Isabel del Hierro , Francisco Reyes-Téllez , Raquel Herrera , Javier Lillo , Josefa Ortiz-Bustos , Yolanda Pérez-Cortes , Alberto Polo-Romero , Gonzalo Viñuales-Ferreiro
{"title":"分析马甘(西班牙托莱多)历史建筑中的石灰砂浆:矿物学和烧制温度的启示","authors":"Isabel del Hierro , Francisco Reyes-Téllez , Raquel Herrera , Javier Lillo , Josefa Ortiz-Bustos , Yolanda Pérez-Cortes , Alberto Polo-Romero , Gonzalo Viñuales-Ferreiro","doi":"10.1016/j.jasrep.2024.104812","DOIUrl":null,"url":null,"abstract":"<div><div>Mortar samples from the remains of a nearly vanished structure in the village of Magán (Toledo, Spain) have been investigated. Their mineralogical and chemical composition have been analyzed to understand the building technology of their historical period and the functionality of the original structure. Furthermore, a wide range of characterization techniques has been employed in the investigation regarding the amount of information they can provide and assess their effectiveness in the field. Chemical characterization of the mortar samples has been performed by XRD and XRF and completed with TGA studies. FTIR and Raman Spectroscopy, together with <sup>28</sup>Si and <sup>27</sup>Al-MAS-NMR and Microscopy Studies complete these characterization studies. Although the samples possess similar composition, since the predominant mineralogy is quartz, feldspars, and phyllosilicates, the differences discovered let us establish a relationship between chemical data and petrographic mineralogical data, and the source of materials.</div></div>","PeriodicalId":48150,"journal":{"name":"Journal of Archaeological Science-Reports","volume":null,"pages":null},"PeriodicalIF":1.5000,"publicationDate":"2024-10-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Analyzing lime mortars from a historic construction in Magán (Toledo, Spain): Insights into mineralogy and firing temperatures\",\"authors\":\"Isabel del Hierro , Francisco Reyes-Téllez , Raquel Herrera , Javier Lillo , Josefa Ortiz-Bustos , Yolanda Pérez-Cortes , Alberto Polo-Romero , Gonzalo Viñuales-Ferreiro\",\"doi\":\"10.1016/j.jasrep.2024.104812\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>Mortar samples from the remains of a nearly vanished structure in the village of Magán (Toledo, Spain) have been investigated. Their mineralogical and chemical composition have been analyzed to understand the building technology of their historical period and the functionality of the original structure. Furthermore, a wide range of characterization techniques has been employed in the investigation regarding the amount of information they can provide and assess their effectiveness in the field. Chemical characterization of the mortar samples has been performed by XRD and XRF and completed with TGA studies. FTIR and Raman Spectroscopy, together with <sup>28</sup>Si and <sup>27</sup>Al-MAS-NMR and Microscopy Studies complete these characterization studies. Although the samples possess similar composition, since the predominant mineralogy is quartz, feldspars, and phyllosilicates, the differences discovered let us establish a relationship between chemical data and petrographic mineralogical data, and the source of materials.</div></div>\",\"PeriodicalId\":48150,\"journal\":{\"name\":\"Journal of Archaeological Science-Reports\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":1.5000,\"publicationDate\":\"2024-10-19\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Archaeological Science-Reports\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2352409X24004401\",\"RegionNum\":2,\"RegionCategory\":\"历史学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"0\",\"JCRName\":\"ARCHAEOLOGY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Archaeological Science-Reports","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2352409X24004401","RegionNum":2,"RegionCategory":"历史学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"0","JCRName":"ARCHAEOLOGY","Score":null,"Total":0}
Analyzing lime mortars from a historic construction in Magán (Toledo, Spain): Insights into mineralogy and firing temperatures
Mortar samples from the remains of a nearly vanished structure in the village of Magán (Toledo, Spain) have been investigated. Their mineralogical and chemical composition have been analyzed to understand the building technology of their historical period and the functionality of the original structure. Furthermore, a wide range of characterization techniques has been employed in the investigation regarding the amount of information they can provide and assess their effectiveness in the field. Chemical characterization of the mortar samples has been performed by XRD and XRF and completed with TGA studies. FTIR and Raman Spectroscopy, together with 28Si and 27Al-MAS-NMR and Microscopy Studies complete these characterization studies. Although the samples possess similar composition, since the predominant mineralogy is quartz, feldspars, and phyllosilicates, the differences discovered let us establish a relationship between chemical data and petrographic mineralogical data, and the source of materials.
期刊介绍:
Journal of Archaeological Science: Reports is aimed at archaeologists and scientists engaged with the application of scientific techniques and methodologies to all areas of archaeology. The journal focuses on the results of the application of scientific methods to archaeological problems and debates. It will provide a forum for reviews and scientific debate of issues in scientific archaeology and their impact in the wider subject. Journal of Archaeological Science: Reports will publish papers of excellent archaeological science, with regional or wider interest. This will include case studies, reviews and short papers where an established scientific technique sheds light on archaeological questions and debates.