{"title":"[从海螺血淋巴中纯化一种伪胆碱酯酶]。","authors":"R Voigtmann, G Uhlenbruck","doi":"10.1515/znb-1971-1237","DOIUrl":null,"url":null,"abstract":"[ 1 9 5 9 ] . The nature of the restricted rotation in dialkylaminosulphinyl chlorides (3) is under investigation. Dimethylaminosulphinyl chloride (3 a) was prepared from O-ethyl ./V,iV-dimethylamidosulphite and thionvl chloride12; b.p. 30°/0.2 mmHg, ng 1.4960 (I.e.13 43 — 45°/0.3 mmHg). The chlorides (3 b) and (3 c) were synthesized directly from the corresponding amines and thionyl chloride 13; 3 b: b.p. 62°/0.6mmHg, tid 1.5165; 3 c: b.p. 75 — 76°/0.4 mmHg, semisolid compound at room temperature.","PeriodicalId":23706,"journal":{"name":"Zeitschrift fur Naturforschung. Teil B, Chemie, Biochemie, Biophysik, Biologie und verwandte Gebiete","volume":"26 12","pages":"1374-5"},"PeriodicalIF":0.0000,"publicationDate":"1971-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"[Purification of a pseudo-cholinesterase from the haemolymph of Helix pomatia].\",\"authors\":\"R Voigtmann, G Uhlenbruck\",\"doi\":\"10.1515/znb-1971-1237\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"[ 1 9 5 9 ] . The nature of the restricted rotation in dialkylaminosulphinyl chlorides (3) is under investigation. Dimethylaminosulphinyl chloride (3 a) was prepared from O-ethyl ./V,iV-dimethylamidosulphite and thionvl chloride12; b.p. 30°/0.2 mmHg, ng 1.4960 (I.e.13 43 — 45°/0.3 mmHg). The chlorides (3 b) and (3 c) were synthesized directly from the corresponding amines and thionyl chloride 13; 3 b: b.p. 62°/0.6mmHg, tid 1.5165; 3 c: b.p. 75 — 76°/0.4 mmHg, semisolid compound at room temperature.\",\"PeriodicalId\":23706,\"journal\":{\"name\":\"Zeitschrift fur Naturforschung. Teil B, Chemie, Biochemie, Biophysik, Biologie und verwandte Gebiete\",\"volume\":\"26 12\",\"pages\":\"1374-5\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1971-12-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Zeitschrift fur Naturforschung. Teil B, Chemie, Biochemie, Biophysik, Biologie und verwandte Gebiete\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1515/znb-1971-1237\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Zeitschrift fur Naturforschung. Teil B, Chemie, Biochemie, Biophysik, Biologie und verwandte Gebiete","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1515/znb-1971-1237","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
[Purification of a pseudo-cholinesterase from the haemolymph of Helix pomatia].
[ 1 9 5 9 ] . The nature of the restricted rotation in dialkylaminosulphinyl chlorides (3) is under investigation. Dimethylaminosulphinyl chloride (3 a) was prepared from O-ethyl ./V,iV-dimethylamidosulphite and thionvl chloride12; b.p. 30°/0.2 mmHg, ng 1.4960 (I.e.13 43 — 45°/0.3 mmHg). The chlorides (3 b) and (3 c) were synthesized directly from the corresponding amines and thionyl chloride 13; 3 b: b.p. 62°/0.6mmHg, tid 1.5165; 3 c: b.p. 75 — 76°/0.4 mmHg, semisolid compound at room temperature.