{"title":"使用 CS2 和环氧胺合成 1,3-噻唑烷-2-硫醚","authors":"Azim Ziyaei Halimehjani , Farzaneh Noorakhtar , Zahra Marjani","doi":"10.1016/j.tetlet.2024.155361","DOIUrl":null,"url":null,"abstract":"<div><div>An efficient method for the synthesis of 5-(hydoxymethyl)-1,3-thiazolidine-2-thiones is developed <em>via</em> the reaction of carbon disulfide with <em>N</em>-alkyl(aryl) epoxy amines. The reaction proceeds via intramolecular epoxide ring opening with <em>in situ</em> prepared dithiocarbamic acid. The products were obtained in good to high yields.</div></div>","PeriodicalId":438,"journal":{"name":"Tetrahedron Letters","volume":"152 ","pages":"Article 155361"},"PeriodicalIF":1.5000,"publicationDate":"2024-11-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis of 1,3-thiazolidine-2-thiones using CS2 and epoxy amines\",\"authors\":\"Azim Ziyaei Halimehjani , Farzaneh Noorakhtar , Zahra Marjani\",\"doi\":\"10.1016/j.tetlet.2024.155361\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>An efficient method for the synthesis of 5-(hydoxymethyl)-1,3-thiazolidine-2-thiones is developed <em>via</em> the reaction of carbon disulfide with <em>N</em>-alkyl(aryl) epoxy amines. The reaction proceeds via intramolecular epoxide ring opening with <em>in situ</em> prepared dithiocarbamic acid. The products were obtained in good to high yields.</div></div>\",\"PeriodicalId\":438,\"journal\":{\"name\":\"Tetrahedron Letters\",\"volume\":\"152 \",\"pages\":\"Article 155361\"},\"PeriodicalIF\":1.5000,\"publicationDate\":\"2024-11-06\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Tetrahedron Letters\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0040403924004568\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"CHEMISTRY, ORGANIC\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Tetrahedron Letters","FirstCategoryId":"92","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0040403924004568","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CHEMISTRY, ORGANIC","Score":null,"Total":0}
Synthesis of 1,3-thiazolidine-2-thiones using CS2 and epoxy amines
An efficient method for the synthesis of 5-(hydoxymethyl)-1,3-thiazolidine-2-thiones is developed via the reaction of carbon disulfide with N-alkyl(aryl) epoxy amines. The reaction proceeds via intramolecular epoxide ring opening with in situ prepared dithiocarbamic acid. The products were obtained in good to high yields.
期刊介绍：
Tetrahedron Letters provides maximum dissemination of outstanding developments in organic chemistry. The journal is published weekly and covers developments in techniques, structures, methods and conclusions in experimental and theoretical organic chemistry. Rapid publication of timely and significant research results enables researchers from all over the world to transmit quickly their new contributions to large, international audiences.
京公网安备 11010802042870号
京ICP备2023020795号-1
分享
求助内容：
应助结果提醒方式：
扫码关注我们
