NiCo基高温合金热压结合过程中非均相界面的微观组织演变及界面愈合机制

IF 5.5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2025-02-01 Epub Date: 2024-12-20 DOI:10.1016/j.matchar.2024.114658
Shaofei Ren , He Xiao , Shengqing Wu , Chenqi Zeng , Xiaolong Bai , Sheng Liu , Bin Xu , Chuanyong Cui , Guangcai Ma , Mingyue Sun
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引用次数: 0

摘要

研究了NiCo基高温合金在热压键合过程中非均相界面的微观组织演变及键合界面的愈合机制。在热变形过程中,粗晶和细晶表现出不同的细化机制。粗晶侧主要通过变形孪晶和变形微带使晶粒细化,残余的初生γ′相也通过颗粒激发形核机制促进再结晶。位错胞在原位转变为高角度晶界的连续动态再结晶也有助于粗晶侧形成项链状再结晶。细晶侧晶粒主要通过应变诱导的不连续动态再结晶进一步细化。在热变形过程中,非均质变形引起的位错密度梯度驱动了键合界面在氧化物界面上由细晶向粗晶方向的迁移。随着变形应变的增大,由于变形不协调,迁移界面在粗晶侧形成第一层项链状再结晶。进一步增大变形应变,局部变形导致变形晶粒中不断扩展出项链状再结晶晶粒和细化再结晶晶粒。力学性能测试表明,异质界面实现了完全愈合,为双微观结构涡轮盘的制造提供了新的思路。
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Microstructure evolution and interfacial healing mechanism of heterogeneous interfaces in NiCo based superalloys during hot compression bonding
This study focuses on the microstructural evolution of heterogeneous interfaces and healing mechanism of bonding interfaces of NiCo based superalloys during hot compression bonding. The coarse and fine grain sides show distinct refinement mechanisms during hot deformation. The coarse grain side refines the grains mainly through deformation twins and deformation microbands, and the residual primary γ' phase also facilitates the recrystallization through particle-stimulated nucleation mechanism. Continuous dynamic recrystallization through in-situ transformation of dislocation cells into high angle grain boundaries also contributes to the formation of necklace-like recrystallization on coarse grain side. The grains on the fine-grain side are further refined mainly by strain-induced discontinuous dynamic recrystallization. Dislocation density gradients induced by heterogeneous deformation drive migration of bonding interfaces across interfacial oxides from fine to coarse grain side during hot deformation. As the deformation strain increases, the migrating interfaces form the first layer of necklace-like recrystallization on coarse grain side due to deformation uncoordinated. Further increasing the deformation strain, the local deformation leads to continuous expansion of necklace-like recrystallized grains in deformed grains and refined recrystallized grains. The testing of mechanical properties indicate that the heterogeneous interface achieves complete healing, which provides a new idea for fabrication of dual microstructure turbine disks.
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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