Aderibigbe F Alade, Adewoye Tunmise Latifat, M. S. Ishola, M. Alhassan, Saka H. Bamidele, Ajala Elijah Olawale, Oluwaseyi Soile Samuel
{"title":"膨润土负载铁钴镍三金属纳米颗粒的非均相催化","authors":"Aderibigbe F Alade, Adewoye Tunmise Latifat, M. S. Ishola, M. Alhassan, Saka H. Bamidele, Ajala Elijah Olawale, Oluwaseyi Soile Samuel","doi":"10.29081/jesr.v27i3.282","DOIUrl":null,"url":null,"abstract":"Herein, the synthesis and characterization of a bentonite-supported Fe-Co-Ni trimetallic nanocatalyst applied in transesterification reaction was reported. The synthesized heterogeneous catalyst was used to investigate the production of biodiesel by varying the reaction parameters using Box-Behnken design response surface methodology (RSM-BBD). An optimum biodiesel yield of 95.2 % was obtained at methanol to oil ratio of 10:1, reaction time of 2 hours, reaction temperature of 55 and catalyst concentration of 5 % (w/w of the oil). The biodiesel produced was later analysed using GC-MS analysis and the results shows a fatty acid methyl esters (FAME) profile that confirms the presence of biodiesel.","PeriodicalId":15687,"journal":{"name":"Journal of Engineering Studies and Research","volume":" ","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-01-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"HETEROGENEOUS CATALYSIS USING BENTONITE-SUPPORTED Fe-Co-Ni TRIMETALLIC NANOPARTICLES\",\"authors\":\"Aderibigbe F Alade, Adewoye Tunmise Latifat, M. S. Ishola, M. Alhassan, Saka H. Bamidele, Ajala Elijah Olawale, Oluwaseyi Soile Samuel\",\"doi\":\"10.29081/jesr.v27i3.282\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Herein, the synthesis and characterization of a bentonite-supported Fe-Co-Ni trimetallic nanocatalyst applied in transesterification reaction was reported. The synthesized heterogeneous catalyst was used to investigate the production of biodiesel by varying the reaction parameters using Box-Behnken design response surface methodology (RSM-BBD). An optimum biodiesel yield of 95.2 % was obtained at methanol to oil ratio of 10:1, reaction time of 2 hours, reaction temperature of 55 and catalyst concentration of 5 % (w/w of the oil). The biodiesel produced was later analysed using GC-MS analysis and the results shows a fatty acid methyl esters (FAME) profile that confirms the presence of biodiesel.\",\"PeriodicalId\":15687,\"journal\":{\"name\":\"Journal of Engineering Studies and Research\",\"volume\":\" \",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-01-10\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Engineering Studies and Research\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.29081/jesr.v27i3.282\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Engineering Studies and Research","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.29081/jesr.v27i3.282","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
HETEROGENEOUS CATALYSIS USING BENTONITE-SUPPORTED Fe-Co-Ni TRIMETALLIC NANOPARTICLES
Herein, the synthesis and characterization of a bentonite-supported Fe-Co-Ni trimetallic nanocatalyst applied in transesterification reaction was reported. The synthesized heterogeneous catalyst was used to investigate the production of biodiesel by varying the reaction parameters using Box-Behnken design response surface methodology (RSM-BBD). An optimum biodiesel yield of 95.2 % was obtained at methanol to oil ratio of 10:1, reaction time of 2 hours, reaction temperature of 55 and catalyst concentration of 5 % (w/w of the oil). The biodiesel produced was later analysed using GC-MS analysis and the results shows a fatty acid methyl esters (FAME) profile that confirms the presence of biodiesel.