利用 GC-MS 和 MOS 电子鼻分析生姜(Zingiber officinale)在远红外结合热风干燥过程中的挥发性化合物

IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Journal of Food Measurement and Characterization Pub Date : 2024-10-04 DOI:10.1007/s11694-024-02843-w
Yongsheng Pei, Changzhi Wang, Lin Fan, Guizhong Tian, Shiyuan Miao, Xiangyi Meng, Zhenfeng Li, Wanxiu Xu
{"title":"利用 GC-MS 和 MOS 电子鼻分析生姜(Zingiber officinale)在远红外结合热风干燥过程中的挥发性化合物","authors":"Yongsheng Pei,&nbsp;Changzhi Wang,&nbsp;Lin Fan,&nbsp;Guizhong Tian,&nbsp;Shiyuan Miao,&nbsp;Xiangyi Meng,&nbsp;Zhenfeng Li,&nbsp;Wanxiu Xu","doi":"10.1007/s11694-024-02843-w","DOIUrl":null,"url":null,"abstract":"<div><p>In this study, ginger slices were dehydrated through a combination of far-infrared radiation and hot-air drying (FIR-HAD). The changes in volatile composition were subsequently identified using gas chromatography-mass spectrometry (GC-MS) and metal oxide semiconductor electronic nose (MOS e-nose). The GC-MS analysis revealed that terpenes comprised over 75% of volatile compounds in all examined samples, with zingiberene, <i>β</i>-sesquiphellandrene, and (<i>E</i>, <i>E</i>)-α-farnesene being the dominant constituents. Fresh ginger contained a higher relative proportion compared to dried samples. After FIR-HAD treatment, the terpene levels decreased by 11.9%, 8.9%, 13.7%, and 18.2% at 50 °C, 60 °C, 70 °C, and 80 °C, respectively. Among the various drying conditions, ginger subjected to FIR-HAD at 60 °C displayed the highest concentrations of volatile compounds and exhibited flavor characteristics closest to those of fresh samples. The flavor profiles were further evaluated using MOS e-nose analysis. The terpene compounds demonstrated a strong correlation with the response values of W1W and W2W sensors according to partial least squares regression models. In addition, the concentrations of 6-gingerol, 8-gingerol, and 10-gingerol in ginger exposed to FIR-HAD at 60 °C were also higher compared to other drying conditions. This indicated that the FIR-HAD at 60 °C is more suitable for producing dried ginger with remaining flavor attributes. These findings offer theoretical insights into the changes in volatile compounds of ginger slices during the FIR-HAD procedure. They also highlight the potential for improving drying efficiency through aroma online control techniques in future research.</p></div>","PeriodicalId":631,"journal":{"name":"Journal of Food Measurement and Characterization","volume":"18 11","pages":"8944 - 8959"},"PeriodicalIF":2.9000,"publicationDate":"2024-10-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Analysis of volatile compounds of ginger (Zingiber officinale) during far-infrared combined with hot-air drying by GC-MS and MOS e-nose\",\"authors\":\"Yongsheng Pei,&nbsp;Changzhi Wang,&nbsp;Lin Fan,&nbsp;Guizhong Tian,&nbsp;Shiyuan Miao,&nbsp;Xiangyi Meng,&nbsp;Zhenfeng Li,&nbsp;Wanxiu Xu\",\"doi\":\"10.1007/s11694-024-02843-w\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>In this study, ginger slices were dehydrated through a combination of far-infrared radiation and hot-air drying (FIR-HAD). The changes in volatile composition were subsequently identified using gas chromatography-mass spectrometry (GC-MS) and metal oxide semiconductor electronic nose (MOS e-nose). The GC-MS analysis revealed that terpenes comprised over 75% of volatile compounds in all examined samples, with zingiberene, <i>β</i>-sesquiphellandrene, and (<i>E</i>, <i>E</i>)-α-farnesene being the dominant constituents. Fresh ginger contained a higher relative proportion compared to dried samples. After FIR-HAD treatment, the terpene levels decreased by 11.9%, 8.9%, 13.7%, and 18.2% at 50 °C, 60 °C, 70 °C, and 80 °C, respectively. Among the various drying conditions, ginger subjected to FIR-HAD at 60 °C displayed the highest concentrations of volatile compounds and exhibited flavor characteristics closest to those of fresh samples. The flavor profiles were further evaluated using MOS e-nose analysis. The terpene compounds demonstrated a strong correlation with the response values of W1W and W2W sensors according to partial least squares regression models. In addition, the concentrations of 6-gingerol, 8-gingerol, and 10-gingerol in ginger exposed to FIR-HAD at 60 °C were also higher compared to other drying conditions. This indicated that the FIR-HAD at 60 °C is more suitable for producing dried ginger with remaining flavor attributes. These findings offer theoretical insights into the changes in volatile compounds of ginger slices during the FIR-HAD procedure. They also highlight the potential for improving drying efficiency through aroma online control techniques in future research.</p></div>\",\"PeriodicalId\":631,\"journal\":{\"name\":\"Journal of Food Measurement and Characterization\",\"volume\":\"18 11\",\"pages\":\"8944 - 8959\"},\"PeriodicalIF\":2.9000,\"publicationDate\":\"2024-10-04\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Food Measurement and Characterization\",\"FirstCategoryId\":\"97\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s11694-024-02843-w\",\"RegionNum\":3,\"RegionCategory\":\"农林科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"FOOD SCIENCE & TECHNOLOGY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Food Measurement and Characterization","FirstCategoryId":"97","ListUrlMain":"https://link.springer.com/article/10.1007/s11694-024-02843-w","RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"FOOD SCIENCE & TECHNOLOGY","Score":null,"Total":0}
引用次数: 0

摘要

在这项研究中,生姜片通过远红外辐射和热风干燥(FIR-HAD)相结合的方法进行脱水。随后使用气相色谱-质谱联用仪(GC-MS)和金属氧化物半导体电子鼻(MOS e-nose)对挥发性成分的变化进行了鉴定。气相色谱-质谱分析表明,在所有检测样品中,萜烯类化合物占挥发性化合物的 75% 以上,其中最主要的成分是辛夷烯、β-鞘氨醇和(E,E)-α-法呢烯。与干燥样品相比,新鲜生姜中的相对比例更高。经过 FIR-HAD 处理后,萜烯含量在 50 ℃、60 ℃、70 ℃ 和 80 ℃ 下分别降低了 11.9%、8.9%、13.7% 和 18.2%。在不同的干燥条件下,60 °C的FIR-HAD条件下生姜的挥发性化合物浓度最高,风味特征最接近新鲜样品。使用 MOS 电子鼻分析法对风味特征进行了进一步评估。根据偏最小二乘法回归模型,萜烯化合物与 W1W 和 W2W 传感器的响应值有很强的相关性。此外,与其他干燥条件相比,在 60 °C的FIR-HAD条件下,生姜中6-姜酚、8-姜酚和10-姜酚的浓度也更高。这表明,60 °C下的FIR-HAD更适于生产具有其余风味特性的干姜。这些发现从理论上揭示了 FIR-HAD 过程中生姜片挥发性化合物的变化。它们还强调了在未来研究中通过香气在线控制技术提高干燥效率的潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Analysis of volatile compounds of ginger (Zingiber officinale) during far-infrared combined with hot-air drying by GC-MS and MOS e-nose

In this study, ginger slices were dehydrated through a combination of far-infrared radiation and hot-air drying (FIR-HAD). The changes in volatile composition were subsequently identified using gas chromatography-mass spectrometry (GC-MS) and metal oxide semiconductor electronic nose (MOS e-nose). The GC-MS analysis revealed that terpenes comprised over 75% of volatile compounds in all examined samples, with zingiberene, β-sesquiphellandrene, and (E, E)-α-farnesene being the dominant constituents. Fresh ginger contained a higher relative proportion compared to dried samples. After FIR-HAD treatment, the terpene levels decreased by 11.9%, 8.9%, 13.7%, and 18.2% at 50 °C, 60 °C, 70 °C, and 80 °C, respectively. Among the various drying conditions, ginger subjected to FIR-HAD at 60 °C displayed the highest concentrations of volatile compounds and exhibited flavor characteristics closest to those of fresh samples. The flavor profiles were further evaluated using MOS e-nose analysis. The terpene compounds demonstrated a strong correlation with the response values of W1W and W2W sensors according to partial least squares regression models. In addition, the concentrations of 6-gingerol, 8-gingerol, and 10-gingerol in ginger exposed to FIR-HAD at 60 °C were also higher compared to other drying conditions. This indicated that the FIR-HAD at 60 °C is more suitable for producing dried ginger with remaining flavor attributes. These findings offer theoretical insights into the changes in volatile compounds of ginger slices during the FIR-HAD procedure. They also highlight the potential for improving drying efficiency through aroma online control techniques in future research.

求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Journal of Food Measurement and Characterization
Journal of Food Measurement and Characterization Agricultural and Biological Sciences-Food Science
CiteScore
6.00
自引率
11.80%
发文量
425
期刊介绍: This interdisciplinary journal publishes new measurement results, characteristic properties, differentiating patterns, measurement methods and procedures for such purposes as food process innovation, product development, quality control, and safety assurance. The journal encompasses all topics related to food property measurement and characterization, including all types of measured properties of food and food materials, features and patterns, measurement principles and techniques, development and evaluation of technologies, novel uses and applications, and industrial implementation of systems and procedures.
期刊最新文献
Red radish anthocyanin-based intelligent starch/pectin films for shrimp sub-freshness monitoring: effect of adjusting pH value of the film-forming solution Comparative analysis of biochemical composition of fried coconut chips: influence of thickness and oil type on nutritional attributes Phytonutrient-rich guava date fruit confection: formulation, quality analysis and shelf-life studies A novel synbiotic edible film based on aquafaba, psyllium husk powder, PEG 400, and Lactiplantibacillus plantarum 299v and applicability on Kashar cheese Microencapsulation of Elaeis guineensis leaf extract powder enriched with bioflavonoid preserves its antioxidant and anti-inflammatory properties: spray drying optimization and powder characterization
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1