纳米压痕测试证明的 L12 金属间化合物 Ni3Si 强度异常的高应变速率持续性

IF 8.3 1区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Acta Materialia Pub Date : 2024-11-27 DOI:10.1016/j.actamat.2024.120598
Benoit Merle, Christopher C. Walker, Christopher H. Zenk, George M. Pharr
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引用次数: 0

摘要

L12 金属间化合物是喷气发动机中广泛使用的镍基超级合金的基本成分。它们的特殊高温机械性能来自屈服强度异常机制。尽管其对碰撞(例如鸟击)具有潜在的安全影响,但其在高应变速率下的持久性仍未得到确证。本文通过在单一纳米压痕测试系统中结合高应变速率和高温测试,研究 L12 单相 Ni3Si 在 0.1 至 100 s-1 应变速率下的强度异常演变,从而克服了实验限制。结果发现,高应变率会将异常行为扩展到更高的温度,而强度异常的起始温度和峰值温度对应用应变率基本不敏感。这些实验结果验证了派达尔-波普-维特克(PPV)理论的基本假设。此外,由于 L12 化合物对应变速率的总体正敏感性,高应变速率会增加峰值异常硬度。
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High strain rate persistence of the strength anomaly in the L12 intermetallic compound Ni3Si evidenced by nanoindentation testing
L12 intermetallic compounds are essential constituents of the nickel-based superalloys widely used in jet engines. They derive their exceptional high-temperature mechanical properties from the yield strength anomaly mechanism. Despite potential safety implications for collisions, e.g. bird strikes, conclusive evidence of its persistence at high strain rates has remained elusive. This is mostly due to experimental limitations, which are overcome here by combining high strain rate and high temperature testing within a single nanoindentation testing system to investigate the evolution of the strength anomaly in the L12 single-phase Ni3Si for strain rates between 0.1 and 100 s-1. High strain rates are found to extend the anomalous behavior toward higher temperatures, while the onset and peak temperatures of the strength anomaly remain largely insensitive to the applied strain rate. These experimental findings validate basic assumptions from the Paidar-Pope-Vitek (PPV) theory of its origin. In addition, high strain rates are found to increase the peak anomalous hardness, owing to the overall positive strain rate sensitivity of the L12 compound.
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来源期刊
Acta Materialia
Acta Materialia 工程技术-材料科学:综合
CiteScore
16.10
自引率
8.50%
发文量
801
审稿时长
53 days
期刊介绍: Acta Materialia serves as a platform for publishing full-length, original papers and commissioned overviews that contribute to a profound understanding of the correlation between the processing, structure, and properties of inorganic materials. The journal seeks papers with high impact potential or those that significantly propel the field forward. The scope includes the atomic and molecular arrangements, chemical and electronic structures, and microstructure of materials, focusing on their mechanical or functional behavior across all length scales, including nanostructures.
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