通过溶液老化处理提高激光添加剂制造的 17-4PHss 的耐磨性和侵蚀磨损性能

IF 3.2 3区 材料科学 Q2 MATERIALS SCIENCE, COATINGS & FILMS Journal of Thermal Spray Technology Pub Date : 2024-10-07 DOI:10.1007/s11666-024-01844-x
T. Wang, M. S. Wang, T. Z. Xu, C. L. Wu, C. H. Zhang, S. Zhang, H. T. Chen, J. Chen
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引用次数: 0

摘要

磨损和侵蚀磨损是流道部件的主要失效机制,积极的预防性维护可以有效延长其使用寿命。本研究利用激光金属沉积技术对 17-4PH 不锈钢(17-4PHss)进行添加制造,然后进行固溶时效处理。研究了固溶时效处理前后的结构变化,以及热处理后 17-4PHss 的干磨损和侵蚀磨损性能。在热处理过程中,固溶处理将微观结构完全转变为马氏体,减轻了添加剂过程产生的应力,并将微观结构细化至 0.64 μm。随后的时效处理进一步细化了晶粒,最终使晶粒大小从添加状态下的 0.68 μm 减小到 0.62 μm。与传统铸造相比,17-4PHss 的晶粒大小减少了 6.83%。此外,NbC 在试样中均匀分布,起到了次相强化作用,从而获得了较高的显微硬度(455.5 HV0.2)。同时,固溶老化(SSA)样品表现出很强的耐磨性,在低负荷时表现出磨料磨损。随着载荷的增加,会出现向磨料磨损和粘着磨损的过渡,同时伴有氧化磨损和疲劳磨损。在 30 N 负荷下,SSA 样品的比磨损率降至 0.17 × 10-5 mm3/Nm,这归因于 SSA 样品在高负载下更稳定的微观结构。在侵蚀磨损试验中,热处理后试样的累积质量损失最低(10.71 mg/m2h),侵蚀磨损机制归因于塑性变形和微切削。
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Enhancing Wear Resistance and Erosion Wear Performance of Laser Additive Manufactured 17-4PHss through Solution Aging Treatment

Wear and erosion wear represent primary failure mechanisms in flow passage components, and proactive preventive maintenance can effectively extend their service life. This study investigates the utilization of laser metal deposition technology for the additive manufacturing of 17-4PH stainless steel (17-4PHss) followed by solid solution aging treatment. Structural transformations before and after the solution aging treatment, along with the dry wear and erosion wear properties of 17-4PHss post-heat treatment, were examined. During the heat treatment process, the solid solution treatment fully transformed the microstructure to martensite, alleviating the stress generated by the additive process, and refined the microstructure to 0.64 μm. The subsequent aging treatment further refined the grains, ultimately reducing the grain size from 0.68 μm in the additive state to 0.62 μm. Compared to traditional casting, the grain size of 17-4PHss was reduced by 6.83%. Additionally, NbC was uniformly distributed in the sample, playing a secondary phase strengthening role, resulting in high microhardness (455.5 HV0.2). Simultaneously, the solid solution-aged (SSA) sample exhibited robust wear resistance, manifesting abrasive wear at low loads. With increasing load, a transition to abrasive wear and adhesive wear occurs, accompanied by oxidative wear and fatigue wear. At a 30 N load, the specific wear rate of the SSA sample decreased to 0.17 × 10−5 mm3/Nm, attributed to the more stable microstructure of the SSA sample under high loads. In the erosion wear test, the cumulative mass loss of the sample after heat treatment was the lowest (10.71 mg/m2h), with the erosion wear mechanism attributed to plastic deformation and micro-cutting.

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来源期刊
Journal of Thermal Spray Technology
Journal of Thermal Spray Technology 工程技术-材料科学:膜
CiteScore
5.20
自引率
25.80%
发文量
198
审稿时长
2.6 months
期刊介绍: From the scientific to the practical, stay on top of advances in this fast-growing coating technology with ASM International''s Journal of Thermal Spray Technology. Critically reviewed scientific papers and engineering articles combine the best of new research with the latest applications and problem solving. A service of the ASM Thermal Spray Society (TSS), the Journal of Thermal Spray Technology covers all fundamental and practical aspects of thermal spray science, including processes, feedstock manufacture, and testing and characterization. The journal contains worldwide coverage of the latest research, products, equipment and process developments, and includes technical note case studies from real-time applications and in-depth topical reviews.
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