一种具有脉冲管和焦耳-汤姆逊冷却的超高真空扫描隧道显微镜,工作在亚pm z噪声下。

IF 1.7 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Review of Scientific Instruments Pub Date : 2024-12-01 DOI:10.1063/5.0230892
Marcus Eßer, Marco Pratzer, Marc Frömming, Jonas Duffhauß, Priyamvada Bhaskar, Michael A Krzyzowski, Markus Morgenstern
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引用次数: 0

摘要

低温扫描隧道光谱是探测原子尺度下的电子和磁性的关键方法,但其振动灵敏度极高。这使得采用脉冲型振动激励的闭式循环冷却具有挑战性,尽管这是强制性的,以避免氦气损失,以抵消不断上涨的氦气价格。在这里,我们描述了一种紧凑的超高真空扫描隧道显微镜(STM)系统,该系统具有集成的主脉冲管冷却器(PTC),用于闭式循环操作。它通过二次焦耳-汤姆逊级实现温度降至1.5 K,在0.1 Hz-5 kHz(反馈回路关闭)的频率范围内,STM结的z噪声降至300 fmRMS。这比许多由外部液氦供应冷却的stm要好。将PTC的有效振动解耦与充分的热传导结合起来的挑战是通过使用多方面的方法来解决的,包括具有最小刚度的波纹管的概念,以使PTC与STM的振动解耦,以及优化的STM设计,将振动传递到STM结。作为重要的基准,我们可以将隧道结中的电压噪声降低到120 μV,并通过附近的天线在结中提供高达40 GHz、幅度高达10 mV的射频激励。这一发展主要实现了其他二次冷却阶段,从而为stm在整个有趣温度范围内的氦保存操作开辟了前景。
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An ultra-high vacuum scanning tunneling microscope with pulse tube and Joule-Thomson cooling operating at sub-pm z-noise.

Low-temperature scanning tunneling spectroscopy is a key method to probe electronic and magnetic properties down to the atomic scale, but suffers from extreme vibrational sensitivity. This makes it challenging to employ closed-cycle cooling with its required pulse-type vibrational excitations, albeit this is mandatory to avoid helium losses for counteracting the continuously raising helium prices. Here, we describe a compact ultra-high vacuum scanning tunneling microscope (STM) system with an integrated primary pulse tube cooler (PTC) for closed-cycle operation. It achieves temperatures down to 1.5 K via a secondary Joule-Thomson stage and a z-noise down to 300 fmRMS in the STM junction for the frequency range of 0.1 Hz-5 kHz (feedback loop off). This is better than many STMs cooled by an external supply of liquid helium. The challenge to combine an effective vibrational decoupling from the PTC with sufficient thermal conduction is tackled by using a multipartite approach including the concept of bellows with minimal stiffness to decouple the PTC vibrationally from the STM and an optimized STM design with minimal vibrational transfer to the STM junction. As important benchmarks, we could reduce the voltage noise in the tunnel junction down to 120 μV and supply radio frequency excitations up to 40 GHz with amplitudes up to 10 mV in the junction via a close-by antenna. The development principally enables other secondary cooling stages such that it opens the perspective for a helium conserving operation of STMs across the whole interesting temperature range.

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来源期刊
Review of Scientific Instruments
Review of Scientific Instruments 工程技术-物理:应用
CiteScore
3.00
自引率
12.50%
发文量
758
审稿时长
2.6 months
期刊介绍: Review of Scientific Instruments, is committed to the publication of advances in scientific instruments, apparatuses, and techniques. RSI seeks to meet the needs of engineers and scientists in physics, chemistry, and the life sciences.
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