在聚酰胺织物上绿色合成银纳米粒子的方法:表征、染色和抗菌性能

IF 5.9 3区 工程技术 Q1 CHEMISTRY, MULTIDISCIPLINARY Journal of Industrial and Engineering Chemistry Pub Date : 2025-05-25 Epub Date: 2024-11-07 DOI:10.1016/j.jiec.2024.10.069
Mousa Sadeghi-Kiakhani , Elaheh Hashemi , Mohammad-Mahdi Norouzi , Parasto Soleimani , Vahid Babaahmadi
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引用次数: 0

摘要

利用天然提取物在纺织品上绿色合成纳米银(Ag NPs)是一种创新的、环保的方法,可以提高抗菌性能和染色性能。本研究介绍了一种在聚酰胺(PA)织物上直接原位合成Ag NPs的新方法,该方法以棘棘提取物(SBE)为天然染料和还原剂。利用紫外可见光谱和动态光散射(DLS)对合成过程进行表征,并确定了银纳米粒子的平均粒径。结果表明,花和茎提取物的粒径分别为62.5 nm和56.1 nm。扫描电镜(SEM)和x射线衍射(XRD)的表面形貌结果证实了Ag NPs在PA织物表面的原位形成。用SBE和Ag NPs染色的织物显示出更高的颜色强度(花和茎的K/S值分别为4.1和5.6),与没有使用银的样品相比,分别增加了64%和100%。此外,PA织物对大肠杆菌和金黄色葡萄球菌具有100%的抑制作用。洗涤10次后,茎提取物的抑菌活性分别保持在88%和85%,花提取物的抑菌活性分别保持在83%和79%。该研究强调了天然染料与纳米颗粒合成的新结合,为多功能纺织品的发展提供了一条可持续的途径。
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Green synthesis of silver nanoparticles on polyamide fabrics using Scrophularia striata Boiss extract: Characterization, dyeing, and antibacterial properties
The green synthesis of silver nanoparticles (Ag NPs) on textiles using natural extracts is emerging as an innovative, eco-friendly approach for enhancing both antibacterial properties and dyeing performance. This study introduces a novel in-situ method for synthesizing Ag NPs directly on polyamide (PA) fabrics, utilizing Scrophularia striata Boiss extract (SBE) as a natural dye and reducing agent. UV–visible spectroscopy and dynamic light scattering (DLS) were used to characterize the synthesis process and determine the average particle size of Ag NPs. The data showed particle sizes of 62.5 nm and 56.1 nm when using flower and stem extracts, respectively. Surface morphology findings from scanning electron microscopy (SEM) and corresponding diffraction peaks in X-ray diffraction (XRD) confirmed the in-situ formation of Ag NPs on the surface of PA fabric. Fabrics dyed with SBE and Ag NPs exhibited higher color strength (K/S values of 4.1 and 5.6 for flower and stem, respectively), showing 64 % and 100 % increases compared to samples without silver. Additionally, PA fabrics exhibited 100 % inhibition against E. coli and S. aureus bacteria. After 10 washing cycles, antibacterial activity was maintained at 88 % and 85 % for the stem extract and 83 % and 79 % for the flower extract. This research highlights the novel integration of natural dye and nanoparticle synthesis, providing a sustainable route for multifunctional textile development.
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来源期刊
CiteScore
10.40
自引率
6.60%
发文量
639
审稿时长
29 days
期刊介绍: Journal of Industrial and Engineering Chemistry is published monthly in English by the Korean Society of Industrial and Engineering Chemistry. JIEC brings together multidisciplinary interests in one journal and is to disseminate information on all aspects of research and development in industrial and engineering chemistry. Contributions in the form of research articles, short communications, notes and reviews are considered for publication. The editors welcome original contributions that have not been and are not to be published elsewhere. Instruction to authors and a manuscript submissions form are printed at the end of each issue. Bulk reprints of individual articles can be ordered. This publication is partially supported by Korea Research Foundation and the Korean Federation of Science and Technology Societies.
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