生物制备SnO2纳米结构在太阳能驱动下的非均相光催化去除水溶液中的2,4二氯苯氧乙酸

IF 2.8 3区 化学 Q2 CHEMISTRY, MULTIDISCIPLINARY Research on Chemical Intermediates Pub Date : 2024-11-18 DOI:10.1007/s11164-024-05445-9
Waseem Ahmad, Akil Ahmad, Mahvish Shameem
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引用次数: 0

摘要

目前的研究重点是利用余甘子叶提取物生物制备氧化锡纳米粒子。这些研究集中在所开发材料的理化特性上,并检验了它们作为光催化剂和抗菌剂的有效性。采用XRD、SEM、FTIR和UV等光谱技术研究了生物合成的SnO2NPs的结构特征。评价了构建材料光催化去除2,4二氯苯氧基乙酸(2,4 D)的效果;同时,对所选菌株肺炎克雷伯菌、大肠杆菌、金黄色葡萄球菌和化脓性链球菌进行抑菌效果评价。XRD和SEM检测表明,颗粒呈球形,直径在50 ~ 60 nm之间。随后,开发的SnO2 NPs在去除水溶液中的2,4 D方面表现出了显著的光催化能力,并且在120 min内去除了水溶液中约74%的有机污染物。抗菌实验表明,开发的材料对所测试的细菌菌株具有显著的抑制作用。在60µg/mL浓度下,对肺炎克雷伯菌的抑制范围为21 mm。
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Solar light-driven heterogeneous photocatalytic removal of 2,4 dichlorophenoxy acetic acid from aqueous solution by bio-fabricated SnO2 nanostructure

The current research work highlighted the bio-fabrication of tin oxide nanoparticles (SnO2 NPs) by employing Phyllanthus emblica leaf extract. These investigations concentrated on the physiochemical characteristics of the developed material and examined their effectiveness as photocatalysts and antibacterial agents. The structural characteristics of the bio-fabricated SnO2NPs were investigated by XRD, SEM, FTIR, and UV spectroscopic techniques. Photocatalytic efficacy of the constructed materials was evaluated in the removal of the 2,4 dicholorophenoxy acetic acid (2,4 D); meanwhile, the antibacterial potency of the developed material was assessed against the chosen bacterial strain Klebsiella pneumoniae, Escherichia coli, Staphylococcus aureus, and Streptococcus pyogenes. The XRD and SEM examination revealed that the particles are spherical with diameters ranging from 50 to 60 nm. Subsequently, the developed SnO2 NPs demonstrated significant photocatalytic potency in the removal of the 2,4 D from the aqueous solution, and approximately 74% of organic pollutants were removed from the aqueous solution within the period of 120 min. The antibacterial assay demonstrated that the developed material shows significant inhibition of the tested bacterial strain. Maximum inhibition was observed against the Klebsiella pneumoniae with the 21 mm zone of inhibition at 60 µg/mL.

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来源期刊
CiteScore
5.70
自引率
18.20%
发文量
229
审稿时长
2.6 months
期刊介绍: Research on Chemical Intermediates publishes current research articles and concise dynamic reviews on the properties, structures and reactivities of intermediate species in all the various domains of chemistry. The journal also contains articles in related disciplines such as spectroscopy, molecular biology and biochemistry, atmospheric and environmental sciences, catalysis, photochemistry and photophysics. In addition, special issues dedicated to specific topics in the field are regularly published.
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