短玻璃纤维增强聚醚醚酮 (PEEK) 的超高循环疲劳特性

IF 5.7 2区 材料科学 Q1 ENGINEERING, MECHANICAL International Journal of Fatigue Pub Date : 2024-10-14 DOI:10.1016/j.ijfatigue.2024.108652
Michael Fitzka , Gabriel Stadler , Bernd M. Schönbauer , Gerald Pinter , Herwig Mayer
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引用次数: 0

摘要

研究了 14 wt-% 短玻璃纤维增强聚醚醚酮(PEEK-GF14)在高循环和超高循环疲劳(VHCF)状态下的疲劳特性。实验采用伺服液压和电动设备,循环频率为 10-20 Hz,超声波设备的循环频率为 19 kHz,载荷比为-1。已开发出一种新的试样几何形状,可在高应力幅值下进行超声波测试。两个测试系列都采用了相同的试样形状,以排除尺寸影响,从而重点研究循环频率和测试技术的影响。间歇加载的超声疲劳测试可避免试样加热。在 10-20 Hz 和 19 kHz 下测量的 S-N 曲线显示出相似的斜率指数(即 10 % 的偏差)。使用超声波设备测定的平均 S-N 曲线向稍低的应力振幅移动,这可能是由于统计散差造成的。PEEK-GF14 没有显示出疲劳极限,在超过 109 次循环后仍会出现故障。与未增强的 PEEK 相比,PEEK-GF14 的 VHCF 强度大约高出两倍。断裂研究显示纤维断裂,纤维拉出的情况较少。
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Very high cycle fatigue properties of short glass fiber reinforced polyetheretherketone (PEEK)
The fatigue properties of 14 wt-% short glass fiber reinforced polyetheretherketone (PEEK–GF14) have been investigated in the high and very high cycle fatigue (VHCF) regime. Experiments were performed at a load ratio of –1 with servohydraulic and electrodynamic equipment at cycling frequency 10–20 Hz, and with ultrasonic equipment at 19 kHz. A new specimen geometry has been developed that allows ultrasonic tests up to high stress amplitudes. The same specimen shape was used in both testing series to exclude size effects, which enabled to focus on the influence of cycling frequency and testing technique. Ultrasonic fatigue testing with intermittent loading served to avoid heating of specimens. The S-N curves measured at 10–20 Hz and 19 kHz show a similar slope exponent (i.e., 10 % deviation). Mean S-N curve determined with ultrasonic equipment is shifted to slightly lower stress amplitudes, which may be attributed to statistical scatter. PEEK–GF14 does not show a fatigue limit and failures still occurred above 109 cycles. The VHCF strength of PEEK-GF14 is approximately two times higher compared with unreinforced PEEK. Fractographic investigations revealed fiber fracture and, less frequently, fiber pull-out.
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来源期刊
International Journal of Fatigue
International Journal of Fatigue 工程技术-材料科学:综合
CiteScore
10.70
自引率
21.70%
发文量
619
审稿时长
58 days
期刊介绍: Typical subjects discussed in International Journal of Fatigue address: Novel fatigue testing and characterization methods (new kinds of fatigue tests, critical evaluation of existing methods, in situ measurement of fatigue degradation, non-contact field measurements) Multiaxial fatigue and complex loading effects of materials and structures, exploring state-of-the-art concepts in degradation under cyclic loading Fatigue in the very high cycle regime, including failure mode transitions from surface to subsurface, effects of surface treatment, processing, and loading conditions Modeling (including degradation processes and related driving forces, multiscale/multi-resolution methods, computational hierarchical and concurrent methods for coupled component and material responses, novel methods for notch root analysis, fracture mechanics, damage mechanics, crack growth kinetics, life prediction and durability, and prediction of stochastic fatigue behavior reflecting microstructure and service conditions) Models for early stages of fatigue crack formation and growth that explicitly consider microstructure and relevant materials science aspects Understanding the influence or manufacturing and processing route on fatigue degradation, and embedding this understanding in more predictive schemes for mitigation and design against fatigue Prognosis and damage state awareness (including sensors, monitoring, methodology, interactive control, accelerated methods, data interpretation) Applications of technologies associated with fatigue and their implications for structural integrity and reliability. This includes issues related to design, operation and maintenance, i.e., life cycle engineering Smart materials and structures that can sense and mitigate fatigue degradation Fatigue of devices and structures at small scales, including effects of process route and surfaces/interfaces.
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