Feasibility of ultrasonic non-destructive testing of ancient funerary urns: Experimental and analytical parametric model

Non-invasive modalities are being developed as the computer tools and industrial non-destructive testing capabilities become more widespread. Using the same investigation methods as those applied to modern objects, we seek to study ancient funerary urns containing human bones. The exploration of ancient urns is key to increasing our understanding of the practices of burial and cremation in archaeo-anthropology. But those urns present at archaeological sites are exposed to diversified environments (wet, temperate or dry environment), and can be subjected to chemical or mechanical destructive actions over time. As ancient funeral urns containers are sometimes made of lead, stone or ceramic, the use of X-ray scanners is difficult or even impossible for in situ control. In this work, we propose an engineering technique based on ultrasonic non-destructive testing and wave propagation in urns. An analytical parametric model is developed using mathematical signal processing tools and validated by means of laboratory experiments under controlled conditions of propagation through reproductions of ancient urns for two ultrasonic frequencies (500 kHz and 1 MHz). The aim is to characterise an ancient urn by creating an analytical model, and to use a parametric identification algorithm to determine the presence or absence of bone fragments. The parametric identification algorithm based on the Levenberg–Marquardt method makes it possible to determine the geometrical (thickness) and physical (wave velocity and attenuation, mass density) parameters when the urn is filled with water, with water and bones, and with water, bones and sand. We show that the model makes it readily (processing time $\approx 15$ sec) possible to find the different times of flight between the transducer and the different walls of the urn and the parameters with an accuracy less than 10$\%$.