Biwu Zhu , Jing Su , Xiao Liu , Changping Tang , Wenhui Liu , Luoxing Li , Congchang Xu , Pengcheng Guo
{"title":"AZ81-La 合金中{10-12}延伸孪晶激发的晶间变形机制","authors":"Biwu Zhu , Jing Su , Xiao Liu , Changping Tang , Wenhui Liu , Luoxing Li , Congchang Xu , Pengcheng Guo","doi":"10.1016/j.jre.2024.06.033","DOIUrl":null,"url":null,"abstract":"<div><div>In polycrystalline Mg-RE magnesium alloys, the lattice parameter, dislocation dynamics and critical resolved shear stress (CRSS) for various deformation modes are altered with the addition of RE atom, finally affecting deformation mode and strain accommodation mechanism among neighboring grains. Uniaxial compression tests were performed on as-extruded AZ81-La Mg alloy samples with the <em>c</em>-axis of the majority of crystals vertical to the compression direction. Twin variants and dominant slip systems were examined by electron backscattered diffraction (EBSD) technique. It is found by in-grain misoriention axis (IGMA) analysis that the plastic deformation is mainly accommodated by a combination of the pyramidal <<em>c</em>+<em>a</em>> slip and the basal <<em>a</em>> slip. The dominant twin variant is <span><math><mrow><mrow><mo>{</mo><mn>0</mn></mrow><mover><mn>1</mn><mo>¯</mo></mover><mrow><mn>12</mn><mo>}</mo></mrow></mrow></math></span> <<span><math><mrow><mn>01</mn><mover><mn>1</mn><mo>¯</mo></mover><mn>1</mn></mrow></math></span>> and <span><math><mrow><mrow><mo>{</mo><mn>1</mn></mrow><mover><mn>1</mn><mo>¯</mo></mover><mrow><mn>02</mn><mo>}</mo></mrow></mrow></math></span> <<span><math><mrow><mover><mn>1</mn><mo>¯</mo></mover><mn>101</mn></mrow></math></span>>. Here, we applied a modified displacement gradient accommodation (m-DGA) method to evaluate the selection mechanism of twin/slip in neighbour grain stimulated by <span><math><mrow><mrow><mo>{</mo><mn>10</mn></mrow><mover><mn>1</mn><mo>¯</mo></mover><mrow><mn>2</mn><mo>}</mo></mrow></mrow></math></span> extension twin. It is found that the activated slip system and/or twin variant in the neighbouring grain is determined by the accommodation of the major shear strain induced by <span><math><mrow><mrow><mo>{</mo><mn>10</mn></mrow><mover><mn>1</mn><mo>¯</mo></mover><mrow><mn>2</mn><mo>}</mo></mrow></mrow></math></span> extension twin in such a way that strain concentration along grain boundaries can be relaxed.</div></div>","PeriodicalId":16940,"journal":{"name":"Journal of Rare Earths","volume":"42 12","pages":"Pages 2325-2331"},"PeriodicalIF":5.2000,"publicationDate":"2024-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Intergranular deformation mechanism stimulated by {10-12} extension twins in AZ81-La alloy\",\"authors\":\"Biwu Zhu , Jing Su , Xiao Liu , Changping Tang , Wenhui Liu , Luoxing Li , Congchang Xu , Pengcheng Guo\",\"doi\":\"10.1016/j.jre.2024.06.033\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>In polycrystalline Mg-RE magnesium alloys, the lattice parameter, dislocation dynamics and critical resolved shear stress (CRSS) for various deformation modes are altered with the addition of RE atom, finally affecting deformation mode and strain accommodation mechanism among neighboring grains. Uniaxial compression tests were performed on as-extruded AZ81-La Mg alloy samples with the <em>c</em>-axis of the majority of crystals vertical to the compression direction. Twin variants and dominant slip systems were examined by electron backscattered diffraction (EBSD) technique. It is found by in-grain misoriention axis (IGMA) analysis that the plastic deformation is mainly accommodated by a combination of the pyramidal <<em>c</em>+<em>a</em>> slip and the basal <<em>a</em>> slip. The dominant twin variant is <span><math><mrow><mrow><mo>{</mo><mn>0</mn></mrow><mover><mn>1</mn><mo>¯</mo></mover><mrow><mn>12</mn><mo>}</mo></mrow></mrow></math></span> <<span><math><mrow><mn>01</mn><mover><mn>1</mn><mo>¯</mo></mover><mn>1</mn></mrow></math></span>> and <span><math><mrow><mrow><mo>{</mo><mn>1</mn></mrow><mover><mn>1</mn><mo>¯</mo></mover><mrow><mn>02</mn><mo>}</mo></mrow></mrow></math></span> <<span><math><mrow><mover><mn>1</mn><mo>¯</mo></mover><mn>101</mn></mrow></math></span>>. Here, we applied a modified displacement gradient accommodation (m-DGA) method to evaluate the selection mechanism of twin/slip in neighbour grain stimulated by <span><math><mrow><mrow><mo>{</mo><mn>10</mn></mrow><mover><mn>1</mn><mo>¯</mo></mover><mrow><mn>2</mn><mo>}</mo></mrow></mrow></math></span> extension twin. It is found that the activated slip system and/or twin variant in the neighbouring grain is determined by the accommodation of the major shear strain induced by <span><math><mrow><mrow><mo>{</mo><mn>10</mn></mrow><mover><mn>1</mn><mo>¯</mo></mover><mrow><mn>2</mn><mo>}</mo></mrow></mrow></math></span> extension twin in such a way that strain concentration along grain boundaries can be relaxed.</div></div>\",\"PeriodicalId\":16940,\"journal\":{\"name\":\"Journal of Rare Earths\",\"volume\":\"42 12\",\"pages\":\"Pages 2325-2331\"},\"PeriodicalIF\":5.2000,\"publicationDate\":\"2024-06-27\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Rare Earths\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1002072124002175\",\"RegionNum\":1,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"CHEMISTRY, APPLIED\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Rare Earths","FirstCategoryId":"92","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1002072124002175","RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"CHEMISTRY, APPLIED","Score":null,"Total":0}
引用次数: 0
摘要
在多晶 Mg-RE 镁合金中,RE 原子的加入会改变晶格参数、位错动力学和各种变形模式的临界分辨剪切应力(CRSS),并最终影响相邻晶粒间的变形模式和应变容纳机制。在大多数晶体的 c 轴垂直于压缩方向的 AZ81-La 镁合金样品上进行了单轴压缩试验。通过电子反向散射衍射(EBSD)技术检测了孪晶变体和主要滑移系统。通过晶粒内失向轴(IGMA)分析发现,塑性变形主要是由金字塔形滑移和基底滑移组合而成。主要的孪生变体是{01¯12} <011¯1>和{11¯02} <1¯101>。在此,我们应用改进的位移梯度容纳(m-DGA)方法来评估{101¯2}延伸孪晶刺激邻近晶粒孪晶/滑移的选择机制。结果发现,{101¯2}延伸孪晶诱发的主要剪切应变的容纳方式决定了邻近晶粒中的激活滑移系统和/或孪晶变体,从而可以放松沿晶界的应变集中。
Intergranular deformation mechanism stimulated by {10-12} extension twins in AZ81-La alloy
In polycrystalline Mg-RE magnesium alloys, the lattice parameter, dislocation dynamics and critical resolved shear stress (CRSS) for various deformation modes are altered with the addition of RE atom, finally affecting deformation mode and strain accommodation mechanism among neighboring grains. Uniaxial compression tests were performed on as-extruded AZ81-La Mg alloy samples with the c-axis of the majority of crystals vertical to the compression direction. Twin variants and dominant slip systems were examined by electron backscattered diffraction (EBSD) technique. It is found by in-grain misoriention axis (IGMA) analysis that the plastic deformation is mainly accommodated by a combination of the pyramidal <c+a> slip and the basal <a> slip. The dominant twin variant is <> and <>. Here, we applied a modified displacement gradient accommodation (m-DGA) method to evaluate the selection mechanism of twin/slip in neighbour grain stimulated by extension twin. It is found that the activated slip system and/or twin variant in the neighbouring grain is determined by the accommodation of the major shear strain induced by extension twin in such a way that strain concentration along grain boundaries can be relaxed.
期刊介绍:
The Journal of Rare Earths reports studies on the 17 rare earth elements. It is a unique English-language learned journal that publishes works on various aspects of basic theory and applied science in the field of rare earths (RE). The journal accepts original high-quality original research papers and review articles with inventive content, and complete experimental data. It represents high academic standards and new progress in the RE field. Due to the advantage of abundant RE resources of China, the research on RE develops very actively, and papers on the latest progress in this field emerge every year. It is not only an important resource in which technicians publish and obtain their latest research results on RE, but also an important way of reflecting the updated progress in RE research field.
The Journal of Rare Earths covers all research and application of RE rare earths including spectroscopy, luminescence and phosphors, rare earth catalysis, magnetism and magnetic materials, advanced rare earth materials, RE chemistry & hydrometallurgy, RE metallography & pyrometallurgy, RE new materials, RE solid state physics & solid state chemistry, rare earth applications, RE analysis & test, RE geology & ore dressing, etc.