白芷适宜干燥加工方法的优化

中药材 Pub Date : 2016-07-01
Bing Zhou, Pei Liu, Xue-jun Lu, Da-wei Qian, Jin-ao Duan
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引用次数: 0

摘要

目的:从白芷根的外观及活性成分的含量等方面优选白芷根的干燥加工方法。方法:对阴凉处自然干燥、日光下自然干燥、热风干燥、短波红外辐射干燥等19种干燥方法进行研究。采用HPLC-PDA法测定香豆素类化合物的含量。采用内标气相色谱-质谱法测定挥发油含量。采用综合评分法对样品外观进行评价。结果:香豆素含量测定结果表明,日光自然干燥高于阴凉处自然干燥,变温干燥效果最好,恒温干燥温度与香豆素含量成反比。挥发油含量测定结果表明,变温干燥效果最好,恒温干燥温度与挥发油含量成反比。综合评分结果表明,50℃热风干燥效果最好,其次为日光自然干燥、阴凉处自然干燥和50℃短波红外辐射干燥。结论:综合考虑干燥时间、外观、活性成分含量等因素,推荐热风干燥方法和温湿度可控的热风干燥机。干燥温度为50℃,湿度为35%。该方法可为白芷等药材的干燥工艺标准提供参考。
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[Optimization of Suitable Drying Processing Methods of Angelica dahurica].

Objective: To optimize the suitable drying processing methods of the root of Angelica dahurica by the appearance and the content of active compounds.

Methods: 19 methods including natural drying in the shade, natural drying in the sun, hot air drying, shortwave infrared radiation drying were studied. HPLC-PDA method was adopted to determine the contents of coumarin compounds. GC-MS with internal standard method was used to determine the content of volatile oil. The appearance of samples was evaluated by the method of composite scores.

Results: The results of coumarins contents showed that the natural drying in the sun was higher than natural drying in the shade, variable-temperature drying was the best, and the temperature of constant temperature drying was inversely proportional to the contents of coumarins. The results of volatile oils contents showed that variable-temperature drying was the best, and the temperature of constant temperature drying was inversely proportional to the contents of volatile oils. The results of composite scores showed that hot air drying in 50 ℃ was the best, followed by natural drying in the sun, natural drying in the shade and shortwave infrared radiation drying in 50 ℃.

Conclusion: Therefore,considering the drying time,the appearance,and the content of active compounds,the hot air drying method and hot air machine with temperature and humidity controlled was recommend. The suitable parameters for the machine were that the drying temperature was 50 ℃,and the humidity was 35%. The method could provide the reference for the drying technology standard of roots such as Angelica dahurica.

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来源期刊
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期刊介绍: "Chinese Materia Medica" magazine was founded in 1978. It is a national-level academic journal of Chinese medicine science and technology approved by the State Science and Technology Commission and the Press and Publication Administration for public distribution at home and abroad. It is sponsored by the Chinese Materia Medica Information Center of the State Food and Drug Administration and is publicly distributed at home and abroad. It mainly reports on new technologies, new methods and new achievements in the production, scientific research and business management of Chinese medicine, and serves to promote the production and scientific and technological development of Chinese medicine, improve the output and quality of Chinese medicine, improve business management, and prosper the Chinese medicine industry.
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