异构体与其他纳米可流动树脂复合材料体外流变特性的比较评价。

Biomaterial investigations in dentistry Pub Date : 2021-11-08 eCollection Date: 2021-01-01 DOI:10.1080/26415275.2021.1996239
Loulwa M Al-Saud
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引用次数: 1

摘要

目的:本研究的目的是确定一组市售的纳米可流动树脂复合材料的粘弹性;并探讨这些性能与材料组成(含氟/不含氟)、填料尺寸描述(纳米填充、纳米杂化和亚微米填充)和填料负载(按体积计算)之间的关系。方法:采用流变仪进行流变学测量。在0.1-100 rad/s的角频率(ω)下,进行了动态扫频测试,以评估复合粘度、储存和损失模量、损失切线和复合剪切模量。对纳米可流动树脂复合材料的流变性能进行了比较评价,并采用单因素方差分析进行了统计分析。结果:试验材料均表现出剪切减薄流动特性。随着剪切速率的增加,纳米可流动复合材料的复合粘度降低。纳米杂化填充可流动树脂复合材料的复合粘度最高,而纳米填充可流动树脂复合材料的复合粘度最低。亚微米填充材料表现出最低的复合剪切模量和损失切线值。结论:本研究结果对不同纳米可流动复合材料的流变性能进行了综合评价。所观察到的被测材料之间流变特性的差异与它们的氟化物含量或填料尺寸无关。此外,所测试的纳米可流动树脂复合材料的复合粘度与填料体积之间没有关系。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Comparative evaluation of Rheological characteristics of Giomers and other Nano-flowable resin composites in vitro.

Objective: The purpose of this research was to determine the viscoelastic properties of a group of commercially available nano-flowable resin composites; and to explore the relation between these properties and the materials' composition (with/without fluoride), filler size description (nano-filled, nanohybrid and submicron-filled) and filler loading (by volume).

Methods: Rheological measurements were performed using a rheometer. A Dynamic frequency sweep test was conducted to evaluate the complex viscosity, storage and loss moduli, loss tangent, and complex shear modulus at an angular frequency (ω) of 0.1-100 rad/s. Comparative evaluations of the nano flowable resin composites on rheological properties was performed, and statistically analyzed using one-way ANOVA.

Results: The results indicated that all the tested materials exhibited shear-thinning flow behaviour. As the shear rate increased, the complex viscosity of the nano-flowable composites decreased. The nanohybrid filled flowable resin composites exhibited the highest complex viscosity, while the nano-filled flowable resin composites exhibited the lowest value. The submicron-filled materials exhibited the lowest complex shear moduli and loss tangent values. Conclusions: The findings from the current study provided comprehensive evaluation of the rheological properties of different nano-flowable composites. The observed differences in rheological properties among the tested materials were independent of their fluoride content or filler size. Furthermore, no relationship was found between the complex viscosity of the tested nano-flowable resin composites and their filler volume.

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