{"title":"非热等离子体处理和 MXene (Ti3C2TX)/WO3 涂层棉织物的抗菌和伤口愈合活性","authors":"Udaya Vaka, M.C. Ramkumar","doi":"10.1016/j.matchemphys.2024.130072","DOIUrl":null,"url":null,"abstract":"<div><div>In this study, MXene (Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>)/WO<sub>3</sub> nanocomposite was directly deposited on the surface of non-thermal plasma treated cotton fabrics. Initially, argon was used as a plasma forming gas to treat the surface of cotton fabrics. Subsequently, the MXene (Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>)/WO<sub>3</sub> nanocomposite was deposited on the surface of non-thermal plasma treated cotton fabrics by co-precipitation method. As prepared cotton fabrics were characterized by various characterization techniques that includes, X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, Field emission scanning electron microscopy (FESEM) with energy-dispersive X-ray (EDX) analysis, and Contact Angle (CA) measurement. SEM and FTIR analysis confirmed the presence of MXene (Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>)/WO<sub>3</sub> nanocomposite on the surface of cotton fabrics. In addition, contact angle analysis unveiled the super hydrophilic nature of cotton fabrics after surface modification. The antibacterial activity and the wound healing assay of the untreated and surface modified cotton fabrics were examined by <em>in vitro</em> analysis. Results unveiled that the surface modified cotton fabrics showed excellent antibacterial activity against gram-negative bacteria (<em>Escherichia coli</em>) and gram-positive bacteria (<em>Staphylococcus aureus</em>) and substantial wound healing activity. From this investigation it is inferred that plasma treated and nanocomposite functionalised cotton fabrics have the potential to be employed as wound dressing material.</div></div>","PeriodicalId":18227,"journal":{"name":"Materials Chemistry and Physics","volume":"329 ","pages":"Article 130072"},"PeriodicalIF":4.3000,"publicationDate":"2024-10-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Antibacterial and wound healing activity of non-thermal plasma treated and MXene (Ti3C2TX)/ WO3 coated cotton fabrics\",\"authors\":\"Udaya Vaka, M.C. Ramkumar\",\"doi\":\"10.1016/j.matchemphys.2024.130072\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>In this study, MXene (Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>)/WO<sub>3</sub> nanocomposite was directly deposited on the surface of non-thermal plasma treated cotton fabrics. Initially, argon was used as a plasma forming gas to treat the surface of cotton fabrics. Subsequently, the MXene (Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>)/WO<sub>3</sub> nanocomposite was deposited on the surface of non-thermal plasma treated cotton fabrics by co-precipitation method. As prepared cotton fabrics were characterized by various characterization techniques that includes, X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, Field emission scanning electron microscopy (FESEM) with energy-dispersive X-ray (EDX) analysis, and Contact Angle (CA) measurement. SEM and FTIR analysis confirmed the presence of MXene (Ti<sub>3</sub>C<sub>2</sub>T<sub>x</sub>)/WO<sub>3</sub> nanocomposite on the surface of cotton fabrics. In addition, contact angle analysis unveiled the super hydrophilic nature of cotton fabrics after surface modification. The antibacterial activity and the wound healing assay of the untreated and surface modified cotton fabrics were examined by <em>in vitro</em> analysis. Results unveiled that the surface modified cotton fabrics showed excellent antibacterial activity against gram-negative bacteria (<em>Escherichia coli</em>) and gram-positive bacteria (<em>Staphylococcus aureus</em>) and substantial wound healing activity. From this investigation it is inferred that plasma treated and nanocomposite functionalised cotton fabrics have the potential to be employed as wound dressing material.</div></div>\",\"PeriodicalId\":18227,\"journal\":{\"name\":\"Materials Chemistry and Physics\",\"volume\":\"329 \",\"pages\":\"Article 130072\"},\"PeriodicalIF\":4.3000,\"publicationDate\":\"2024-10-19\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Chemistry and Physics\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0254058424012008\",\"RegionNum\":3,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Chemistry and Physics","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0254058424012008","RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
摘要
在这项研究中,MXene(Ti3C2Tx)/WO3 纳米复合材料被直接沉积在经过非热等离子体处理的棉织物表面。首先,使用氩气作为等离子体形成气体来处理棉织物表面。随后,通过共沉淀法将 MXene(Ti3C2Tx)/WO3 纳米复合材料沉积在经过非热等离子体处理的棉织物表面。对制备的棉织物采用了多种表征技术,包括 X 射线衍射 (XRD)、傅立叶变换红外光谱 (FTIR)、场发射扫描电子显微镜 (FESEM) 和能量色散 X 射线 (EDX) 分析以及接触角 (CA) 测量。扫描电子显微镜和傅立叶变换红外光谱分析证实了棉织物表面存在 MXene(Ti3C2Tx)/WO3 纳米复合材料。此外,接触角分析揭示了棉织物表面改性后的超亲水性。体外分析检验了未处理棉织物和表面改性棉织物的抗菌活性和伤口愈合试验。结果表明,表面改性棉织物对革兰氏阴性菌(大肠杆菌)和革兰氏阳性菌(金黄色葡萄球菌)具有极佳的抗菌活性,并具有显著的伤口愈合活性。这项研究推断,经过等离子处理和纳米复合功能化的棉织物有望用作伤口敷料。
Antibacterial and wound healing activity of non-thermal plasma treated and MXene (Ti3C2TX)/ WO3 coated cotton fabrics
In this study, MXene (Ti3C2Tx)/WO3 nanocomposite was directly deposited on the surface of non-thermal plasma treated cotton fabrics. Initially, argon was used as a plasma forming gas to treat the surface of cotton fabrics. Subsequently, the MXene (Ti3C2Tx)/WO3 nanocomposite was deposited on the surface of non-thermal plasma treated cotton fabrics by co-precipitation method. As prepared cotton fabrics were characterized by various characterization techniques that includes, X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, Field emission scanning electron microscopy (FESEM) with energy-dispersive X-ray (EDX) analysis, and Contact Angle (CA) measurement. SEM and FTIR analysis confirmed the presence of MXene (Ti3C2Tx)/WO3 nanocomposite on the surface of cotton fabrics. In addition, contact angle analysis unveiled the super hydrophilic nature of cotton fabrics after surface modification. The antibacterial activity and the wound healing assay of the untreated and surface modified cotton fabrics were examined by in vitro analysis. Results unveiled that the surface modified cotton fabrics showed excellent antibacterial activity against gram-negative bacteria (Escherichia coli) and gram-positive bacteria (Staphylococcus aureus) and substantial wound healing activity. From this investigation it is inferred that plasma treated and nanocomposite functionalised cotton fabrics have the potential to be employed as wound dressing material.
期刊介绍:
Materials Chemistry and Physics is devoted to short communications, full-length research papers and feature articles on interrelationships among structure, properties, processing and performance of materials. The Editors welcome manuscripts on thin films, surface and interface science, materials degradation and reliability, metallurgy, semiconductors and optoelectronic materials, fine ceramics, magnetics, superconductors, specialty polymers, nano-materials and composite materials.