{"title":"通过激光粉末床熔融技术提高化学制备的纳米钛强化 IN738LC 的高温力学性能和强化机理","authors":"","doi":"10.1016/j.matchar.2024.114434","DOIUrl":null,"url":null,"abstract":"<div><div>Fabrication of high-strength nickel-based composites to meet the demanding service requirements in aerospace environments is a significant challenge. This paper introduces the wet chemical method to prepare the nano-TiC reinforced IN738LC. In contrast to the conventional ball milling approach, this method attains superior attachment of nanoparticles. By employing a full-factorial experimental design, the correlation between Laser-powder bed fusion (L-PBF) processing parameters and the porosity, micro-hardness, and high-temperature tensile strength of as-built samples was examined. The results indicate that the optimal processing parameters are a laser power of 225 W, scanning speed of 750 mm/s, and hatch space of 0.09 mm, with a Volumetric energy density (VED) of 111.1 J/mm<sup>3</sup>. Compared to IN738LC, the chemically prepared TiC-IN738LC exhibits a 45 % increase in room temperature tensile strength (400 MPa) and a 65 % increase in high-temperature tensile strength (120 MPa). Compared with ball-milled TiC-IN738LC, the chemically prepared samples present superior microstructure with more equiaxed grains. The morphological analysis of the tensile samples reveals that the presence of dimples are crucial in enhancing the ductility properties. Furthermore, this study identifies the Orowan strengthening mechanism and the grain refinement strengthening mechanism as the principal mechanisms of reinforcement by nano-ceramics.</div></div>","PeriodicalId":18727,"journal":{"name":"Materials Characterization","volume":null,"pages":null},"PeriodicalIF":4.8000,"publicationDate":"2024-10-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Enhanced high-temperature mechanical properties and strengthening mechanisms of chemically prepared nano-TiC reinforced IN738LC via laser powder bed fusion\",\"authors\":\"\",\"doi\":\"10.1016/j.matchar.2024.114434\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Fabrication of high-strength nickel-based composites to meet the demanding service requirements in aerospace environments is a significant challenge. This paper introduces the wet chemical method to prepare the nano-TiC reinforced IN738LC. In contrast to the conventional ball milling approach, this method attains superior attachment of nanoparticles. By employing a full-factorial experimental design, the correlation between Laser-powder bed fusion (L-PBF) processing parameters and the porosity, micro-hardness, and high-temperature tensile strength of as-built samples was examined. The results indicate that the optimal processing parameters are a laser power of 225 W, scanning speed of 750 mm/s, and hatch space of 0.09 mm, with a Volumetric energy density (VED) of 111.1 J/mm<sup>3</sup>. Compared to IN738LC, the chemically prepared TiC-IN738LC exhibits a 45 % increase in room temperature tensile strength (400 MPa) and a 65 % increase in high-temperature tensile strength (120 MPa). Compared with ball-milled TiC-IN738LC, the chemically prepared samples present superior microstructure with more equiaxed grains. The morphological analysis of the tensile samples reveals that the presence of dimples are crucial in enhancing the ductility properties. Furthermore, this study identifies the Orowan strengthening mechanism and the grain refinement strengthening mechanism as the principal mechanisms of reinforcement by nano-ceramics.</div></div>\",\"PeriodicalId\":18727,\"journal\":{\"name\":\"Materials Characterization\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":4.8000,\"publicationDate\":\"2024-10-04\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Characterization\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1044580324008155\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, CHARACTERIZATION & TESTING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Characterization","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1044580324008155","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, CHARACTERIZATION & TESTING","Score":null,"Total":0}
Enhanced high-temperature mechanical properties and strengthening mechanisms of chemically prepared nano-TiC reinforced IN738LC via laser powder bed fusion
Fabrication of high-strength nickel-based composites to meet the demanding service requirements in aerospace environments is a significant challenge. This paper introduces the wet chemical method to prepare the nano-TiC reinforced IN738LC. In contrast to the conventional ball milling approach, this method attains superior attachment of nanoparticles. By employing a full-factorial experimental design, the correlation between Laser-powder bed fusion (L-PBF) processing parameters and the porosity, micro-hardness, and high-temperature tensile strength of as-built samples was examined. The results indicate that the optimal processing parameters are a laser power of 225 W, scanning speed of 750 mm/s, and hatch space of 0.09 mm, with a Volumetric energy density (VED) of 111.1 J/mm3. Compared to IN738LC, the chemically prepared TiC-IN738LC exhibits a 45 % increase in room temperature tensile strength (400 MPa) and a 65 % increase in high-temperature tensile strength (120 MPa). Compared with ball-milled TiC-IN738LC, the chemically prepared samples present superior microstructure with more equiaxed grains. The morphological analysis of the tensile samples reveals that the presence of dimples are crucial in enhancing the ductility properties. Furthermore, this study identifies the Orowan strengthening mechanism and the grain refinement strengthening mechanism as the principal mechanisms of reinforcement by nano-ceramics.
期刊介绍:
Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials.
The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal.
The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include:
Metals & Alloys
Ceramics
Nanomaterials
Biomedical materials
Optical materials
Composites
Natural Materials.