机械合金化 Al-Mn-Cu 合金的强化特性

IF 0.8 4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Metallurgist Pub Date : 2024-10-15 DOI:10.1007/s11015-024-01773-8
O. A. Yakovtseva, A. G. Mochugovskii, N. B. Emelina, E. N. Zanaeva, A. S. Prosviryakov, A. V. Mikhaylovskaya
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引用次数: 0

摘要

在 250-450 °C 的温度范围内进行退火,并在 400-450 °C 的温度范围内进行压实后,对 Al-7.7Mn-3.1Cu (wt.%) 合金机械合金颗粒的结构和机械性能进行了研究。结果表明,球磨 10 小时可形成铝基过饱和固溶体和 Al6Mn 相。X 射线结构数据和差热分析以及颗粒硬度变化的比较表明,在加热过程中发生了再结晶过程和过饱和固溶体的分解,并析出了 Al6Mn 和 CuAl2 相。在 400 °C 下压制颗粒,样品密度为 2.87 g/sm3,显微硬度为 310±16 HV。在 400-450 °C 下获得的压实物退火后,密度和强度都有所提高。450 °C 下的压实使材料密度增至 3.01 g/sm3,压缩试验结果表明其具有更好的机械性能。该合金的屈服强度为 910±10 兆帕,极限拉伸强度为 1060±20 兆帕,室温下的失效变形率为 0.9%,在 350 °C 下压缩 40% 后的屈服强度平均值为 287±20 兆帕,且无微失效。
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Strenghthening features of mechanically alloyed Al-Mn-Cu alloy

Structure and mechanical property of mechanically alloyed granules of the Al–7.7Mn–3.1Cu (wt.%) alloy are studied after annealing in the temperature range of 250–450 °C and compaction at 400–450 °C. It is shown that a ball milling for 10 h provides for a formation of aluminum based supersaturated solid solution and Al6Mn phase. Comparison of X‑ray structural data and differential thermal analysis and the change in granule hardness demonstrates the occurrence of recrystallization processes and decomposition of supersaturated solid solution with precipitation of Al6Mn and CuAl2 phases at heating. Compaction of granules at 400 °C provides a sample’s density of 2.87 g/sm3 and microhardness of 310±16 HV. Annealing of the compacts obtained at 400–450 °C leads to an increase in density and strength. Compaction at 450 °C increases the density of material to 3.01 g/sm3 and provides better mechanical properties according to compression tests results. The alloy exhibits yield strength of 910±10 MPa, ultimate tensile strength of 1060±20 MPa, deformation to failure of 0.9% at room temperature and an average value of yield strength of 287±20 MPa without microfailures after 40% of compression at 350 °C.

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来源期刊
Metallurgist
Metallurgist 工程技术-冶金工程
CiteScore
1.50
自引率
44.40%
发文量
151
审稿时长
4-8 weeks
期刊介绍: Metallurgist is the leading Russian journal in metallurgy. Publication started in 1956. Basic topics covered include: State of the art and development of enterprises in ferrous and nonferrous metallurgy and mining; Metallurgy of ferrous, nonferrous, rare, and precious metals; Metallurgical equipment; Automation and control; Protection of labor; Protection of the environment; Resources and energy saving; Quality and certification; History of metallurgy; Inventions (patents).
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