轧制温度对活化Cu-3.0Be合金二次电子发射性能线性电流范围的影响

IF 5.5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2025-02-01 Epub Date: 2024-12-20 DOI:10.1016/j.matchar.2024.114661
Si Zou , Daibo Zhu , Xiaochen Ding , Tao Deng , Fan Zhou , Wenming Zhu , Haining Liu , Xinyan Liu , Xiaoyu Jiang , Yanbin Jiang
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引用次数: 0

摘要

本文研究了热轧对活化Cu-3.0Be薄板二次电子产率曲线线性电流范围的影响。SEY曲线测试分析表明,BeO层在650°C时表现出良好的线性动态范围,范围约为0-201 eV。SEM结果表明,650℃轧制的BeO层表面致密光滑,而800℃轧制的BeO层表面织构粗糙。由于电荷积累和电场效应的增强,不均匀的表面形貌会阻碍二次电子的发射或吸收。在650℃轧制的样品中,BeO层厚度为15-27 nm,而在800℃轧制的样品中,BeO层厚度仅为8-15 nm。此外,在650°C轧制样品的TEM图像中检测到许多位错线。这些线有利于Be元素的扩散,在其激活后导致更厚的BeO层。过薄的BeO层会导致合金衬底中激发的二次电子和自由电子之间的碰撞,导致初始速度降低,并且在低电压下阻碍到下一个节点的进展,从而导致电流的线性范围窄。
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Rolling temperature effects on linear current range of secondary electron emission properties of an activated Cu–3.0Be alloy
This study investigates the impact of hot rolling on the linear current range of the secondary electron yield (SEY) curve for activated Cu-3.0Be sheets. Analysis of the SEY curve tests revealed that the BeO layer exhibited a favorable linear dynamic range at 650 °C, spanning approximately 0–201 eV. SEM results indicated BeO layer rolled at 650 °C has a compact and smooth surface, while BeO layer rolled at 800 °C has a rough surface texture. The non-uniform surface morphology can hinder the emission or absorption of secondary electrons due to charge accumulation and enhanced electric field effect. BeO layer thickness was found to be 15-27 nm for samples rolled at 650 °C, while it was only 8-15 nm for those rolled at 800 °C. Furthermore, numerous dislocation lines were detected in the TEM images of samples rolled at 650 °C. These lines facilitate the diffusion of the Be element, leading to a thicker BeO layer following its activation. Excessively thin BeO layers can lead to collisions between excited secondary electrons and free electrons in the alloy substrate, resulting in reduced initial velocity and hindered progression to the next dynode at low voltages, which leads to a narrow linear range of current.
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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