沸石在二甲基乙醇胺衍生的二季烷基铵盐存在下的结晶

IF 1.3 4区工程技术 Q3 CHEMISTRY, ORGANIC Petroleum Chemistry Pub Date : 2021-07-08 DOI:10.1134/S0965544121080089

D. E. Tsaplin, E. R. Naranov, L. A. Kulikov, I. S. Levin, S. V. Egazar’yants, A. L. Maximov, E. A. Karakhanov

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引用次数: 2

摘要

采用基于季铵盐的有机模板，水热法制备了不同结构类型(MFI、MEL、MTW)的含沸石材料。通过x射线衍射分析、低温氮吸附-解吸、程序升温氨解吸、红外光谱、扫描电镜、x射线荧光分析、透射电镜、固态27Al核磁共振光谱和吸附吡啶的红外光谱对材料进行了表征。揭示了模板对所得材料结构的影响。

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Crystallization of Zeolites in the Presence of Diquaternary Alkylammonium Salts Derived from Dimethylethanolamine

Zeolite-containing materials of various structural types (MFI, MEL, MTW) were prepared by the hydrothermal method using organic templates based on quaternary polymethylenediammonium salts. The materials were characterized by X-ray diffraction analysis, low-temperature nitrogen adsorption–desorption, temperature-programmed ammonia desorption, IR spectroscopy, scanning electron microscopy, X-ray fluorescence analysis, transmission electron microscopy, solid-state ²⁷Al NMR spectroscopy, and IR spectroscopy of adsorbed pyridine. The effect of the template on the structure of the material obtained was revealed.

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来源期刊

Petroleum Chemistry 工程技术-工程：化工

CiteScore

2.50

自引率

21.40%

发文量

102

审稿时长

6-12 weeks

期刊介绍： Petroleum Chemistry (Neftekhimiya), founded in 1961, offers original papers on and reviews of theoretical and experimental studies concerned with current problems of petroleum chemistry and processing such as chemical composition of crude oils and natural gas liquids; petroleum refining (cracking, hydrocracking, and catalytic reforming); catalysts for petrochemical processes (hydrogenation, isomerization, oxidation, hydroformylation, etc.); activation and catalytic transformation of hydrocarbons and other components of petroleum, natural gas, and other complex organic mixtures; new petrochemicals including lubricants and additives; environmental problems; and information on scientific meetings relevant to these areas. Petroleum Chemistry publishes articles on these topics from members of the scientific community of the former Soviet Union.