具有不同长周期有序堆积相(LPSO)体积分数的挤压成型 Mg-Zn-Y-Mn 合金的力学性能和各向异性

IF 5.2 1区 化学 Q1 CHEMISTRY, APPLIED Journal of Rare Earths Pub Date : 2024-06-29 DOI:10.1016/j.jre.2024.06.034
Dahui Liang , Mincong Chen , Chuanqiang Li , Zhipei Tong , Yong Dong , Dong Bian
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引用次数: 0

摘要

通过光学显微镜、扫描电子显微镜、纹理分析、透射电子显微镜和拉伸试验研究了不同体积分数的长周期堆积有序相(LPSO)对挤压成型的Mg-xZn-yY-0.1Mn(x=1 wt%、2 wt%、4 wt%,y=2 wt%、4 wt%、8 wt%)合金的显微组织、力学性能和各向异性的影响。结果表明,随着 Zn 和 Y 含量的增加,在 Y/Zn 值不变的情况下,LPSO 相的体积分数从 ZW12 到 ZW24 再到 ZW48,含 LPSO 的 Mg-Zn-Y-Mn 体系的机械强度随着 LPSO 相的增加而逐渐提高。在 LPSO 相体积分数最高的情况下,ZW48 合金沿挤压方向(ED)的极限拉伸强度(UTS)最高,达到 427 MPa,而 ZW12 合金的极限拉伸强度(UTS)为 307 MPa,ZW24 合金的极限拉伸强度(UTS)为 347 MPa。此外,ZW48 合金的伸长率保持在适中的 9.9%,也是所研究的三种合金中最高的。另一方面,纹理分析表明,ZW48 合金中 α-Mg 相的基底纹理因生成更多 LPSO 相而明显减弱。相反,ZW12 合金中的α-Mg 相具有较高的纹理强度和明显的力学各向异性。然而,在含有大量 LPSO 相的 ZW48 合金中,机械各向异性仍然存在,这主要归因于大型 LPSO 沿 ED 的带状分布。
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Mechanical property and anisotropy of as-extruded Mg–Zn–Y–Mn alloys with different volume fraction of long-period stacking ordered (LPSO) phase
Effects of different volume fraction of long-period stacking ordered (LPSO) phase on the microstructure, mechanical property and anisotropy of the as-extruded Mg-xZn-yY-0.1Mn (x = 1 wt%, 2 wt%, 4 wt% and y = 2 wt%, 4 wt%, 8 wt%) alloys were studied by an optical microscope, a scanning electron microscope, texture analysis, a transmission electron microscope and tensile testing. The results reveal that the volume fraction of LPSO phase increases from ZW12 to ZW24 to ZW48 alloys with the elevating Zn and Y content but constant Y/Zn value, and the mechanical strength of the LPSO-containing Mg–Zn–Y–Mn system is gradually improved when increasing LPSO phases. With the highest volume fraction of LPSO phase, ZW48 alloy presents the highest ultimate tensile strength (UTS) of 427 MPa along the extrusion direction (ED) when compared with those of ZW12 alloy with the UTS of 307 MPa and ZW24 alloy with the UTS of 347 MPa. Moreover, the elongation ratio of ZW48 alloy is maintained to moderate 9.9%, which is also the highest among three studied alloys. On the other hand, texture analysis demonstrates that the basal texture of the α-Mg phase in the ZW48 alloy is significantly weakened by the generation of more LPSO phases. On the contrary, a high texture intensity of α-Mg phase and obvious mechanical anisotropy can be observed for the ZW12 alloy. However, mechanical anisotropy still exists in the ZW48 alloy containing massive LPSO phases, which is attributed primarily to the zonal distribution of large LPSO along the ED.
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来源期刊
Journal of Rare Earths
Journal of Rare Earths 化学-应用化学
CiteScore
8.70
自引率
14.30%
发文量
374
审稿时长
1.7 months
期刊介绍: The Journal of Rare Earths reports studies on the 17 rare earth elements. It is a unique English-language learned journal that publishes works on various aspects of basic theory and applied science in the field of rare earths (RE). The journal accepts original high-quality original research papers and review articles with inventive content, and complete experimental data. It represents high academic standards and new progress in the RE field. Due to the advantage of abundant RE resources of China, the research on RE develops very actively, and papers on the latest progress in this field emerge every year. It is not only an important resource in which technicians publish and obtain their latest research results on RE, but also an important way of reflecting the updated progress in RE research field. The Journal of Rare Earths covers all research and application of RE rare earths including spectroscopy, luminescence and phosphors, rare earth catalysis, magnetism and magnetic materials, advanced rare earth materials, RE chemistry & hydrometallurgy, RE metallography & pyrometallurgy, RE new materials, RE solid state physics & solid state chemistry, rare earth applications, RE analysis & test, RE geology & ore dressing, etc.
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