 和 GO 混合环氧基质粘合而成的导电复合材料。使用波导法分析复合材料的射频吸收、反射和透射。紫外可见光谱分析隐形复合材料的吸波能力。对隐形复合材料进行显微分析,以了解导电填料的分布情况。
Mechanical and electromagnetic absorption study on polyaniline and graphene oxide filled epoxy reinforced with graphite‐carbon plate composites for stealth application
This research focuses on understanding of polymer composites' ability to absorb Radio frequency waves for stealth application, specifically for evading radar detection. The composites were developed using a Carbon‐Graphite base plate layered with carbon fiber mat on both sides reinforced in a polyaniline (PANI) and Graphene oxide (GO) mixed Epoxy matrix with added triethylamine (TEA). Four samples with different volume percentage were fabricated, having same Epoxy of 52%, Hardener of 26% and PANI of 10%, but different volume percentages of GO and TEA. The fabricated composites are named as EPCG‐1 (4% GO and 8% TEA), EPCG‐2 (5% GO and 7% TEA, no Carbon fiber), EPCG‐3 (5% GO and 7% TEA) and EPCG‐4 (7% GO and 5% TEA). The developed composites were characterized by subjecting to tensile testing, Scanning Electron Microscopy analysis, Ultraviolet–visible spectroscopy, Fourier Transform Infrared spectroscopy, Impedance spectroscopy and Directional Coupler test. The EPCG‐4 composites achieve a highest tensile strength of 45.61 N/mm2 and highest absorbance of 1.574 AU corresponding to a wavelength of 875.00 nanometers. The microwave absorbing capacity was evaluated in terms of absorption, reflection and transmission, where the highest shielding efficiency of 32.76 is observed in EPCG‐4 composite when tested in X‐band frequency range (8–12 GHz). Infrared indicated the stretching of bonds like CN and CH due to addition of graphene oxide. The permittivity of the composite is higher for EPCG‐4 composite. Compared to all the tested composites, EPCG‐4 exhibits better mechanical and stealth properties.HighlightsDevelopment of electromagnetic absorbing composites material for stealth application.Conductive composites of Graphite‐Carbon plate, layered with Carbon fiber mat bonded by PANI and GO mixed Epoxy matrix are prepared.Analyzing radio‐frequency absorption, reflection and transmission of the composites using wave guide method.UV–vis spectroscopy analysis the wave absorbing capacity of stealth composites.Microscopic analysis on stealth composite to understand the conducting fillers distribution.
期刊介绍:
Polymer Composites is the engineering and scientific journal serving the fields of reinforced plastics and polymer composites including research, production, processing, and applications. PC brings you the details of developments in this rapidly expanding area of technology long before they are commercial realities.