分析镁对薄荷介导的 Mn2O3 纳米粒子在储能和生物医学应用中的协同效应

IF 4.4 3区 化学 Q1 CHEMISTRY, INORGANIC & NUCLEAR Inorganic Chemistry Communications Pub Date : 2024-11-14 DOI:10.1016/j.inoche.2024.113539
Sainta Jostar T. , G. Johnsy Arputhavalli , Nithyadharseni Palaniyandy , S. Jebasingh , Mohammad Y. Alshahrani , G.S. Divya , P. Muthu Vijayalakshmi
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引用次数: 0

摘要

本文介绍了用绿色合成法轻松制备立方结构纯锰氧化物和掺镁锰氧化物纳米粒子的方法。研究了所制备的纯 Mn2O3 纳米粒子和掺杂 Mg 纳米粒子的结构、官能团、带隙、形貌和成分。X 射线衍射(XRD)和场发射扫描电子显微镜(FE-SEM)显微照片清楚地证实了立方结构的 Mn2O3 和掺镁 Mn2O3 纳米粒子。傅立叶变换红外光谱(FTIR)显示了两个不同的振动峰,分别对应于对称伸展的 Mn-O 和 Mn-O-Mn,紫外和聚光结果也充分证明了这一点。在不同的扫描速率(mV/s)下,对制备的纯样品和掺镁样品进行了循环伏安研究。显然,掺杂镁的 Mn2O3 纳米粒子的比电容值最高,达到 266 F/g,能量密度为 430 Wh/kg。制备的样品还表现出抗菌活性,对特定细菌和真菌的抑制区有所变化。研究结果表明,制备的掺镁纳米粒子可以作为一种很有前途的超级电容器、抗生物膜、抗氧化剂和净水器。
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Analyzing the synergistic effect of Mg on Mentha spicata L. mediated Mn2O3 nanoparticles for energy storage and bio-medical applications
This article describes the facile preparation of cubic structured pure and Mg-doped Mn2O3 nanoparticles by green synthesis method. The prepared pure and Mg-doped Mn2O3 nanoparticles were investigated to determine their structure, functional group, band gap, morphology and composition. The cubic structured Mn2O3 and Mg-doped Mn2O3 nanoparticles were clearly confirmed by X-Ray Diffraction (XRD) and Field Emission Scanning Electron Microscope (FE-SEM) micrographs. Fourier transform infrared (FTIR) spectroscopy spectra revealed two distinct vibration peaks corresponding to the symmetric stretching Mn–O and Mn–O–Mn, which was well supported by the UV and PL outcomes. A Cyclic Voltammetry study was explored for the prepared pure and Mg-doped samples at different scan rates (mV/s). Apparently, Mg-doped Mn2O3 nanoparticles exhibited the highest specific capacitance value of 266 F/g with an energy density of 430 Wh/kg. The prepared sample also exhibited antimicrobial activity by showing variation in the zone of inhibition with respect to selected bacteria and fungi. The results of the study suggest that the prepared Mg-doped nanoparticles could act as a promising supercapacitor, anti-biofilm, anti-oxidant agent and water purifier.
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来源期刊
Inorganic Chemistry Communications
Inorganic Chemistry Communications 化学-无机化学与核化学
CiteScore
5.50
自引率
7.90%
发文量
1013
审稿时长
53 days
期刊介绍: Launched in January 1998, Inorganic Chemistry Communications is an international journal dedicated to the rapid publication of short communications in the major areas of inorganic, organometallic and supramolecular chemistry. Topics include synthetic and reaction chemistry, kinetics and mechanisms of reactions, bioinorganic chemistry, photochemistry and the use of metal and organometallic compounds in stoichiometric and catalytic synthesis or organic compounds.
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