Michael Berg, Dirk Furrer, Vincent Thominet, Xiaoqiang Wang, Stefan Zeugin, Helmut Grabner, Kurt Stockinger, Cinthia Piamonteze
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引用次数: 0
摘要
软 X 射线光谱学是测量材料基本特性的重要技术。然而,对于亚毫米范围的样品测量,许多实验装置都存在局限性。在系统热稳定过程中,数百微米量级的位置漂移可能会持续数小时昂贵的光束时间。为了补偿漂移,必须使用样品跟踪和反馈系统。然而,在复杂的样品环境中,样品存取非常有限,许多现有的解决方案都无法应用。在这项工作中,我们采用了一种稳健的计算机视觉算法,在数十微米的范围内自动跟踪和重新调整样品位置。我们的方法适用于复杂的样品环境,样品位于超高真空室中,周围有冷却热屏蔽,样品温度可低至 2.5 K,并位于超导分裂线圈的中心。我们的实施方案允许在垂直方向上对样品位置进行跟踪和调整,因为在我们的设置中,样品温度变化时会在这一维度上发生漂移。这种方法可以很容易地扩展到二维。该算法可将垂直尺寸小至 70 微米的样品中一系列 X 射线吸收光谱的重叠提高 10 倍。该解决方案可用于各种实验站,在这些实验站中,光学通道可用,而通过其他方式获取样品的机会较少。
distect: automatic sample-position tracking for X-ray experiments using computer vision algorithms.
Soft X-ray spectroscopy is an important technique for measuring the fundamental properties of materials. However, for measurements of samples in the sub-millimetre range, many experimental setups show limitations. Position drifts on the order of hundreds of micrometres during thermal stabilization of the system can last for hours of expensive beam time. To compensate for drifts, sample tracking and feedback systems must be used. However, in complex sample environments where sample access is very limited, many existing solutions cannot be applied. In this work, we apply a robust computer vision algorithm to automatically track and readjust the sample position in the dozens of micrometres range. Our approach is applied in a complex sample environment, where the sample is in an ultra-high vacuum chamber, surrounded by cooled thermal shields to reach sample temperatures down to 2.5 K and in the center of a superconducting split coil. Our implementation allows sample-position tracking and adjustment in the vertical direction since this is the dimension where drifts occur during sample temperature change in our setup. The approach can be easily extended to 2D. The algorithm enables a factor of ten improvement in the overlap of a series of X-ray absorption spectra in a sample with a vertical size down to 70 µm. This solution can be used in a variety of experimental stations, where optical access is available and sample access by other means is reduced.
期刊介绍:
Synchrotron radiation research is rapidly expanding with many new sources of radiation being created globally. Synchrotron radiation plays a leading role in pure science and in emerging technologies. The Journal of Synchrotron Radiation provides comprehensive coverage of the entire field of synchrotron radiation and free-electron laser research including instrumentation, theory, computing and scientific applications in areas such as biology, nanoscience and materials science. Rapid publication ensures an up-to-date information resource for scientists and engineers in the field.