竹叶生物质生物炭作为能源的潜力:温度和加热时间的影响。

IF 3 Q3 MATERIALS SCIENCE, BIOMATERIALS International Journal of Biomaterials Pub Date : 2019-12-14 eCollection Date: 2019-01-01 DOI:10.1155/2019/3526145
Bidayatul Armynah, Dahlang Tahir, Monalisa Tandilayuk, Zuryati Djafar, Wahyu H Piarah
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引用次数: 21

摘要

以竹叶为原料,在无氧环境下通过退火法制备了生物炭。采用近似分析、傅里叶变换红外(FTIR)、x射线衍射(XRD)、扫描电镜(SEM)和能量色散光谱(EDS)对样品进行了表征。加热温度为250°C、300°C和350°C,每种温度下,时间在30分钟、60分钟和90分钟之间变化。加热30分钟,温度为250℃时FC为30.777%,热值为15 MJ/Kg,温度为350℃时FC为4.004%,热值为6 MJ/Kg。能谱分析表明,加热时间是一个重要的参数,随着加热时间的延长,碳、氮含量逐渐减少,硅、氧含量逐渐增加。XRD在20°~ 30°范围内显示出宽的(002)反射,表明石墨烯片具有小域的相干和平行堆叠,这与SEM图像的表面形貌一致。实验结果表明,在300℃下加热30分钟是竹叶制备低成本碳的有效参数,竹叶是一种有用的能源。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Potentials of Biochars Derived from Bamboo Leaf Biomass as Energy Sources: Effect of Temperature and Time of Heating.

Biochars from bamboo leaves as a potential energy resource were synthesized by annealing in the oxygen-free environment. Samples were characterized using proximate analysis, Fourier-transform infrared (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy-dispersive spectroscopy (EDS). Heating temperatures are 250°C, 300°C, and 350°C and for each temperature, the time was varied between 30, 60, and 90 minutes. The heating time for 30 minutes results in FC 30.777% and calorific value 15 MJ/Kg at temperature 250°C and decreased to 4.004% and 6 MJ/Kg at temperature 350°C, respectively. EDS shows the time of heating is an important parameter which shows the carbon and nitrogen contents were decreasing with the increase in the heating time, and silicon and oxygen contents were increasing with increase in the heating time. XRD shows broad (002) reflections between 20° and 30°, which indicated disordered carbon with small domains of coherent and parallel stacking of the graphene sheets, which is consistent with surface morphology of the SEM image. The experimental results indicated that heating at 300°C for 30 minutes is an effective and efficient parameter for fabrication of low-cost carbon from bamboo leaves which is a source of useful energy.

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来源期刊
International Journal of Biomaterials
International Journal of Biomaterials MATERIALS SCIENCE, BIOMATERIALS-
CiteScore
4.30
自引率
3.20%
发文量
50
审稿时长
21 weeks
期刊最新文献
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