{"title":"利用分子印迹聚合物开发检测受污染食品和饲料中伏马菌素的先进分析程序:微型综述","authors":"M.A. Diab , Heba A. El-Sabban , Kwang-Hyun Baek","doi":"10.1016/j.microc.2024.111858","DOIUrl":null,"url":null,"abstract":"<div><div>Fumonisins (FMS), a class of Mycotoxins mostly produced by fusarium species, are found in polluted food and feed and can seriously harm humans and animals. To ensure food safety and regulatory compliance, accurate and dependable analytical techniques are utilized in detecting and measuring these pollutants. This mini-review focused on sophisticated clean-up techniques for Fumonisin (FM) analysis utilizing molecularly imprinted polymer solid phase extraction (MIPSPE). The majority of the molecularly imprinted polymers (MIPs) categories that are intended to extract FMs from the food matrix were discussed, along with a list of well-known chromatographic techniques and MIP-based electrochemical sensors to detect FMs<strong>.</strong></div><div>By imitating FM-specific natural sites, MIPSPE provides great selectivity, sensitivity, and reproducibility while improving the accuracy of subsequent analytical tests. This review includes the synthesis of MIPs, extraction protocol optimization, and integration with several detection techniques like High-Performance Liquid Chromatography <strong>(</strong>HPLC) and Liquid Chromatography-Mass Spectroscopy (LC-MS). It also covers recent advancements in MIPSPE technology.</div></div>","PeriodicalId":391,"journal":{"name":"Microchemical Journal","volume":"207 ","pages":"Article 111858"},"PeriodicalIF":4.9000,"publicationDate":"2024-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Toward advanced analytical procedures for detecting Fumonisins in contaminated food and feed using molecularly imprinted polymers: A mini review\",\"authors\":\"M.A. Diab , Heba A. El-Sabban , Kwang-Hyun Baek\",\"doi\":\"10.1016/j.microc.2024.111858\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Fumonisins (FMS), a class of Mycotoxins mostly produced by fusarium species, are found in polluted food and feed and can seriously harm humans and animals. To ensure food safety and regulatory compliance, accurate and dependable analytical techniques are utilized in detecting and measuring these pollutants. This mini-review focused on sophisticated clean-up techniques for Fumonisin (FM) analysis utilizing molecularly imprinted polymer solid phase extraction (MIPSPE). The majority of the molecularly imprinted polymers (MIPs) categories that are intended to extract FMs from the food matrix were discussed, along with a list of well-known chromatographic techniques and MIP-based electrochemical sensors to detect FMs<strong>.</strong></div><div>By imitating FM-specific natural sites, MIPSPE provides great selectivity, sensitivity, and reproducibility while improving the accuracy of subsequent analytical tests. This review includes the synthesis of MIPs, extraction protocol optimization, and integration with several detection techniques like High-Performance Liquid Chromatography <strong>(</strong>HPLC) and Liquid Chromatography-Mass Spectroscopy (LC-MS). It also covers recent advancements in MIPSPE technology.</div></div>\",\"PeriodicalId\":391,\"journal\":{\"name\":\"Microchemical Journal\",\"volume\":\"207 \",\"pages\":\"Article 111858\"},\"PeriodicalIF\":4.9000,\"publicationDate\":\"2024-10-10\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Microchemical Journal\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0026265X24019702\",\"RegionNum\":2,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"CHEMISTRY, ANALYTICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Microchemical Journal","FirstCategoryId":"92","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0026265X24019702","RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"CHEMISTRY, ANALYTICAL","Score":null,"Total":0}
Toward advanced analytical procedures for detecting Fumonisins in contaminated food and feed using molecularly imprinted polymers: A mini review
Fumonisins (FMS), a class of Mycotoxins mostly produced by fusarium species, are found in polluted food and feed and can seriously harm humans and animals. To ensure food safety and regulatory compliance, accurate and dependable analytical techniques are utilized in detecting and measuring these pollutants. This mini-review focused on sophisticated clean-up techniques for Fumonisin (FM) analysis utilizing molecularly imprinted polymer solid phase extraction (MIPSPE). The majority of the molecularly imprinted polymers (MIPs) categories that are intended to extract FMs from the food matrix were discussed, along with a list of well-known chromatographic techniques and MIP-based electrochemical sensors to detect FMs.
By imitating FM-specific natural sites, MIPSPE provides great selectivity, sensitivity, and reproducibility while improving the accuracy of subsequent analytical tests. This review includes the synthesis of MIPs, extraction protocol optimization, and integration with several detection techniques like High-Performance Liquid Chromatography (HPLC) and Liquid Chromatography-Mass Spectroscopy (LC-MS). It also covers recent advancements in MIPSPE technology.
期刊介绍:
The Microchemical Journal is a peer reviewed journal devoted to all aspects and phases of analytical chemistry and chemical analysis. The Microchemical Journal publishes articles which are at the forefront of modern analytical chemistry and cover innovations in the techniques to the finest possible limits. This includes fundamental aspects, instrumentation, new developments, innovative and novel methods and applications including environmental and clinical field.
Traditional classical analytical methods such as spectrophotometry and titrimetry as well as established instrumentation methods such as flame and graphite furnace atomic absorption spectrometry, gas chromatography, and modified glassy or carbon electrode electrochemical methods will be considered, provided they show significant improvements and novelty compared to the established methods.