用纳米纤维素改性氧化石墨烯制备纳米复合材料

IF 0.3 Q4 CHEMISTRY, MULTIDISCIPLINARY Chemical Bulletin of Kazakh National University Pub Date : 2021-09-22 DOI:10.15328/cb1238
K. Akatan, T. Kuanyshbekov, S. Kabdrakhmanova, Aidana Imasheva, A. Battalova, R. Abylkalykova, A. Nasyrova, Zhanar Ibraeva
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引用次数: 3

摘要

纳米复合材料的深入研究有助于开发医学、纳米电子学、能源、生物技术、信息技术等领域的新材料。因此,用纳米纤维素对氧化石墨烯(GO)进行改性合成新材料及其性能研究具有重要意义。本研究以活性炭(BAU-A)为原料,以1:1体积比的氧化石墨烯(GO)与一年生植物大麻茎中的纳米纤维素(NC)进行改性,合成了纳米复合材料,并用FTIR和UV光谱对其化学结构进行了研究。研究结果表明,在全长243nm的紫外光谱中,醚化键C=O被吸收。红外光谱在1625cm-1波长处显示了所有新的醚键O=C-OH。GO的平均粒径为352nm,NC的长度为470nm,宽度为80nm。SEM分析表明NC是GO层的超低厚度之间的接触层。XRD分析表明,GO-NC复合膜是一种由GO和NC组成的物质。结果表明,氧化石墨烯的改性表明其范围可以尽可能扩大。
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Synthesis of nanocomposite material through modification of graphene oxide by nanocellulose
Intensive research of nanocomposites contributes to the development of new materials in the fields of medicine, nanoelectronics, energy, biotechnology, information technology. Therefore, the synthesis of new materials by modifying of graphene oxide (GO) with nanocellulose and the study of its properties are of great interest. In this study synthesized nanocomposite material by modifying of graphene oxide (GO) from activated carbon (BAU-A) in a 1:1 volume ratio with nanocellulose (NC) from hemp stems belonging to the annual plant, and their chemical structure was studied by FTIR and UV-spectroscopy. The results of the study showed the absorption of the etheric bond C = O in the UV spectrum at full length 243 nm. The IR spectrum showed all the new etheric bonds O = C - OH at a wavelength of 1625 cm-1. The average particle sizes of GO was 352 nm and NC was 470 nm in length and 80 nm in width. The SEM analysis indicating the NC as a contact layer between ultralow thicknesses of the GO layers. The XRD analysis indicated GO-NC composite film is a substance comprising GO and NC. According to the results, modification of graphene oxide showed that its scope can be expanded as much as possible.
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审稿时长
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